Static and fatigue characterisation of new basalt fibre reinforced composites

Basalt reinforced composites are recently developed materials. These mineral amorphous fibres are a valid alternative to carbon fibres for their lower cost, and to glass fibres for their strength. In order to use basalt reinforced composites for structural applications, it is necessary to perform a mechanical characterisation. With this aim in the present work experimental results of several static and fatigue tests are described. Two polymeric matrices are taken into account, vinylester and epoxy, to assess their influence on the evaluated parameters. In parallel to these mechanical tests, also the thermal answer of the specimens to mechanical loads is evaluated by means of thermography. This experimental technique allows defining the composite local heating during the application of mechanical loads and its behaviour in details. Final discussion on obtained results is proposed focussing the attention on basalt fibre composite behaviour, and comparing mechanical properties of BFRP with other composite materials in glass and carbon fibres.     

Fatigue analysis of unidirectional GFRP composites under combined bending and torsional loads

Fatigue behavior of unidirectional glass fiber reinforced polyester (GFRP) composites at room temperature under in-phase combined torsion/bending loading was investigated. All fatigue tests were carried out on constant-deflection fatigue machine with frequency of 25 Hz. A 30% reduction from the initial applied moments was taken as a failure criterion in the combined torsion/bending fatigue tests of the composite materials. A series of pure torsional fatigue tests were conducted to construct the failure contour of GFRP composites using different failure theories. The obtained S–N curves from combined torsion/bending tests were compared with both, pure torsion fatigue test results and published results of pure bending fatigue tests of GFRP rods. Pictures by scanning electron microscope were used to closely examine the failure mode of the tested specimens under combined torsion/bending loading.

The results showed that, the unidirectional glass fiber reinforced polyester composites have poor torsional fatigue strength compared with the published results of pure bending fatigue strength. Endurance limit value (calculated from S–N equation at N = 10⁷ cycles) of GFRP specimens tested under combined torsion/bending loading equals 8.5 times the endurance limit of pure torsion fatigue. On the other hand the endurance limit of combined torsion/bending fatigue strength approximately half the fatigue limit of pure bending fatigue strength. The predicted values of combined torsion/bending fatigue strength at different number of cycles, using the published failure theory are in good agreement with the experimental data. For the investigated range of fiber volume fractions (V_f) it was found that higher stress levels are needed to produce fatigue failure after the same number of cycles as V_f increases.     

Fatigue at high number of cyclic loads: Testing methods and failure mechanism

A significant proportion of machinery and equipment is operated up to a number of cycles greater 10⁸, which is in the range of conventionally fatigue limit design. For materials with a face‐centred cubic crystal lattice and for high‐strength steels with a body‐centred cubic crystal lattice fatigue failures were observed even in the Very High Cycle Fatigue (VHCF) regime of load‐cycles greater N = 10⁷. To reduce the testing time in the VHCF regime, one possibility is to perform the tests at a higher frequency. In addition to the typical servo‐hydraulic testing machines or resonant fatigue testing machine with test frequencies up to f = 400 Hz, ultrasonic fatigue testing machines with frequencies up to f = 20 kHz were used. In different comparative investigations it was shown that the testing method has a significant influence on fatigue life and fatigue strength. In this paper the influence of the testing method and test frequency on fatigue behaviour in the VHCF regime is presented using the example of steels and aluminium alloys and different hypotheses for the decrease in fatigue strength in this area are discussed.     

Fatigue crack propagation behavior of RC beams strengthened with CFRP under cyclic bending loads

A fatigue crack propagation equation of reinforced concrete (RC) beams strengthened with a new type carbon fiber reinforced polymer was proposed in this paper on the basis of experimental and numerical methods. Fatigue crack propagation tests were performed to obtain the crack propagation rate of the strengthened RC beams. Digital image correlation method was used to capture the fatigue crack pattern. Finite element model of RC beam strengthened with carbon fiber reinforced polymer was established to determinate J‐integral of a main crack considering material nonlinearities and degradation of material properties under cyclic loading. Paris law with a parameter of J‐integral was developed on the basis of the fatigue tests and finite element analysis. This law was preliminarily verified, which can be applied for prediction of fatigue lives of the strengthened RC beams.     

Fatigue behavior and modeling of short fiber reinforced polymer composites: A literature review

Applications of short fiber reinforced polymer composites (SFRPCs) have been rapidly increasing and most of the components made of these materials are subjected to cyclic loading. Therefore, their fatigue behavior and modeling have been of much interest in recent years. This literature review presents a broad review of the many factors influencing cyclic deformation, fatigue behavior, and damage development in SFRPCs. These include microstructural related effects as well as effects related to loading condition and their service environment. Microstructural related effects include those related to fiber length, content and orientation, surface treatment, and failure mechanisms. Cyclic deformation and softening, viscous characteristics, and dissipative response used to characterize and model their fatigue damage behavior and accumulation are discussed. The effects of stress concentrations and their gradient on fatigue behavior are also discussed, due to their significant influence. The effects related to the loading condition include mean stress effects which may be accompanied by cyclic creep, variable amplitude loading, and multiaxial stress effects. Since fatigue behavior is substantially influenced by the testing frequency with self-heating as the primary consequence of increased frequency, this effect is also investigated. Environmental effects considered include the effects of moisture content and temperature, as well as thermo-mechanical fatigue behavior. The effect of welded joints in manufactured components made of SFRPCs and fatigue analysis and life estimation techniques used for such components are also included.     

Fatigue behavior of CoCrFeMnNi high-entropy alloy under fully reversed cyclic deformation

Bulk ultrafine-grained (UFG) CoCrFeMnNi high-entropy alloy (HEA) with fully recrystallized microstructure was processed by cold rolling and annealing treatment. The high-cycle fatigue behaviors of the UFG HEA and a coarse-grained (CG) counterpart were investigated under fully reversed cyclic deformation. The fatigue strength of the UFG HEA can be significantly enhanced by refining the grain size. However, no grain coarsening was observed in the UFG HEA during fatigue tests. Mechanisms for the superior mechanical properties of the UFG HEA were explored.     

Fatigue damage behaviors of carbon fiber-reinforced epoxy composites containing nanoclay

The effects of nanoclay inclusion on cyclic fatigue behavior and residual properties of carbon fiber-reinforced composites (CFRPs) after fatigue have been studied. The tension–tension cyclic fatigue tests are conducted at various load levels to establish the S-N curve. The residual strength and modulus are measured at different stages of fatigue cycles. The scanning electron microscopy (SEM) and scanning acoustic microscopy (SAM) are employed to characterize the underlying fatigue damage mechanisms and progressive damage growth. The incorporation of nanoclay into CFRP composites not only improves the mechanical properties of the composite in static loading, but also the fatigue life for a given cyclic load level and the residual mechanical properties after a given period of cyclic fatigue. The corresponding fatigue damage area is significantly reduced due to nanoclay. Nanoclay serves to suppress and delay delamination damage growth and eventual failure by improving the fiber/matrix interfacial bond and through the formation of nanoclay-induced dimples.     

Evaluation of prestressed basalt fiber and hybrid fiber reinforced polymer tendons under marine environment

This paper studies the degradation of the tensile properties of prestressed basalt fiber-reinforced polymer (BFRP) and hybrid FRP tendons in a marine environment. Two levels of prestressing toward typical prestressing applications were applied in the experiment. The variations of tensile strength, elastic modulus and the relevant coefficient of variation (CV) were first investigated. The effect of prestressing on tensile property degradation was discussed. The characteristics of prestressed hybrid FRP tendons in a marine environment simulated by a salt solution were clarified. Moreover, a prediction model of BFRP tendons with different levels of prestressing in a marine environment was proposed. The results show that the BFRP tendons’ superior resistance to salt corrosion and the degradation rate of their tensile strength is nonlinearly proportional to the prestressing ratios, whereas the elastic modulus remains constant regardless the prestressing ratio and aging duration. Although prestressing on BFRP tendons accelerates degradation, it can still lower the variation of the strength of the BFRP tendon. Hybridization can lower the degradation rate of basalt and carbon FRP (B/CFRP) without prestressing, whereas basalt and steel-wire FRP (B/SFRP) exhibit much faster degradation due to the internal corrosive steel wires. The model regression by the Napierian logarithm equation well represents the degradation trend of BFRP tendons under different levels of prestressing.     

循环荷载作用下钢桥面铺装疲劳损伤失效行为研究

针对钢桥面铺装工程中普遍采用的改性沥青(Stone Matrix Asphalt,SMA)、浇筑式沥青(Guss asphalt,GA)、环氧沥青(Epoxy asphalt,EP)混合料双层铺装结构,进行了循环车载作用下钢桥面与沥青混凝土铺装疲劳损伤特性理论分析与试验研究。基于疲劳损伤度,研究了钢桥面铺装疲劳损伤失效行为和疲劳开裂过程中损伤场、应力和应变场动态演变机制,推导出疲劳失效时的损伤场、应力和应变场计算表达式,并给出钢桥面铺装疲劳寿命理论公式。以三座钢箱梁桥桥面铺装(润扬长江大桥2005,南京长江三桥2005,苏通大桥2008)为例,对不同铺装结构组合方案下的复合梁进行疲劳试验分析和使用寿命理论预测。实例研究结果表明,钢桥面铺装疲劳损伤失效行为预估模型合理可行;相较于改性沥青、浇筑式沥青,环氧沥青混合料具有较强高的强度低变形能力,更适合于大跨径钢桥面铺装抗疲劳的设计要求;由环氧沥青混合料组合而成的“双层环氧沥青混凝土”和“浇注式沥青混凝土(下层)+环氧沥青混凝土(上层)”的抗疲劳性能优于其它沥青混合料铺装结构组合方案,同等厚度组合情况下疲劳使用寿命可延长1倍~2倍以上;“双层环氧沥青混凝土”已应用于润扬长江大桥、南京长江三桥和苏通长江大桥钢桥面工程,并已成功运行10年以上,其跟踪观测结果良好。     

Fatigue of cemented hip replacements under torsional loads

Fatigue resistance of hip replacement prostheses is becoming ever more important as the operation is carried out on younger and more active patients. Torsional loading of the implant, which occurs especially during activities, such as rising from a chair or climbing stairs, is implicated in the failure process. To examine fatigue failure of the implant–bone fixation, which is made using polymethylmethacrylate cement, an experimental model was designed and 16 specimens tested at torsional moments of 50 Nm and 80 Nm to both 1 and 2 million cycles. The numbers and lengths of cracks initiated under cyclic loading were quantified using dye penetrant to highlight the cracks and a profile projector to magnify them. The majority of cracks initiated from the PMMA/metal and PMMA/bone interfaces, more often than from pores in the PMMA. A bimaterial fracture mechanics analysis confirmed that the interfaces are too weak to sustain in vivo levels of cyclic loading. It is proposed that, under torsional loading, fatigue failure of PMMA fixated implants originates from pores located on the interfaces.     

Fatigue behavior and modeling of short fiber reinforced polymer composites including anisotropy and temperature effects

Effects of anisotropy and temperature on cyclic deformation and fatigue behavior of two short glass fiber reinforced polymer composites were investigated. Fatigue tests were conducted under fully-reversed (R = −1) and positive stress ratios (R = 0.1 and 0.3) with specimens of different thicknesses, different fiber orientations, and at temperatures of −40 °C, 23 °C, and 125 °C. In samples with 90° fiber orientation angle, considerable effect of thickness on fatigue strength was observed. Effect of mold flow direction was significant at all temperatures and stress ratios and the Tsai–Hill criterion was used to predict off-axis fatigue strengths. Temperature also greatly influenced fatigue strength and a shift factor of Arrhenius type was developed to correlate fatigue data at various temperatures, independent of the mold flow direction and stress ratio. Micromechanisms of fatigue failure at different temperatures were also investigated. Good correlations between fatigue strength and tensile strength were obtained and a method for obtaining strain–life curves from load-controlled fatigue test data is presented. A fatigue life estimation model is also presented which correlates data for different temperatures, fiber orientations, and stress ratios.     

Mechanical,thermal expansion,and flammability properties of co-extruded wood polymer composites with basalt fiber reinforced shells

Basalt fiber (BF) filled high density polyethylene (HDPE) and co-extruded wood plastic composites (WPCs) with BF/HDPE composite shell were successfully prepared and their mechanical, morphological and thermal properties characterized. The BFs had an average diameter of 7 μm with an organic surfactant surface coating, which was thermally decomposed at about 210 °C. Incorporating BFs into HDPE matrix substantially enhanced flexural, tensile and dynamic modulus without causing a noticeable decrease in the tensile and impact strength of the composites. Micromechanical modeling of tensile properties for the BF/HDPE composites showed a good fit of the selected models to the experimental data. Compared to neat HDPE, BF/HDPE composites had reduced linear coefficient of thermal expansion (LCTE) values. The use of the pure HDPE and BF/HDPE layers over a WPC core greatly improved impact strength of core–shell structured composites. However, the relatively less-stiff HDPE shell with large LCTE values decreased the overall composite modulus and thermal stability. Both flexural and thermal expansion properties were enhanced with BF reinforced HDPE shells, leading to well-balanced properties of core–shell structured material. Cone calorimetry analysis indicated that flammability performance of core–shell structured composites was improved as the BF content increased in the shell layer.     

Fatigue behavior of laminated composites with a circular hole under in-plane multiaxial loading

A modified fiber failure fatigue model is presented for characterizing the behavior of laminated composites with a central circular hole under in-plane multiaxial fatigue loading. The analytical model presented is based on minimum strength model and fiber failure criterion under static loading available in the literature. The analysis starts with the determination of location of a characteristic curve around the hole and the stress state along the characteristic curve under in-plane multiaxial fatigue loading. Number of cycles to failure and location of failure are determined under given fatigue loading condition. Based on ply-by-ply analysis, ultimate fatigue failure and the corresponding number of cycles are determined. Analytical predictions are compared with the experimental results for uniaxial and multiaxial fatigue loading cases. A good match is observed. Further, studies are carried out for different in-plane biaxial tension–tension and biaxial compression–compression loading cases.     

Experimental and numerical modeling of basalt textile reinforced mortar behavior under uniaxial tensile stress

During the last years several projects and studies have improved the knowledge about textile reinforced mortar (TRM) technology. TRM has already been used in strengthening masonry and reinforced concrete structural elements such as walls, arches, columns and beams. This material is presented as a real alternative to the use of fiber-reinforced polymers (FRP) in situations where these composites have presented some drawbacks or their use is banned. Textile reinforced mortar show a complex mechanical behavior derived from the heterogeneity of the constituent materials. This paper aims to deepen the knowledge of this composite material in terms of tensile behavior.Following this scope, this paper presents an experimental campaign focused on thirty-one TRM specimens reinforced with four different reinforcing ratios. The results are analyzed and contrasted with two distinct models. (i) The Aveston–Cooper–Kelly theory (ACK) which is based on a tri-linear analytical approach; and (ii) a non-linear numerical simulation with a 3D finite element code.The finite element analysis (FEA) of the TRM tensile tests also showed no significant dependence on the basalt-to-mortar interface, i.e., the choice of a bond-slip curve in order to reproduce the bond stresses and slippages along the interface is irrelevant and it can be simply considered as rigid interface.     

Deformation behaviour of elastomeric matrix composites under static loading conditions

Damage mechanisms of elastomeric matrix composites (EMCs), propose a complex interplay between material properties and service conditions. The occurrence of defects such as the cavitations in EMCs specimens in using conditions is an important problem. This situation requires the well understanding of the damage mechanisms of EMCs used in automotive and aeronautical fields.Elastomeric matrix composites subjected to static and fluctuating loads basically fail due to the initiation and growth of defects (cracks, cavities, etc.). In fact, high hydrostatic pressures influence mechanical behaviours of EMCs. This paper reviews the damage mechanism of EMCs under static loading. In order to evaluate mechanical properties and fracture behaviour of EMCs, in situ observations were made by using X-rays computed tomography (CT). Two types of specimens are investigated in this work; Natural rubber, NR vulcanised and reinforced by carbon black, and synthetic rubber (styrene-butadiene-rubber), SBR. A detailed study was carried out by scanning electron microscopy (SEM) for a better understanding the damage mechanisms and confirming the CT results.     

Fatigue behavior of Zr-based bulk-metallic glasses

The objective of this paper was to study the fatigue characteristics of zirconium (Zr)-based bulk-metallic glasses (BMGs) and to investigate the mechanisms of fatigue-crack initiation, crack propagation, and fracture in BMGs. The fatigue ratios (fatigue limit/tensile strength) (0.30–0.55) of Zr-based BMGs were found to be generally comparable with those of crystalline alloys, such as steel and titanium alloys. Fatigue cracks typically initiate from shear bands, inclusions, and/or porosities. The striations resulting from the blunting and resharpening of the fatigue-crack tip formed in the fatigue-crack-growth region. The fine striation spacing seems to be comparable to that of the crystalline alloys.     

Analysis of the strain-rate behavior of a basalt fiber reinforced natural hydraulic mortar

Fiber reinforced inorganic materials, such as concrete or mortars are expected to present good mechanical properties under high dynamic loading conditions, such as those induced by earthquakes. Furthermore, basalt fibers, which are being increasingly investigated in structural applications, are also expected to present good performance under high strain-rate conditions.This paper presents the results of a dynamic characterization of a basalt fiber reinforced natural hydraulic mortar, in order to verify its capability to withstand high dynamic loading conditions. In particular, the reinforced mortar was morphologically characterized by SEM and mercury intrusion porosimetry; then, quasi-static flexural and tensile tests were conducted. Finally, dynamic tensile failure tests were carried out at medium and high strain-rates, using a Hydropneumatic machine and a Modified Hopkinson bar apparatus, respectively. The results were elaborated to derive Dynamic Increase Factors for the tensile strength.The fiber addition leads to a bridge action effect, and consequently to a more ductile behavior and higher toughness of the fiber reinforced mortar compared to a plain mortar. In addition, the fiber reinforced mortar appears to be highly strain-rate sensitive, as the tensile strength DIF increased up to 5.1, for a high strain-rate of about 10² s⁻¹.     

Fatigue behavior of aluminum alloys under biaxial loading

The biaxiality effect, especially the effect of non-singular stress cycling, on the fatigue behavior was studied, employing cruciform specimens of aluminum alloys 1100-H14 and 7075-T651. The specimens, containing a transverse or a 45^o inclined center notch, were subjected to in-phase (IP) or 100% out-of-phase (hereinafter referred to as “out-of-phase or OP”) loading of stress ratio 0.1 in air. The biaxiality ratio λ ranged from 0 to 1.5, and 3 levels of stress were applied. It was observed that: (1) at a given λ, a lower longitudinal stress induced a longer fatigue life under IP and OP loading, and the fatigue life was longer under IP loading, (2) the fatigue crack path profile was influenced by λ, phase angle (0^o or 180^o), and initial center notch (transverse or 45^o inclined); (3) the fatigue crack path profiles, predicted analytically and determined experimentally, had similar features for the specimens with a transverse center notch under IP loading; and (4) the fatigue crack growth rate was lower and the fatigue life longer for a greater λ under IP loading, whereas it changed little with change in λ under OP loading. These results demonstrate that non-singular stress cycling affects the biaxial fatigue behavior of aluminum alloys 1100-H14 and 7065-T651under IP and OP loading.     

Special manufacturing and characteristics of basalt fiber reinforced hybrid polypropylene composites: Mechanical properties and acoustic emission study

Basalt fiber reinforced, polypropylene matrix hybrid composites were manufactured in the process of carding, needle-punching and pressing. Hemp, glass and carbon fibers were applied besides basalt fiber in these composites. In order to achieve a sufficient interfacial adhesion, the fibers were treated with the reaction mixture of maleic acid anhydride and sunflower oil. The hybrid effect in these composites was examined as a function of fiber content and fiber combination. The strength properties of hybrid composites improved owing to surface treatment and this was proven by mechanical tests and microscopic analysis, as well. Acoustic emission methods revealed that there is a correlation between the physical parameters of sound waves that occurred during failure and the mechanical properties.     

Characterization of strain-softening behavior and failure mechanisms of composites under tension and compression

A methodology is presented to directly measure the damage properties and strain softening response of laminated composites by conducting over-height compact tension (OCT) and compact compression (CC) tests. Through the use of digital image correlation (DIC) technique, and analysis of the measured surface displacement/strain data, the strain-softening response of composites is constructed. This method leads to a direct determination of the Mode I translaminar fracture properties with the assumption that the shear stress is negligible around the damage zone and the crack growth occurs in the symmetric opening mode. Using this methodology, and by correlating the observed failure mechanisms with the strain-softening curves, the interaction of failure mechanisms leading to the final failure and also the distinction between the tensile and compressive failure mechanisms can be studied. The effectiveness of the method in accurate identification of the damage parameters is demonstrated through sectioning and deplying techniques. As a consistency check and further verification of the method, the obtained strain-softening curves are fed into a numerical damage mechanics model and successfully used to simulate the detailed response of the very same OCT and CC specimens from which the strain-softening curves were extracted.