Fatigue strength of a single crystal in the gigacycle regime

The objective of this work is to investigate the fatigue behavior of a single crystal nickel-based superalloy in the gigacycle regime. Testing from 10⁶ to 10⁹ cycles at 593 °C was performed using an ultrasonic fatigue system operating at 20 kHz. Multiple tests were performed at stresses near the fatigue limit to determine the variability in fatigue life in this regime. Endurance limit results were compared to similar data generated on conventional servohydraulic test systems to determine if there are any frequency effects. Scanning electron microscopy was then used to determine the initiation sites and the failure mechanisms. Initial results indicate little or no frequency effect on the fatigue strength or failure mechanisms of PWA 1484 at 593 °C.     

Fatigue behavior and modeling of short fiber reinforced polymer composites including anisotropy and temperature effects

Effects of anisotropy and temperature on cyclic deformation and fatigue behavior of two short glass fiber reinforced polymer composites were investigated. Fatigue tests were conducted under fully-reversed (R = −1) and positive stress ratios (R = 0.1 and 0.3) with specimens of different thicknesses, different fiber orientations, and at temperatures of −40 °C, 23 °C, and 125 °C. In samples with 90° fiber orientation angle, considerable effect of thickness on fatigue strength was observed. Effect of mold flow direction was significant at all temperatures and stress ratios and the Tsai–Hill criterion was used to predict off-axis fatigue strengths. Temperature also greatly influenced fatigue strength and a shift factor of Arrhenius type was developed to correlate fatigue data at various temperatures, independent of the mold flow direction and stress ratio. Micromechanisms of fatigue failure at different temperatures were also investigated. Good correlations between fatigue strength and tensile strength were obtained and a method for obtaining strain–life curves from load-controlled fatigue test data is presented. A fatigue life estimation model is also presented which correlates data for different temperatures, fiber orientations, and stress ratios.     

Ultrasonic fatigue of a single crystal Ni-base superalloy at 1000 °C

An ultrasonic fatigue testing system capable of operating at temperatures up to 1000 °C has been developed and utilized to study the fatigue behavior of a single crystal superalloy (PWA 1484) at a temperature of 1000 °C and loading frequency of approximately 20 kHz. The stress-life data generated from the ultrasonic testing system were comparable to those from conventional servo-hydraulic fatigue tests for similar single crystal alloys. Interior Ta-rich carbides were the major microstructural feature responsible for crack initiation in the alloy. Crack growth under ultrasonic loading frequency at 1000 °C for PWA 1484 occurred in a crystallographic manner on {1 1 1} octahedral slip planes, in contrast to the normal Mode-I growth mode typically observed for single crystal superalloys at high temperature (>850 °C) with conventional servo-hydraulic loading frequencies (<100 Hz).     

Influence of temperature and thickness on the off-axis behaviour of short glass fibre reinforced polyamide 6.6 – cyclic loading

This paper investigates the anisotropic properties of short glass fibre reinforced polyamide 6.6 (PA66-GF35) under tension–tension and tension–compression cyclic loading. Tensile fatigue tests were carried out on dog-bone specimens, machined out from injection-moulded plates 80 × 80 mm, of three different thicknesses t (1 and 3 mm) at three different nominal fibre orientation angles θ (0°, 30° and 90°). The tests were carried out at RT as well as at 130 °C.The Tsai–Hill failure criterion, modified to account for cyclic loading, is applied to the fatigue data for estimating the fatigue strength parameters of the material under investigation. Results are compared to the strength parameters obtained under quasi-static loading in a previous part of this work [De Monte M, Moosbrugger E, Quaresimin M. Influence of temperature and thickness on the off-axis behaviour of short glass fibre reinforced polyamide 6.6 – quasi-static loading. Composites: Part A, 2010;41(10):1368–79]. The experimental results highlight how specimen thickness remarkably affects mechanical properties: the thinner the specimen the higher will be the degree of anisotropy. Also temperature strongly reduces the fatigue strength under cyclic loading. The Tsai–Hill criterion allows for an adequate fitting of experimental data at the investigated temperatures and load ratios.     

Environmental effects on fatigue behavior of adhesively-bonded pultruded structural joints

The fatigue response of adhesively-bonded pultruded GFRP double-lap joints has been investigated under different environmental conditions. Tests were performed at ?35 °C, 23 °C and 40 °C. A fourth set of fatigue data was collected from tests on preconditioned specimens in warm (40 °C) water. The tests were performed at 40 °C and at 90% relative humidity. Specimens were instrumented with strain and crack gages to record fatigue data. In addition to the S–N curves, stiffness fluctuations and crack initiation and propagation during fatigue were monitored. The dominant failure mode was a fiber-tear failure that occurred in the mat layers of the GFRP laminates. In the presence of high humidity, the failure shifted to the adhesive/composite interface. Although the testing temperature was lower than the glass transition temperature of the adhesive, its influence on the fatigue life and fracture behavior of the examined joints was apparent and was aggravated by the presence of humidity.     

Tensile and fatigue behavior of superelastic shape memory rods

The tensile and fatigue behavior of superelastic shape memory alloy (SMA) bars heat-treated at three different temperatures were examined. Low cycle fatigue tests at variable load rates were carried out to determine the effect of stress and frequency on residual strain and energy dissipation in a fatigue cycle. The mechanism of energy dissipation was studied by monitoring the temperature changes in the fatigued samples as a function of applied stress and frequency of testing. Results from the tensile tests revealed that the stress for the Austenite to Martensite transformation decreased from 408 MPa to 204 MPa with an increase in temperature of heat treatment from 300 to 450 °C. The ultimate strength of the SMA increased from 952 MPa to 1115 MPa when the heat treatment temperature was increased from 300 to 450 °C. Fatigue testing prior to conducting the tensile test decreased the ultimate strength of the SMA and also reduced the failure strain. The energy dissipation in fatigue tests was found to decrease as test frequency increased from 0.025 Hz to 0.25 Hz and the change in sample temperature during the test at the lower test frequency was found to be considerably higher than at the higher frequency.     

Gigacycle fatigue initiation mechanism in Armco iron

Microstructure irreversibility plays a major role in the gigacycle fatigue crack initiation. Surface Persistent Slip Bands (PSB) formation on Copper and its alloy was well studied by Mughrabi et al. as typical fatigue crack nucleation in the very high cycle fatigue regime. In the present paper, Armco iron sheet specimens (1 mm thickness) were tested under ultrasonic frequency fatigue loading in tension–compression (R = −1). The test on the thin sheets has required a new design of specimen and new attachment of specimen. After gigacycle fatigue testing, the surface appearance was observed by optical and Scanning Electron Microscope (SEM). Below about 88 MPa stress, there is no PSBs even after fatigue cycle up to 5 × 10⁹. With a sufficient stress (above 88 MPa), PSBs in the ferrite grain was observed by optic microscope after 10⁸ cycles loading. Investigation with the SEM shows that the PSB can appear in the body-centered cubic crystal in the gigacycle fatigue regime. Because of the grain boundary, however, the local PSB did not continually progress to the grain beside even after 10⁹ cycles when the stress remained at the low level.     

Bonding strength of heat treated compressed Eastern redcedar wood

The objective of this study was to evaluate effect of heat treatment and compression on some properties of Eastern redcedar (Juniperus virginiana) including bonding strength, hardness and surface quality. Specimens were exposed to three temperature levels of 120 °C, 160 °C and 190 °C for 6 h before they were compressed using 2.5 MPa pressure for 5 min. Polyvinyl acetate (PVAc) bonded specimens showed 23.6% reduction in their shear strength when they were exposed to a temperature of 120 °C. Such strength reduction values were 44.4% and 64.1% for the specimens exposed to temperature levels of 160 °C and 190 °C, respectively. The lowest average Janka hardness value of 214.08 kg was determined for the samples exposed to a temperature of 190 °C while those treated with a temperature of 120 °C had the highest hardness value of 397.73 kg. It appears that combination of heat treatment and compression enchanced overall surface quality of the samples in the form of their roughness determined using stylus type equipment.     

Strengthening of AISI 2205 duplex stainless steel by strain ageing

In this study, static strain ageing behavior of commercially available and solution heat treated duplex stainless steel was investigated and the effect of static strain ageing on the mechanical properties was also determined in detail. Some of as-received duplex stainless steel test specimens were pre-strained in tension by 5% and then aged at 100 °C, 200 °C, 300 °C, 400 °C, 500 °C and 600 °C for 30 min in furnace. Some of duplex stainless steel test specimens were solution heat treated at 1050 °C for 30 min, water quenched and then pre-strained for 5% in tension shortly after the solution heat treatment.In order to identify the effect of static strain ageing on the mechanical properties, the tensile strength, the change in the strength due to ageing (ΔY), elongation fracture and hardness were determined. The test results showed that the mechanical properties were affected by static strain ageing mechanism which was applied at different temperatures for same time interval.     

Effect of stress ratio on VHCF behavior for a compressor blade titanium alloy

Effect of stress ratio on fatigue properties of a titanium alloy (TC-17) in the high cycle fatigue (HCF) and very high cycle fatigue (VHCF) were investigated by electromagnetic and ultrasonic fatigue testing. The S–N curves at R = −1, 0.1, 0.5 and 0.7 at 110 Hz and 20 kHz were obtained and discussed. The effects of frequency on fatigue strength was also investigated. It was concluded that the fatigue strength with 50% fatigue failure probability at R = 0.1, 0.5 and 0.7 is lower to the Goodman line and shows a bilinear decreasing trend. Cleavage fracture of primary grains in the surface and interior initiation zone were observed. The formation of the facets induced by the basal or prismatic slips of the H.C.P grains decreased the fatigue strength with variation in mean stress.     

Experimental study of type 316 stainless steel failure under LCF/TMF loading conditions

A detailed investigation of low cycle fatigue (LCF) and thermo-mechanical fatigue (TMF) of a 316FR type stainless steel is presented in this paper in order to identify the failure mechanism based on the experimental results and the subsequent metallography of the samples. The LCF–TMF servohydraulic testing with a temperature uniformity of less than ±5 °C within the gauge section of the specimens was employed to conduct the experimental tests. Fully-reversed, strain-controlled isothermal tests were conducted at 650 °C for the strain ranges of Δɛ = ±0.4%, ±0.8%, ±1.0% and ±1.2%. Strain-controlled in-phase (IP) thermo-mechanical fatigue tests were conducted on the same material and the temperature was cycled between 500 °C and 650 °C. Additionally, the creep–fatigue interactions were investigated with the introduction of symmetrical hold time under both LCF–TMF tests. The cyclic behaviour was further studied by performing microstructural investigations using the scanning electron microscope (SEM).     

Effect of the loading frequency on fatigue properties of JIS S15C low carbon steel and some discussions based on micro-plasticity behavior

Ultrasonic testing method has been often used to investigate fatigue properties of various metallic materials. Since ultrasonic fatigue tests are conducted at a very high loading frequency, they are particularly convenient for fatigue tests in the very high cycle regime. Indeed, ultrasonic fatigue method allows us to conduct fatigue tests up to 10⁹–10¹⁰ cycles in a definite period. However, due to the huge gap of loading frequency between ultrasonic testing method (around 20 kHz) and usual testing method (most of the cases in the range 1–100 Hz), the frequency effect on the fatigue property is still unclear. Low carbon steel is one of typical metallic materials to provide a significant discrepancy between fatigue strengths obtained under ultrasonic testing frequency and under usual testing frequency range.Thus, by preparing a lot of specimens of JIS S15C low carbon steel (0.15% C), fatigue tests were carried out in a wide range of the loading frequency. The frequency effect on the S–N property was first examined and a useful procedure was proposed to obtain a common S–N property normalized by the lower yield stress. In addition, micro-plasticity behavior such as the stress–strain hysteresis loop and the local misorientation were also measured and the frequency effect on the fatigue property was discussed.     

Temperature effects on mixed mode I/II delamination under quasi-static and fatigue loading of a carbon/epoxy composite

This paper addresses the effect of temperature on the mixed-mode interlaminar fracture toughness and fatigue delamination growth rate of a carbon-fibre/epoxy material, namely IM7/8552. Quasi-static and fatigue characterisation tests were carried out at −50 °C, 20 °C, 50 °C and 80 °C, using asymmetric cut-ply coupons. The experimental results show that temperature may have an accelerating or delaying effect on delamination growth, depending on the loading regime, i.e. either quasi-static or fatigue. Fractographic examinations were also carried out in order to assist the interpretation of the experimental data. A semi-empirical equation is introduced to describe the experimentally observed fatigue delamination growth rates at elevated temperatures.     

The investigation of crack growth in specimens with rectangular cross-sections under out-of-phase bending and torsional loading

The paper presents the fatigue test results of rectangular cross-section specimens made of 10HNAP (S355J2G1W) steel. The specimen height to width ratio was 1.5. The tests under bending with torsion were performed for the following ratios of bending to torsional moments M_aB/M_aT = 0.47, 0.94, 1.87 and the loading frequency 26.5 Hz. Nominal stresses were chosen for the equivalent stress according to the Huber-Mises hypothesis equal to 360 MPa. The tests were performed in the high cycle fatigue regime for the stress ratio R = −1 and phase shift between bending and torsion loading equal to ϕ = 0 and 90°. Crack initiation and propagation phases were observed on the specimen surface using the optical microscope (magnification 20×) with an integrated digital camera. The test results for the fatigue crack growth rate versus the stress intensity factor range for mode I and mode III have been described with the Paris equation.     

Elevated temperature low cycle fatigue of grey cast iron used for automotive brake discs

This paper evaluates the fatigue life properties of low carbon grey cast iron (EN-GJL-250), which is widely used for automotive brake discs. Although several authors have examined mechanical and fatigue properties at room temperatures, there has been a lack of such data regarding brake discs operating temperatures. The tension, compression and low cycle fatigue properties were examined at room temperature (RT) and at brake discs’ working temperatures: 500 °C, 600 °C and 700 °C. The microstructure of the material was documented and analysed. Tensile stress–strain curves, cyclic hardening/softening curves, stress–strain hysteresis loops, and fatigue life curves were obtained for all the above-mentioned temperatures. It was concluded, that Young’s modulus is comparable with both tension and compression, but yield its strength and ultimate strength are approximately twice as great in compression than in tension. All the mechanical properties remained quite stable until 500 °C, where at 700 °C all deteriorated drastically. During fatigue testing, the samples endured at 500 °C on average at around 50% of cycles at room temperature. Similar to other materials’ properties, the cycles to failure have dropped significantly at 700 °C.     

Microstructure design and dissolution behavior between 2024 Al/Sn with the ultrasonic-associated soldering

Here we present recent progress on α-Al dendrite-reinforced joints of 2024 aluminum produced by the ultrasonic-assisted soldering method. In ultrasonic-assisted soldering of Al2024, pure Sn was utilized as a filler metal, the vibration frequency was 21 kHz, and the temperature was 300 °C. Interestingly, the aluminum content in the bond was up to 3.2 mass%, which is much higher than the solubility limit of aluminum in Sn at 300 °C. The evolution of the microstructure of the aluminum dendrites in bonds with different ultrasonic time was observed to investigate the dissolution behavior of 2024 Al in Sn under ultrasonic conditions. A migration model of aluminum dendrites in the bonds is proposed, which enables control of the extent of reinforcing α-Al dendrites by varying the ultrasonic time. The shear strength of the α-Al dendrite-reinforced joints is improved significantly, with the maximum shear strength approaching 60 MPa.     

Fatigue strength of sharp V-notched specimens made of ductile cast iron

In the present, the high cycle fatigue strength of notched ductile cast iron is investigated. Experimental tests under axial loading, has been carried out on sharp V-notched specimens taken from heavy section casting considering nominal load ratios (R = 0). All specimens, taken from a heavy section casting, are characterized by a notch tip radius less than 0.1 mm, a notch depth of 10 mm and a notch opening angle = 90°. In order to evaluate the influence of chunky graphite morphology on fatigue life, fatigue tests were carried out also on a second set of specimens without that microstructural defect.Metallurgical analyses were performed on all the samples and some important microstructural parameters (nodule count and nodularity rating, among others) were measured and compared. It was found that a mean content of 40% of chunky graphite in the microstructure (with respect to total graphite content) does not influence significantly the fatigue strength properties of the analysed cast iron.     

Low cycle fatigue behavior of Cr–Mo–V low alloy steel used for railway brake discs

The cyclic stress–strain response and the low cycle fatigue (LCF) behavior of Cr–Mo–V low alloy steel which was used for forged railway brake discs was studied. Tensile strength and LCF properties were examined over a range from room temperature (RT) to 600 °C using specimens cut from circumferential direction of a forged disk. The fully reversed strain-controlled LCF tests were conducted at a constant total strain rate with different axial strain amplitude levels. The cyclic strain–stress relationships and the strain–life relationships were obtained through the test results, and related LCF parameters of the steel were calculated. The studied steel exhibits cyclic softening behavior and behaves Masing type, especially at higher strain amplitudes. At higher than 600 °C, carbide particles aggregated and a decarburized layer developed near the specimen surface. Micro voids distribute within the depth of 50 μm from the specimen surface could coalesce with fatigue cracks. Multiple crack initiation sites were observed on the fracture surface. The oxide film that generated at 600 °C covered the fatigue striations and accelerated the crack propagation. Final fracture area with bigger and deeper dimples showed better ductility at higher temperature. The investigated LCF behavior can provide reference for brake disc life assessment and fracture mechanisms analysis.     

Solute cluster size effect on the fatigue crack propagation resistance of an underaged Al–Cu–Mg alloy

The effect of Cu–Mg cluster size and number density on the fatigue fracture behavior of Al–Cu–Mg alloy with various aging conditions was investigated by means of transmission electron microscopy (TEM), atom probe tomography (APT), scanning electron microscopy (SEM) and fatigue testing. Results showed that the fatigue crack propagation (FCP) resistances of 170 °C/1 h and 170 °C/8 h samples were higher than that of 170 °C/0.5 h sample due to increased number density of great size Cu–Mg co-clusters (>50 atoms). These large clusters were harder to dissolve during cycle deformation, thus reduced the cyclic softening effect and enhanced the FCP resistance. Moreover, as aging prolonged, the critical shear stress (τ_m) of co-clusters by modulus hardening increased from 10.2 (MPa) in 170 °C/0.5 h sample to 12.4 in 170 °C/1 h sample and 12.1 in 170 °C/8 h sample. Thus the force required for the movement of dislocations impeded by co-clusters, as well as the resistance of FCP caused by co-clusters, in 170 °C/1 h and 170 °C/8 h sample was higher than that in 170 °C/0.5 h sample. The 170 °C/8 h sample possessed the lower FCP resistance than 170 °C/1 h sample because of the existence of S′ phase. S′ phase was a kind of semi-coherent unshearable precipitate and hence reduced the planar-reversible slip.     

Compressive strength of high strength class C fly ash-based geopolymers with reactive granulated blast furnace slag aggregates designed by Taguchi method

Compressive strength of geopolymeric specimens produced by class C fly ash and granulated blast furnace slag aggregates has been studied. Four different independent factors comprising of aggregate content, sodium hydroxide concentration, curing time and curing temperature were considered as the variables. To attain the maximum possible accurate responses by means of the smallest amount of examinations, Taguchi design of experiment method was followed. By taking into account three levels for each factor, 9 series of experiments were conducted on the specimens at 2 and 7 days of water curing regime. For both considered regimes, a specimen with 30 weight percent of aggregate and sodium hydroxide concentration of 12 M cured at 90 °C for 16 h had the highest compressive strength. On account of reactivity between aggregates and the fly ash, the compressive strength was reached to 69.3 ± 5.3 MPa and 76.2 ± 3.6 MPa at 2 and 7 days of water curing, respectively. Fracture surface of specimens with the highest and the lowest strengths as well as effect of each considered factor on the compressive strength of the specimens were studied.