共查询到19条相似文献,搜索用时 78 毫秒
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亚临界水提取技术(SCWE),是一种以亚临界水(SCW)为提取溶剂的新型提取技术,具有高效、绿色等优势。本文在简要介绍亚临界水的基础上,综述了其在生物活性物质提取,环境、食品中有害成分提取检测等方面的研究进展,并概述了提取过程的影响因素,以及与多种辅助强化技术联用的研究结果。最后展望了其未来可能的发展方向,为该技术的进一步发展及实际应用提供参考。 相似文献
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亚临界水萃取紫草中左旋/右旋紫草素的工艺优化 总被引:2,自引:0,他引:2
研究了亚临界水萃取技术富集紫草中左旋/右旋紫草素的工艺过程,采用响应曲面法对影响紫草素提取率的工艺参数进行分析优化.考察了萃取温度、萃取时间和固液比对紫草素提取率的影响,结果发现三个因素在各自考察的实验范围内均有显著影响.采用可见分光光度法对亚临界水提取液中紫草素的浓度进行分析,在510 nm波长下测得的标准线性方程为y=24.77x+0.0311,相关系数为0.9905,紫草素浓度的线性范围是0.0084~0.0540 mg·mL-1.响应曲面分析模型预测的最佳提取条件是:固液比为7.875 g·L-1,在20 MPa、117.5℃下提取18 min,此时紫草素最大提取率是2.02 mg·g-1,与模型预测值基本相符.采用亚临界水萃取紫草素具有高效、环保、操作简便等优势,利用响应曲面设计能够有效地优化萃取过程,为该技术的推广提供了一定的理论支持. 相似文献
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Membrane-supported liquid-liquid extraction uses artificial membranes for the generation of a phase interface between the two liquid phases involved in extraction. Additional equipment for the generation of droplets as well as phase separation afterwards is no longer necessary. Since the membranes used for this special type of extraction are quite well described concerning thickness, porosity, tortuosity and material it is possible to generate information about the diffusion coefficient of the component to be extracted within the preferred solvent from extraction trails easily. This article describes an experimental set-up for both the proof of principle of membrane-supported liquid-liquid extraction and, using a dedicated computer-aided data treatment, how to calculate the overall mass transfer coefficient as well as the diffusion coefficient for a given system within moderate testing duration. 相似文献
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D. K. Bredeson 《Journal of the American Oil Chemists' Society》1978,55(11):762-764
The mechanical screw press was the principal means of extracting vegetable oilseeds in the United States from the 1930s through
the 1940s and 1950s. Then the utilization of solvent extraction cut drastically into their use for full extraction, but created
a great demand for screw presses for prepressing of high oil content seeds for solvent extraction. However, use of the screw
press for full extraction has been increasing over the years in the less developed countries, and is the main modern machine
utilized for some products such as palm fruit. Today ever larger and more efficient machines are being developed for full
extraction and pre-pressing of vegetable oilseeds and fruits. 相似文献
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Comparison of membrane extraction with traditional extraction methods for biodiesel production 总被引:1,自引:0,他引:1
Three traditional methods for the refining step in biodiesel production were compared: (i) washing with distilled water; (ii)
washing with acid (HCl); and (3) dissolving and extracting in a solvent (hexane or petroleum ether) and then washing with
distilled water. Biodiesel with a high purity (97.5%) could be obtained by all three methods, but serious emulsification occurred
during the refining processes, which led to high refining losses. A novel refining method was developed by using hollow fiber
membrane extraction, and polysulfone was selected as the most suitable membrane. This process effectively avoided emulsification
during refining and decreased the refining loss. The purity of the biodiesel obtained was about 99%; and other properties,
such as density, kinematic viscosity, water content, and acid value, conformed to the standards. 相似文献
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W. Becker 《Journal of the American Oil Chemists' Society》1978,55(11):754-761
The removal of edible oils from oilseeds was practiced by the Egyptians many centuries ago. Some of the developments leading
to today’s worldwide extraction industry are discussed, and a brief history of the industry in the United States from 1940
to the present is included. The theory of solvent extraction is outlined in practical terms. Several types of solvent extraction
and desolventizing systems are explained. Also, typical preparation and extraction processes for presscake, soybeans, and
some high oil content seeds are illustrated. Some reasons for taking extra precautions in the preparation process and the
desolventizing process when producing human edible soy protein products are explained. Energy conservation suggestions are
included. 相似文献
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Multistep extraction of coal 总被引:3,自引:0,他引:3
Unlike many natural and synthesized polymers, coal is a mixture of polyfunctional high-molecular-mass material. The usually observed limited extractability of coal is attributed to the disregard of various relatively strong intra- and intermolecular interactions and their co-operativity. Due to the polyfunctionality, ionic, charge-transfer and so-called π-π interactions are present, and their abundances are highly rank-dependent. Such relatively strong interactions are not completely solvated in a single step with any solvent. In this paper, multistep extraction was studied to solvate these interactions. Pyridine was mostly used after treatments to disrupt these interactions without breaking covalent bonds. Much larger pyridine extractability was obtained compared to a single step extraction. As solubilization or extraction is the first step to characterize coal, caution is advised against the limited extractability obtained by conventional procedures. 相似文献
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