Experimental and numerical analysis of oil shale drying in fluidized bed

The main objective of this work was to experimentally and numerically investigate the Liu Shu River oil shale drying by the means of flue gas in a fluidized bed dryer. Several experiments were performed under different temperatures conditions. The moisture content of oil shale was measured during the experiments. The two-stage drying model was incorporated in computational fluid dynamics (CFD) package FLUENT via user-defined functions (UDF) and utilized for simulation of heat and mass transfer of oil shale drying in the fluidized bed dryer. The simulation results for solid moisture content agreed well with experimental data. The effects of the temperature and velocity of flue gas, initial bed height, and the particle size on the drying characteristics were predicted and analyzed. It is shown that the gas temperature and velocity are the important parameters in the whole drying process. The particle size has more obvious influence in the falling drying period than the constant drying period. The temperatures of gas and solid phases were monitored. It is shown that the so-called “near gas distributor zone” is the most effective heat transfer zone, which agrees well with the calculated value. The system quickly reached thermal equilibrium, characterizing a nearly isothermal bed. The developed model provides a very good demonstration to describe the oil shale drying in the fluidized bed dryer, and may provide important information for design, optimization of operation conditions.     

Modelling of batch fluidised bed drying of pharmaceutical granules

This paper presents a mathematical model based on a three-phase theory, which is used to describe the mass and heat transfer between the gas and solids phases in a batch fluidised bed dryer. In the model, it is assumed that the dilute phase (i.e., bubble) is plug flow while the interstitial gas and the solid particles are considered as being perfectly mixed. The thermal conductivity of wet particles is modelled using a serial and parallel circuit. The moisture diffusion in wet particles was simulated using a numerical finite volume method. Applying a simplified lumped model to a single solid particle, the heat and mass transfer between the interstitial gas and solid phase is taken into account during the whole drying process as three drying rate periods: warming-up, constant rate and falling-rate. The effects of the process parameters, such as particle size, gas velocity, inlet gas temperature and relative humidity, on the moisture content of solids in the bed have been studied by numerical computation using this model. The results are in good agreement with experimental data of heat and mass transfer in fluidised bed dryers. The model will be employed for online simulation of a fluidised bed dryer and for online control.     

Effects of Operating Conditions on the Quality of Mango Pulp Dried in a Spout Fluidized Bed

The influence of process temperature, feed flow rate and spout, and annular gas velocity on the drying process of mango pulp in a spout fluidized bed dryer was evaluated using a full factorial design. The process was carried out with an intermittent paste flow rate since the high sugar concentration of the fruit led to bed collapse using continuous feeding. The drying performance was assessed by the efficiency of powder production, product moisture, feed, and process time. The final product quality was evaluated by color, vitamin C, and carotenoid content. High process temperatures provided a better drying performance and product quality.     

Experimental Study and Mathematical Modeling of Green Pea Drying in a Spouted Bed

In this study, green pea drying is investigated experimentally in a laboratory-scale spouted bed dryer. A mathematical model is also developed to investigate the effect of operating conditions on the performance of the system. The effect of operating parameters such as inlet air temperature, particle size, and flow rate of the drying air on the performance of the dryer are studied experimentally. In order to build the process model, it is necessary to analyze the transport in both solid and gas phases. A complete set of equations with no adjustable parameters is derived for existing zones in the spouted bed dryer in order to predict variations in the temperature and moisture content of the solid and gas phases with time for batch drying conditions. Model results are compared with corresponding experimental data. Agreement between the model results and experimental data is good.     

CFD Modeling of Microwave-Assisted Fluidized Bed Drying of Moist Particles Using Two-Fluid Model

The drying behavior of moist spherical particles in a microwave-assisted fluidized bed dryer was simulated. The two-fluid Eulerian model incorporating the kinetic theory of granular flow was applied to simulate the gas–solid flow. The simulations were carried out using the commercial computational fluid dynamics (CFD) package Fluent 6.3.26. The effects of different levels of microwave power densities as well as initial gas temperature on the prediction of solids moisture content, gas temperature, and gas absolute humidity were investigated. The effect of microwaves was incorporated into calculations using a concatenated user-defined function (UDF). The simulation results were compared with experimental data obtained from drying of soybeans in a pilot-scale microwave-assisted fluidized bed dryer and reasonable agreement was found. The mean relative deviation for prediction of solids moisture content, gas temperature, and gas absolute humidity were less than 3, 10, and 5%, respectively. Further work is needed to validate the proposed model for large-scale plants.     

Drying characteristics of millet in a continuous multistage fluidized bed

The effects of gas velocity, inlet gas temperature and the solid feed rate on the drying efficiency, the outlet solid moisture content, bed temperature in each stage, the outlet gas humidity and temperature in a rectangular acryl multistage fluidized bed (0.172 m×0.192 m×1.5 m-high) with a downcomer (0.04 m-I.D.) were investigated. The experiments were performed by using 1.9 mm millet particles. The final moisture contents of the solids increased with increasing the solid feed rate. The drying efficiency increased with increasing the wetted solid feed rate but decreased with increasing the inlet gas temperature. The drying performance of the multistage fluidized bed was compared with the single-stage fluidized bed and found to be superior under identical operation conditions. The model predicted values were well matched with the experimental data in the multistage fluidized bed dryer. This paper is dedicated to Professor Dong Sup Doh on the occasion of his retirement from Korea University.     

循环流化床中C类颗粒连续干燥的研究

循环流化床(CFB)作为一种新兴反应器,其结构简单、气固接触效率高、处理量大,成为气固二相干燥应用研究的新方向.文中在自建的循环流化床(内径0.104 m×高2.35 m)内,以玉米淀粉(dp=8 μm,ρp=800 kg/m3)为C类颗粒,进行了连续干燥.实验初步研究了进料速率、进风温度及气速等操作参数对淀粉平均停留...     

A COMPREHENSIVE MATHEMATICAL AND NUMERICAL MODELING OF DEEP-BED GRAIN DRYING

This paper deals with comprehensive mathematical and numerical modeling of deep-bed grain drying. In order to build the process model, it is necessary to analyze the transport in both grain and gas phases. Experimental works were carried out for a layer of grain bed in order to validate the models. The models consider momentum, energy, and mass conservation within grain and drying air phase. The two-dimensional dynamic equations of energy and mass conservation are solved numerically by finite-difference method (FDM) and utilizing alternating direction implicit algorithm within grain and drying air phase, while momentum conservation are solved by finite difference method by utilizing Semi-Implicit Method for Pressure-Linked Equations (SIMPLE) algorithm. Furthermore, the models will be applied in consideration with developing and designing dryer in order to simulate humidity and temperature profiles of the drying gas together with moisture content and temperature of grain across dryer in term of the dryer performance. The simulations show that the models can be used to predict the dynamic drying characteristic profiles as well as the superficial velocity of drying air phase across dryer.     

Comparison of Moving Bed Dryers of Solids Operating in Parallel and Counterflow Modes

Abstract

The drying rates in moving bed dryers are compared. The gas and the solids to be dried are in parallel flow or counterflow. A new simplified method to simulate the drying in parallel and counterflow moving beds is developed. This model is based on the solution of arbitrary experimental or theoretical drying rate Equations of single solid particles (or thin-layer drying rate equation) coupled with heat and mass conservation Equations of the dryer. The solution is presented in an integral form of the drying equation showing the relation between time or location in the dryer and degree of drying. The method allows rapid calculation of the moisture, vapor mass fraction, and temperature distributions along the dryer in drying with moist air or steam. The model is demonstrated by using a result based on the receding front evaporation model as the specific thin-layer drying equation in the moving bed model. Wood chips are chosen as an example of the substance to be dried, but the method applies also for other medium, if the dependence of the drying rate on moisture and ambient temperature and humidity (thin layer drying rate) is known. The size of the dryer needed to reach the same degree of drying operating in the parallel mode is much greater than that of counterflow type, when the drying medium is air or flue gases. The reason for the poorer drying in parallel flow is mainly the unfavorable distribution of the evaporation temperature. In steam drying, the difference in the size is not so great, since the evaporation takes place approximately at constant temperature.     

Comparison of Moving Bed Dryers of Solids Operating in Parallel and Counterflow Modes

The drying rates in moving bed dryers are compared. The gas and the solids to be dried are in parallel flow or counterflow. A new simplified method to simulate the drying in parallel and counterflow moving beds is developed. This model is based on the solution of arbitrary experimental or theoretical drying rate Equations of single solid particles (or thin-layer drying rate equation) coupled with heat and mass conservation Equations of the dryer. The solution is presented in an integral form of the drying equation showing the relation between time or location in the dryer and degree of drying. The method allows rapid calculation of the moisture, vapor mass fraction, and temperature distributions along the dryer in drying with moist air or steam. The model is demonstrated by using a result based on the receding front evaporation model as the specific thin-layer drying equation in the moving bed model. Wood chips are chosen as an example of the substance to be dried, but the method applies also for other medium, if the dependence of the drying rate on moisture and ambient temperature and humidity (thin layer drying rate) is known. The size of the dryer needed to reach the same degree of drying operating in the parallel mode is much greater than that of counterflow type, when the drying medium is air or flue gases. The reason for the poorer drying in parallel flow is mainly the unfavorable distribution of the evaporation temperature. In steam drying, the difference in the size is not so great, since the evaporation takes place approximately at constant temperature.     

低阶煤干燥脱水技术的研究

介绍了转筒式干燥工艺、流化床干燥工艺、气流床干燥工艺等蒸发干燥工艺和热力脱水工艺（HTD）、机械热挤压脱水工艺（MTE）、UBC低阶煤干燥提质技术等非蒸发脱水工艺的工艺流程、技术特点及发展现状等。分析了低阶煤脱水工艺系统建设过程中干燥工艺、厂址、干燥介质与能源消耗的选择原则和依据。发现低阶煤干燥脱水工艺的选择应考虑目标用户对产品质量的要求,产品加工工艺对提质煤水分的要求且应尽量选择安全可靠、能耗较小、成本较低的干燥技术。厂址的选择需多方面综合考虑。干燥介质的选择应因地制宜,同时必须综合考虑干燥介质的成本及安全性。较低的干燥能耗才能够保证干燥工艺的长期运行,并产生经济价值。低阶煤干燥脱水技术的研究为低阶煤干燥工艺的选择及良好运行提供参考。     

Moisture readsorption and low temperature oxidation characteristics of upgraded low rank coal

This study investigated the behavior of upgraded low rank coal produced by a coal-oil slurry dewatering process regarding moisture readsorption, low temperature oxidation, and spontaneous combustion. The upgraded low rank coal had higher heating values than raw coal. It also showed lower moisture readsorption than raw coal and had less susceptibility to low temperature oxidation and spontaneous combustion. This seemed to result from the coating of the asphalt on the surface of the coal, which covered fine pores and suppressed the active functional groups from reacting with moisture and oxygen in the air. The increasing upgrading pressure negatively affected the moisture readsorption, low temperature oxidation, and spontaneous combustion.     

用高露点空气干燥小木块时挥发性有机物的释放

Emission of volatile organic compounds (VOCs) during drying of wood particles for particleboard manufacture, or for production of refined biofuels, is a potential environmental problem. The aim of this work is to study the emissions of VOCs during drying, and the influence on the emissions by different drying parameters. The experiments have mainly been done in a batch fluidized bed dryer, but measurements have also been done in a, pilot scale, continuous fluidized bed dryer. The parameters studied are air flow rate through the bed, air temperature, air dewpoint, and bed height. Since the present trend in biofuels and particle drying is towards very high dewpoints during drying, some measurements have been made at dewpoints up to 95℃, corresponding to a water content of 3.2 kg water per kilogram dry air. The emissions have been measured in two different ways, online during drying with a flame ionization detector and through wood analyses of the terpene content in the wood particles before and after dryi     

A COMPREHENSIVE MATHEMATICAL AND NUMERICAL MODELING OF DEEP-BED GRAIN DRYING

ABSTRACT

This paper deals with comprehensive mathematical and numerical modeling of deep-bed grain drying. In order to build the process model, it is necessary to analyze the transport in both grain and gas phases. Experimental works were carried out for a layer of grain bed in order to validate the models. The models consider momentum, energy, and mass conservation within grain and drying air phase. The two-dimensional dynamic equations of energy and mass conservation are solved numerically by finite-difference method (FDM) and utilizing alternating direction implicit algorithm within grain and drying air phase, while momentum conservation are solved by finite difference method by utilizing Semi-Implicit Method for Pressure-Linked Equations (SIMPLE) algorithm. Furthermore, the models will be applied in consideration with developing and designing dryer in order to simulate humidity and temperature profiles of the drying gas together with moisture content and temperature of grain across dryer in term of the dryer performance. The simulations show that the models can be used to predict the dynamic drying characteristic profiles as well as the superficial velocity of drying air phase across dryer.     

油页岩干燥特性实验研究

以柳树河油页岩颗粒为原料,在恒温介质干燥器内进行油页岩干燥动力学研究,考察干燥介质温度和颗粒直径对油页岩干燥性能的影响,采用薄层干燥模型中的Lewis模型,对油页岩干燥实验数据进行模拟,确定油页岩干燥方程和干燥速率方程,建立油页岩干燥常数表达式。研究结果表明:薄层干燥模型中Lewis模型能较好的描述油页岩在恒温介质干燥器内的干燥过程;其干燥过程主要发生在降速干燥阶段;200℃时油页岩无性质变化,干燥达到平衡时,油页岩含水量可降到0.5%左右,油页岩表观活化能为17～19kJ/mol。     

Prediction of Moisture Content Evolution in a Grain Batch Dryer Based on On–line Temperature Measurements

ABSTRACT

The time evolution of the moisture content in a grain batch fluidized bed dryer is estimated by means of an on–line non–linear estimator (Marquardt–Levenberg algorithm). The inputs to the estimation algorithm are on–line temperature measurements and the output is the surface moisture content. The surface moisture content is used for predicting the grain moisture content through the solution of a single ordinary differential equation that combines the moisture and energy balances over the dryer. In this way the drying curves are obtained through incorporating in a very simple model easily obtainable physical information of the process.     

垂直内挡板对流态化流体动力学及谷物干燥特性之影响

The effect of vertical internal baffles on the particle mixing and grain drying characteristics in a batch fluidized bed column is investigated. Experimental work was carried out in a 3 m high rectangular fluidized bed dryer of cross sectional area of 0.15 mx0.61 m at different operating conditions using paddy, a group D particle, as the fluidizing material. The results of the study showed that the fluidized bed dryer system with vertical internal baffles gave better particle mixing effect in the bed of particles than that without vertical internal baffles. This is due to the fact that the vertical internal baffle act as gas bubble breakers by breaking up the large gas bubbles into smaller ones. The smaller bubbles cause a more vigorous mixing in the bed of particles before finally erupting at the bed surface. This improves the contacting efficiency and enhanced the heat and mass transfer of the fluidized bed system. Thus a higher drying rate was obtained in the falling rate period because the higher contactin efficiency increases the evaporation rate at the particle surface. However, the drying rate in the diffusion regiol shows little improvement because the moisture diffusivity does not depend on the contacting efficiency. The fluidized bed dryer with vertical internal baffles could therefore be used in the initial rapid drying stage in a two stage drying strategy for paddy. The insertion of vertical internal baffles into a fluidized bed system improves the processing of Group D particles in a fluidized bed system especially if the system is large in scale.     

循环流化床中C类颗粒的干燥

为将循环流化床(CFB)技术应用于C类颗粒(＜30μm)的干燥,在自建的循环流化床(内径0.104 m×高2.35 m)内,以玉米淀粉(dp=8 μm,ρp=800 kg/m3)为研究对象,考察了不同操作参数对其干燥特性及干湿分离情况的影响.结果表明:循环流化床适用于C类颗粒的干燥;干燥速率随气速及进风温度的增大而增大...     

Combined Microwave/Fluidized Bed Drying of Fresh Peppercorns

A fluidized bed dryer (FBD) and a combined microwave/fluidized bed dryer (CMFD) are used to dry the fresh ripe peppercorns. The average moisture content vs. elapsed drying time, and drying rate vs. average moisture content are experimentally investigated. It is found that the microwave field from the CMFD can increase the potential of the conventional fluidized bed drying. The drying rates of both dryers are dependent on the inlet air temperature and velocity. For the CMFD, the effects of the air velocity on the drying rate are found to be opposite to our previous results tested with white pepper seeds i.e., the drying rates of the fresh ripe peppercorns decreased with increasing air velocity. By using a CMFD, the drying time required to reach the desired moisture content can be reduced to 80-90% of the drying time required for a FBD at the same drying air temperature and velocity. The color of the product dried by a CMFD is also attractive: it becomes flaming yellow, instead of black as obtained from a FBD. The physical structure of the peppercorn, before and after the drying process is also investigated by a metallurgical macroscope and an image analyzer. Different from drying by a FBD, the external form and matter of the white pepper seed are still maintained, even after passing through the drying process.