Effect of Air and Helium on the Head–Disk Interface During Load–Unload

The tribological characteristics of the head–disk interface are investigated during load–unload for air and helium-filled drives as a function of the pitch static angle and the roll static angle between slider and disk. A custom-made experimental tester inside a sealed environmental chamber was used to determine the regions of “safe” pitch static angle and “safe” roll static angle in air and helium environment during the load–unload process. The presence of head–disk contacts during load–unload were evaluated by measuring the acoustic emission signal and the decrease in rotational speed of the spindle. Scanning electron microscopy and optical surface analysis were used to investigate wear of the slider and the redistribution of lubricant on the disk surface after 10,000 load–unload cycles. The results indicate that the tribological performance of the head–disk interface is improved in helium environment compared to air environment.     

Investigation of disk damage caused during load/unload using a surface reflectance analyzer

Wear of the carbon layer of a magnetic recording disk is investigated during load/unload using a surface reflectance analyzer (SRA). Wear is determined as a function of the number of the load/unload (L/UL) cycles, the vertical head speed, the disk rotational speed, and the air bearing design. Two types of subambient pressure sliders are used in the experiments, the difference between the two designs being related to the size and position of the subambient pressure region. The load/unload behavior of the two slider types is determined numerically using a finite element air bearing simulator.     

Load/unload measurements using laser doppler vibrometry and acoustic emission

The dynamics of the load/unload process are studied using a so-called ‘periscope approach’ which allows us to follow the slider motion during load/unload (L/UL) with the beam of a Laser Doppler Vibrometer (LDV). LDV signals and acoustic emission signals are obtained for three different slider airbearing designs and for load/unload conditions with different vertical velocities and spindle speeds. The load process is investigated statistically using the acoustic emission signal in order to determine the effect of vertical load speed and spindle speed on the probability of contacts between slider and disk.The results indicate that small vertical load speeds decrease the number of head/disk contacts, and that slider designs with a cavity centered close to the trailing edge enable a smooth unloading process.     

The Influence of Lubrication on Head and Disk Wear

Magnetic disks are usually lubricated with fluorocarbon-type lubricants to reduce head and disk wear during the start/stop process of the disk rotation. In this paper, the influence of disk lubrication on the tribological characteristics of the head/disk interface is investigated by pin-on-disk wear tests and the head/disk friction tests.

The anti-wear performance of a lubricant is very high. For example, a lubricant coating of 8.4 × 10^?5 mg/cm² exhibits 1/20 of the ferrite pin wear rate of an unlubricated disk. For a lubricated disk, ferrite pin wear decreases at increased sliding velocities as high as 10 m/s, while pin wear increases rapidly with increased velocity for an unlubricated disk. The lubricant used here performs well in suppressing the wear increase caused by increased load. Regarding friction characteristics, however, an excessive amount of lubricant induces severe head/disk sticking, causing head crash. With respect to head/disk sticking, the upper-limit of the amount of lubricant is 8.4 × 10^?5 mg/cm².     

The effects of texture height and thickness of amorphous carbon nitride coating of a hard disk slider on the friction and wear of the slider against a disk

In order to minimize the stiction force caused by contact of the extremely smooth surfaces of head sliders and disks in hard disk drives, texture is usually applied on the disk surface. For future contact/near-contact recording, the stiction-induced high friction between slider and disk will become a problem. Texture on the slider/disk interface will still be an expected method to reduce friction. Recently, it was suggested to texture the slider surface. A protective coating is usually required on the textured slider surface to reduce wear of the texture. The results showed that texture on the slider surface was effective in reducing the friction between head sliders and disks. On the other hand, the texture and coating on the slider surface increase the spacing between the read/write element and the magnetic layer of the disk. The necessary and effective texture height and coating thickness are still not clear. In the present research, island-type textures with different heights (3–18 mn) were formed on slider surfaces by ion-beam etching. Amorphous carbon nitride (a-CN_x) coatings of different thicknesses (0–50 nm) were coated on the textured slider surfaces as a protective overcoat. The friction and wear properties of these sliders were evaluated by constant-speed drag tests against hard disks coated with diamond-like carbon (DLC). The results show that 2 nm texture on a slider surface is sufficient for low (0.3–0.5) and stable friction of the slider against the disk in a drag test, and coatings thicker than 5 nm show similar wear resistances of the texture on slider surfaces.     

The Effect of Slider Texture on the Tribology of Near Contact Recording Sliders

Island-type texture was fabricated on two types of pico-sliders using plasma etching and ion beam etching. Laser–Doppler interferometry was used to investigate the vibrations of textured and untextured pico-sliders in near-contact situations. Lubricant depletion on the disk surface was investigated in the slider wear tracks using scanning ellipsometry (Surface Reflectance Analyzer (SRA)). The results show that slider in-plane and out-of-plane vibrations were reduced as a consequence of the texture on the slider surface. In addition, lubricant depletion on the disk surface was found to be less severe for textured sliders than for untextured sliders at flying heights below 10 nm.     

Measurement of wear of carbon coated sliders using atomic force microscopy and Raman spectroscopy

Wear of carbon coated sub-ambient pressure “pico” sliders is investigated during sweep testing as a function of interference height, slider design and sliding distance using atomic force microscopy. The wear results from atomic force microscopy measurements are compared with wear measurements of the carbon overcoat using Raman spectroscopy. The effect of interference on wear and disk burnishing is studied using acoustic emission measurements and atomic force microscopy. The results show that wear of a slider is higher for larger interference height and higher stiffness of the air-bearing.     

Tribology of X-1P vapor lubricated hard disks

The tribological characteristics of vapor lubricated X-1P films on carbon coated disks were investigated as a function of lubricant thicknesses (0.2–2 nm) and compared with traditionally dip-coated X-1P and PFPE films. Glide and flyablity tests were performed and the lubricant redistribution in the ‘wear track’ was investigated using a surface reflectance analyzer (SRA). A critical lubricant thickness was found to exist for X-1P below which lubricant accumulation was observed, while lubricant loss was found to be present if the thickness of the lubricant film was greater than the critical thickness.     

Effect of Molecularly Thin Lubricant on Roughness and Adhesion of Magnetic Disks Intended for Extremely High-Density Recording

For extremely high-density recording using conventional technologies, the fly-height needs to decrease to less than ten nanometers. To allow such operation, disk and slider surfaces must become extremely smooth, down to root-mean-square (RMS) roughness values of a few angstroms. For super-smooth disks, molecularly thin lubricants are applied to improve tribological performance of head/disk interfaces. The focus of this study is to quantify the effect of lubricant thickness in terms of detailed roughness parameters and to evaluate the effect of roughness and molecularly thin lubricant on adhesion of magnetic disks intended for extremely high-density recording. Three identical ultra-low-flying disks have been fabricated from the same batch for this particular experiment. To investigate the effect of molecularly thin lubricants on disk roughness, super-smooth magnetic disks with increasing lubricant thickness have been measured and studied, using a primary roughness parameter set. It describes amplitude, spatial, hybrid, and functional aspects of surface roughness and is used to quantify the extremely smooth disk roughness as a function of lubricant thickness. It is found that in addition to simple amplitude parameters, hybrid and functional parameters also capture small features on the disk roughness and show distinct trends with increasing lubricant thickness. Subsequently, a continuum-based adhesion model that uses three parameters from the primary roughness parameter set, is used to predict how the varying thickness of molecularly thin lubricant and the resulting disk roughness affect intermolecular forces at ultra-low-flying head-disk interfaces. It is found that a thicker lubricant layer of 2nm causes higher adhesion forces for ultra-low-flying-heights in the range of 1–3 nm     

Slider Wear on Disks Lubricated by Ultra-Thin Perfluoropolyether Lubricants with Different Molecular Weights

In this study, the wear properties of a magnetic head slider on disks lubricated by ultra-thin perfluoropolyether (PFPE) lubricants with different molecular weights were evaluated by the continuous sliding of magnetic head sliders using the slider contact by the dynamic flying height control. Two types of PFPE lubricants (Z-tetraol and D-4OH) with different molecular weights were evaluated. Results show that the slider wear depended on the coverage of the lubricant film; i.e., the lubricant film with sufficient coverage reduced slider wear. The lubricant film with a low molecular weight (low-Mw), including a lubricant material with a Fomblin and Demnum main chain, exhibited better coverage on a diamond-like carbon surface. Sliders with a low-Mw lubricant film showed less wear than those of a high molecular weight (high-Mw), and the depletion of the low-Mw lubricant film was less than that of the high-Mw lubricant film.     

Experimental Comparison of Load/Unload Slider Dynamics For Two Different Pico-Slider Designs

A comparison of Laser-Doppler vibrometry (LDV) and acoustic emission (AE) data is presented for two different slider designs during load/unload (L/UL). The behavior of the slider is measured for three different vertical load/unload velocities using a transparent glass disk with the slider flying at the bottom surface of the disk. The LDV laser spot can be positioned on the slider alrbearing surface during the complete load/unload process with the help of a so-called “periscope.” A characteristic velocity peak during unloading is observed that is caused by the slider pull-off force.     

Molecular Dynamics Simulation of Lubricant Redistribution and Transfer at Near-Contact Head-Disk Interface

When the spacing between the slider and lubricant in a hard disk drive decreases to less than 5 nm, the effect of the intermolecular force between these two surfaces can no longer be ignored. This effect on the lubricant distribution at the near-contact head disk interface is investigated via molecular dynamics method. In this study, the lubricant is confined between a smooth disk surface and a rough slider surface represented as a partially cosinusoidal wave. The simulation results reveal that the intermolecular force-induced meniscus formation at the near-contact head disk interface is strongly sensitive to the slider-to-disk separation, lubricant film thickness and the asperity shape (or roughness) of the slider. The attractive van der Waals forces between the slider and lubricant become weaker with increasing slider-to-disk separation and asperity mid-height, but decreasing lubricant film thickness and asperity mid-width. The Hamaker theory application to van der Waals interactions is also introduced to verify the molecular dynamics simulation. It is found that the critical separation, below which the lubricant will lose its stability to form a meniscus, increases approximately linearly with the lubricant film thickness, for slider surfaces with or without roughness both in the molecular dynamics simulation and Hamaker theory application to van der Waals interactions. Moreover, it is observed that the critical separation between a smooth disk and rough slider surface will slightly decrease when the asperity mid-height increases. The same phenomenon is observed when the asperity mid-width reduces.     

Wear durability studies of ultra-thin perfluoropolyether lubricant on magnetic hard disks

This paper presents wear and friction studies on ultra-thin (~2 nm) film of perfluoropolyether (PFPE) coated on glass substrate magnetic hard disks. The lubricant was coated on the disk by the dip-coating method and the tribological tests were carried out by sliding a 3 mm diameter glass ball slider (normal load=20 mN) on the rotating disk surface. Lube thickness and lube wear profile were measured using an ellipsometer whereas the worn disk surface was studied using a surface reflectivity analyzer. The sliding speed and the lube bonding conditions were varied during the test. From the results, it is concluded that about 80% bonding of the lube to the disk surface leads to an increase in the wear durability of the lubricant by a factor of 2 when compared to the as-lubed condition. Lube bonding has an effect on increasing the coefficient of friction. Initially, increasing sliding speed increases both friction and wear but for very high sliding speed these values tend to decrease. The glass ball surface showed wear due to asperity interactions as well as lube transfer from the disk to the glass surface.     

Dynamics in the Bridged State of a Magnetic Recording Slider

A novel region of tribological interaction is explored by inducing near contact between the magnetic recording slider and disk. In this study, we performed frictional measurements over a wide range of subambient air pressure and disk rotation rate. Since the slider is supported over the disk by an air bearing, it has been found that cycling from ambient to subambient and then back up to ambient pressure over several minutes of time forms a frictional hysteresis loop. The high-friction branch of the loop, referred to as the bridged state, is characterized by an average frictional displacement and resonant vibration of the suspension mount assembly. The bridged state is currently employed for accelerated wear testing of magnetic slider/disk/lubricant systems. Future magnetic recording systems designed to operate at increasingly lower physical spacing will need to take into account these frictional forces which accompany the incipient contact between the lubricated disk and slider with finite surface roughness. A single degree of freedom model is solved to determine the equivalent dynamic friction force on the slider as an impulse series with random impulse frequency and amplitude from the measured frictional displacement in the bridged state. The mean slider-disk spacing in the bridged state is derived from the experimental friction force, the spacing probability density function, and the adhesion stress from the Lifshitz model for dispersion interaction energy.     

Investigation of Slider Dynamics Considering Bias Voltage and Lubricant Charge in the Unsteady Proximity Condition

The relationship between slider and lubricant becomes increasingly important as the mechanical spacing between slider and disk is reduced to satisfy the demand for higher areal density. At a reduced flying height, the slider easily contacts the lubricant, which can cause slider instability. This study analyzed slider dynamics to improve the head–disk reliability in the unsteady proximity condition, considering bias voltages between the slider, disk, and lubricant. Force–distance curves were measured using atomic force microscopy to investigate changes in lubricant performance induced by an applied voltage. Additionally, the touch-down power and take-off power were measured under various applied voltage conditions. Experiments were carried out to estimate slider instability as a function of charged disk and slider conditions, to improve the slider dynamics in the unsteady proximity condition. The effect of the bias voltage induced by a voltage applied to the lubricant was carefully examined to accurately understand slider dynamics. The relationship between the lubricant behavior and the applied voltage was investigated; the voltage applied to the disk was more influential in improving slider dynamics. Consequently, the effects of bias voltage and lubricant, as induced by a charged disk, should be considered when analyzing slider dynamics to improve head–disk interface reliability in an unsteady proximity condition.     

Formation of lubricant “moguls” at the head/disk interface

In a typical head/disk interface of a rigid disk drive, the motion and redistribution of a 14 Å thick lubricant film on the disk under a flying slider is analyzed with an optical surface analyzer. At short times (seconds to a few minutes), the film is rearranged in an isotropic manner, creating a pattern of moguls¹ of 100 m in lateral size and a few angstroms in height. A strong correlation is demonstrated between the resulting distribution of the lubricant film and the underlying substrate topography. Surprisingly, lubricant becomes thicker on the peaks of the micro-waviness, and thinner in the valleys. Possible mechanisms for this unexpected behavior will be discussed, as well as its tribological implications. At longer times, the lubricant film is pushed away from underneath the slider, creating the previously reported circumferentially depleted tracks beneath the slider rails. In the timeframe of our experiment, no significant net lubricant loss was observed.     

A Model for Lubricant Transfer from Media to Head During Heat-Assisted Magnetic Recording (HAMR) Writing

One of the challenges in heat-assisted magnetic recording (HAMR) is the creation of write-induced head contamination at the near-field transducer. A possible mechanism for the formation of this contamination is the transfer of lubricant from the disk to the slider (lubricant pickup) due to temperature-driven evaporation/condensation and/or mechanical interactions. Here we develop a continuum model that predicts the head-to-disk lubricant transfer during HAMR writing. The model simultaneously determines the thermocapillary shear stress-driven deformation and evaporation of the lubricant film on the disk, the convection and diffusion of the vapor phase lubricant in the air bearing and the evolution of the condensed lubricant film on the slider. The model also considers molecular interactions between disk–lubricant, slider–lubricant and lubricant–lubricant in terms of disjoining pressure. We investigate the effect of media temperature, head temperature and initial lubricant thickness on the lubricant transfer process. We find that the transfer mechanism is initially largely thermally driven. The rate of slider lubricant accumulation can be significantly reduced by decreasing the media temperature. However, as the amount of lubricant accumulation increases with time, a change in the transfer mechanism occurs from thermally driven to molecular interactions driven. A similar change in transfer mechanism is predicted as the head–disk spacing is reduced. There exists a critical value of head lubricant thickness and a critical head–disk spacing at which dewetting of the disk lubricant begins, leading to enhanced pickup.     

Experimental investigation of AE and friction signals related to the durability of head/disk interface

The durability of a hard disk drive is one of the most critical issues that must be optimized for best performance. Especially as the flying height of the head slider of a hard disk drive decreases over the years, the concern for surface damage and head contamination continues to grow. In this paper the characteristics of AE and friction signals for various operating conditions using CSS and drag tests were investigated from the durability point of view. Also, the wear characteristics of the laser bumps on a magnetic disk were compared between the CSS and drag tests. The general shapes of the AE and friction signals during a single CSS test were quite similar even under less than ideal operating conditions. However, it was found that the AE signal was more sensitive than the friction signal in assessing the damage of the slider/disk interface. Finally, a correlation was established between the CSS and drag testing methods with respect to the laser bump wear. This outcome suggests that the drag test may be used to accelerate the surface damage effect of head/disk system.     

The Effect of Phosphazene additives to passivate and stabilize lubricants at the head/disk interface

There have been a number of applications for lubricant additives in the disk drive media area, the first of which was for pseudo-contact recording with inductive heads (tri-pad sliders) in an effort to stabilize the head/disk interface and minimize lube decomposition under hot/wet conditions. A number of additives have been tried which include antioxidants as well as Lewis bases, the latter in an effort to passivate the catalytic activity of the Lewis Acid sites on the slider which results in the decomposition of the perfluoropolyether (PFPE) lubricants such as Z-Dol, AM and Z-Tetraol. In addition to this passivation action of the phosphazene toward catalytic decomposition of the lubricant, it has recently been reported that the use of X-1P (a cyclic phosphazene) also enhances reflow of the lube, increasing the durability of the head disk interface. In this regard there are still a number of unanswered questions that pertain to the mechanism of the interaction of the X-1P with the lubricant and/or carbon to cause this increase in mobility of the lubricant resulting in the enhanced durability.There are numerous technical issues associated with the use of the various additives with the main one being compatibility between the additive and the PFPEs as well as the carbon surfaces on which they are coated. These issues include bonding, phase separation of the components, and the transfer mechanism for the additive to the slider where the passivation is required.In this paper, we will look at the interaction of the X-1P with the carbon overcoat on the media in an effort to try to better understand the mechanism of such an interaction and its effect on the mobility of the lubricant as well as the amount of bonded lube on the disks.     

A study of contact-start-stop wear tracks by TOF SIMS

In magnetic hard disk drive system, an ultra thin layer of lubricant is coated to the thin film media surface to prevent wear. Under the condition of relative motion, the displacement and replenishment of the lubricant at the head and media contact area are the factors that control the friction and wear behavior of the system. In this study, we investigate the sliding wear disk surface prepared by contact-start-stop (CSS) test using TOF SIMS (Time of Flight Secondary Ion Mass Spectrometry). TOF SIMS is a power tool for surface analysis with both high spatial and high mass resolution. Our investigations show that the lubricant thickness variation of the disk media at the contact area can be captured by sharp ion map images of TOF SIMS, and the thickness can be inferred based on the relative ion fragment intensity. In addition, the composition variation of the slider material and the magnetic layer materials can also be monitored. Finally the sliding effect is analyzed.