Fatigue properties and fracture analysis of a SiC fiber-reinforced titanium matrix composite

Tension–tension fatigue properties of SiC fiber reinforced Ti–6Al–4V matrix composite (SiC_f/Ti–6Al–4V) at room temperature were investigated. Fatigue tests were conducted under a load-controlled mode with a stress ratio 0.1 and a frequency 10 Hz under a maximum applied stress ranging from 600 to 1200 MPa. The relationship between the applied stress and fatigue life was determined and fracture surfaces were examined to study the fatigue damage and fracture failure mechanisms using SEM. The results show that, the fatigue life of the SiC_f/Ti–6Al–4V composite decreases substantially in proportion to the increase in maximum applied stress. Moreover, in the medium and high life range, the relationship between the maximum applied stress and cycles to failure in the semi-logarithmic system could be fitted as a linear equation: S_max/μ = 1.381 − 0.152 × lgN_f. Fractographic analysis revealed that fatigue fracture surfaces consist of a fatigued region and a fast fracture region. The fraction of the fatigued region with respect to the total fracture surface decreases with the increase of the applied maximum stresses.     

Effect of stitch density on fatigue characteristics and damage mechanisms of stitched carbon/epoxy composites

The effect of stitch density (SD) on fatigue life, stiffness degradation and fatigue damage mechanisms in carbon/epoxy (T800SC/XNRH6813) stitched using Vectran thread is presented in this paper. Moderately stitched composite (SD = 0.028/mm²; ‘stitched 6 × 6’) and densely stitched composite (SD = 0.111/mm²; ‘stitched 3 × 3’) are tested and compared with composite without stitch thread (SD = 0.0; ‘unstitched’). The experiments show that the fatigue life of stitched 3 × 3 is moderately better than that of unstitched and stitched 6 × 6. Stitched 3 × 3 pattern is also able to postpone the stiffness degradation onset. The improvement of fatigue properties and postponement of stiffness degradation onset in stitched 3 × 3 is primarily due to an effective impediment of edge-delamination. Quantification of damage at various cycles and stress levels shows that stitch density primarily affects the growth rate of delamination.     

Repair of shear-deficient normal weight concrete beams damaged by thermal shock using advanced composite materials

The use of advanced composite materials such as Fiber Reinforced Polymers (FRPs) in repairing and strengthening reinforced concrete structural elements has been increased in the last two decades. Repairing and strengthening damage structures is a relatively new technique. The aims of this study was to investigate the efficiency and effectiveness of using Carbon Fiber Reinforced Polymer (CFRP) to regain shear capacity of shear-deficient normal weight high strength RC beams after being damaged by thermal shock. Sixteen high strength normal weight RC beams (100 × 150 × 1400 mm) were cast, heated at 500 °C for 2 h and then cooled rapidly by immersion in water, repaired, and then tested under four-point loading until failure. The composite materials used are carbon fiber reinforced polymer plates and sheets. The experimental results indicated that upon heating then cooling rapidly, the reinforced concrete (RC) beams exhibited extensive map cracking without spalling. Load carrying capacity and stiffness of RC beams decreased about 68% and 64%, respectively, as compared with reference beams. Repairing the thermal damaged RC beams allowed recovering the original load carrying without achieving the original stiffness. Repaired beams with CFRP plates with 90° and 45° regained from 90% to 99% of the original load capacity with a corresponding stiffness from 79% to 95%, whereas those repaired with CFRP sheet on the web sides and a combination of CFRP plates and sheet regained from 102% to 107% of the original load capacity with a corresponding stiffness from 81% to 93%, respectively. Finally, finite element analysis model is developed and validated with the experimental results. The finite element analysis showed good agreement as compared with the experimental results in terms of load–deflection and load–CFRP strain curves.     

Effect of cellulose nano fiber (CNF) on fatigue performance of carbon fiber fabric composites

The effect of cellulose nano fibers (CNF): micro-fibrillated cellulose and bacteria cellulose fibers were investigated on the fatigue life of carbon fiber (CF) fabric/epoxy (EP) composites. Epoxy used as the matrix was physically modified with CNF in advance before fabricating the laminates. The high cycle fatigue strength was significantly improved at 0.3 wt% CNF. There exists an appropriate CNF content which makes the fatigue life longest. An increase of adhesive strength between CF and matrix results due to physical modification with CNF. The adhesive strength much increases with increasing the CNF content. Almost no interfacial debonding occurs at 0.8 wt% CNF content when CF breakage takes place. On the other hand, some debonding occurs along CFs from the breaking point at 0.3 wt% CNF. Debonding is more significant in the case of no CNF addition to the matrix. An appropriate interfacial strength brought at 0.3 wt% CNF is the key of fatigue life extension.     

On the strengthening effect of increasing cycling frequency on fatigue behavior of some polymers and their composites: Experiments and modeling

Effect of cycling frequency on fatigue behavior of neat, talc filled, and short glass fiber reinforced injection molded polymer composites was investigated by conducting load-controlled fatigue tests at several stress ratios (R = −1, 0.1, and 0.3) and at several temperatures (T = 23, 85 and 120 °C). A beneficial or strengthening effect of increasing frequency was observed for some of the studied materials, before self-heating became dominant at higher frequencies. A reduction in loss tangent (viscoelastic damping factor), width of hysteresis loop, and displacement amplitude, measured in load-controlled fatigue tests, was observed by increasing frequency for frequency sensitive materials. Reduction in loss tangent was also observed for frequency sensitive materials in DMA tests. It was concluded that the fatigue behavior is also time-dependent for frequency sensitive materials. A Larson–Miller type parameter was used to correlate experimental fatigue data and relate stress amplitude, frequency, cycles to failure, and temperature together. An analytical fatigue life estimation model was also used to consider the strengthening effect of frequency in addition to mean stress, fiber orientation, and temperature effects on fatigue life.     

Heat conduction analysis of laser CFRP processing with IR and UV laser light

To investigate carbon fiber reinforced plastic (CFRP) composite processing, cutting experiments are performed using a Nd:YAG laser. Both ultraviolet (λ = 266 nm) and infrared (λ = 1064 nm) lights are examined to optimize the laser conditions for cutting CFRP. The experimental data are compared to the results calculated by heat conduction models. The good agreement between the experimental and calculated results indicates that the cutting quality depends on the wavelength of the cutting laser.     

Fatigue behavior of RC T-beams strengthened in shear with EB CFRP L-shaped laminates

The use of externally bonded carbon fiber-reinforced polymer (EB-CFRP) to strengthen deficient reinforced concrete (RC) beams has gained in popularity and has become a viable and cost-effective method. Fatigue behavior of RC beams strengthened with FRP is a complex issue due to the multiple variables that affect it (applied load range, frequency, number of cycles). Very few research studies have been conducted in shear under cyclic loading. The use of prefabricated CFRP L-shaped laminates (plates) for strengthening RC beams under static loading has proven to be technically feasible and very efficient. This study aimed to examine the fatigue performance of RC T-beams strengthened in shear for increased service load using prefabricated CFRP L-shaped laminates. The investigation involved six laboratory tests performed on full-size 4520 mm-long T-beams. The specimens were subjected to fatigue loading up to six million load cycles at a rate of 3 Hz. Two categories of specimens (unstrengthened and strengthened) and three different transverse-steel reinforcement ratios (Series S0, S1, and S3) were considered. Test results were compared with the upper fatigue limits specified by codes and standards. The specimens that did not fail in fatigue were then subjected to static loading up to failure. The test results confirmed the feasibility of using CFRP L-shaped laminates to extend the service life of RC T-beams subjected to fatigue loading. The overall response was characterized by an accelerated rate of damage accumulation during the early cycles, followed by a stable phase in which the rate slowed significantly. In addition, the strains in the stirrups decreased after the specimens were strengthened with CFRP, despite the higher applied fatigue loading. Moreover, the addition of L-shaped laminates enhanced the shear capacity of the specimens and changed the failure mode from brittle to ductile under static loading. Finally, the presence of transverse steel in strengthened beams resulted in a substantially reduced gain in shear resistance due to CFRP, confirming the existence of an interaction between the transverse steel and the CFRP.     

Intralaminar fatigue crack growth properties of conventional and interlayer toughened CFRP laminate under mode I loading

Intralaminar and interlaminar fatigue crack growth behaviours under mode I loading were investigated with conventional and interlayer toughened unidirectional CFRP laminates. For intralaminar crack growth tests, initial defects were introduced using “intralaminar film insertion method”, in which a release film is inserted inside a single lamina prepreg. A fatigue test under a constant maximum energy release rate, G_max, was carried out using DCB specimens. It was found that the intralaminar fatigue crack growth property of the interlayer toughened CFRP laminates was the same as that of the conventional CFRP laminates. For the interlayer toughened CFRP laminates, the G_max with a given crack growth rate, da/dN, was much lower for intralaminar crack growth than for interlaminar crack growth. The da/dN-G_max curve at zero crack extension, Δa = 0, which was estimated by extrapolating the da/dN-Δa relationship, was not affected by bridging fibres, and most conservative for the interlayer toughened CFRP laminates.     

Structural limits of FRP-balsa sandwich decks in bridge construction

The span limits of two glass fiber-reinforced polymer (GFRP) bridge concepts involving GFRP-balsa sandwich plates are discussed. The sandwich plates were either used directly as slab bridges or as decks of a hybrid sandwich-steel girder bridges. In the latter case, the potential of the sandwich decks to replace reinforced concrete (RC) decks was also evaluated. Taking the limits of manufacturing into account (800 mm slab thickness), maximum bridge spans of approximately 19 m can be reached with FRP-balsa sandwich slab bridges, if a carbon-FRP (CFRP) arch is integrated into the balsa core. Above this limit, hybrid sandwich-steel girder bridges can be used up to spans of 30 m. RC deck replacement requires timber and steel plate inserts into the balsa core above the steel girders. GFRP-balsa sandwich slabs or decks exhibit full composite action between lower and upper face sheets. Stress concentrations occur at the joints between balsa core and timber inserts which however can effectively be reduced by changing from butt to scarf joints.     

An investigation of contact resistance between carbon fiber/epoxy composite laminate and printed silver electrode for damage monitoring

An addressable conducting network (ACN) enables the structural condition to be monitored by the electrical resistance between electrodes on surface of CFRP (carbon fiber reinforced polymer) structure. To improve the reliability of ACN for damage detection, the contact resistance between the electrodes and CFRP laminates needs to be minimized. In this paper, the silver nanoparticles electrodes were fabricated via printed electronics techniques on CFRP composite. The contact resistance between the silver electrodes and CFRP was measured with respect to various fabrication conditions such as the sintering temperature of silver nanoink and the surface roughness of CFRP laminates. The interfaces between silver electrode and carbon fibers were observed using scanning electron microscope (SEM). From the study, it was found that the lowest contact resistance of 0.3664 Ω could be achieved when the sintering temperature of the silver nanoink and surface roughness were 120 °C and 230 nm, respectively.     

Structure property relation of hybrid biocomposites based on jute,viscose and polypropylene: The effect of the fibre content and the length on the fracture toughness and the fatigue properties

In the present study, the extent of jute and viscose fibre breakage during the extrusion process on the fracture toughness and the fatigue properties was investigated. The composite materials were manufactured using direct long fibre thermoplastic (D-LFT) extrusion, followed by compression moulding. The fracture toughness (K_IC) and the fracture energy (G_IC) of the PP–J30 composites were significantly improved (133% and 514%, respectively) with the addition of 10 wt% viscose fibres, indicating hindered crack propagation. The addition of viscose fibres resulted in three times higher fatigue life compared with that of the unmodified jute composites. Further, with the addition of (2 wt%) MAPP, the PP–J30–V10 resulted in a higher average viscose fibre length of 8.1 mm, and the fracture toughness and fracture energy increased from 9.1 to 10.0 MPa m^1/2 and 28.9 to 31.2 kJ/m², respectively. Similarly, the fatigue life increased 51% compared with the PP–J30–V10, thus demonstrating the increased work energy due to hindrance of the propagation of cracks.     

Very high cycle fatigue of nitrided 18Ni maraging steel sheet

Thin sheets of nitrided 18Ni maraging steel are tested under cyclic tension (load ratio R = 0.1) in the very high cycle fatigue (VHCF) regime. The ultrasonic fatigue testing method with a cycling frequency of about 20 kHz has been further developed for these experiments. Sheet specimens with 0.35 mm thickness are mounted on a carrier specimen, they are pre-stressed and are forced to vibrate jointly. Between 10⁷ and 10⁹ cycles, fatigue cracks are initiated exclusively at internal TiN inclusions. The areas of the crack initiating inclusions projected perpendicular to the applied tensile stress are evaluated. The square root of inclusion areas, (area_INC)^1/2 lies between 2.5 μm and 5.3 μm. Considering inclusions as cracks, their stress intensity range is between ΔK_INC = 1.3 MPa m^1/2 and 2.4 MPa m^1/2. The sizes of crack initiating inclusions influence fatigue lifetimes. This is considered in a crack propagation model and by presenting lifetimes versus the stress amplitudes multiplied by (area_INC)^1/12. A mean lifetime of 10⁹ cycles is found at a stress amplitude of 22% of the tensile strength, which is comparable to other high strength steels tested under cyclic tension.     

Research on fatigue behavior of welded joint spraying fused by low transformation temperature alloy powder

Modification of spraying fused (MSF) of plasma arc as heat source was used to improve the fatigue performance of welded joint, which both fundamentally reduced stress concentration at weld toe and achieved metallurgical bond between spraying fused coating and welding. The low transformation temperature alloy powder was applied to the method of MSF. After spraying fusion, especially spraying fused joint by low transformation temperature alloy powder, the distribution of residual stress is more difficult to be obtained. Finite element (FE) simulation as an important tool was used to determine the stress field and temperature field of spraying fused joint. Simulated results show that as-welded joint and welded joint spraying fused by conventional nickel base alloy powder (Conventional-joint) present tensile stress. The stress of welded joint spraying fused by low transformation temperature alloy powder (LTT-joint) is compressive stress. Fatigue test results indicated that under the condition of 2 × 10⁶ cycles, the fatigue strength of as-welded joint is 135 MPa, while that of Conventional-joint and LTT-joint is 218 MPa and 235 MPa, respectively. The fatigue strength of Conventional-joint increases by 61.48%, and fatigue strength of LTT-joint increases by 74.07%.     

Fatigue behavior and modeling of short fiber reinforced polymer composites including anisotropy and temperature effects

Effects of anisotropy and temperature on cyclic deformation and fatigue behavior of two short glass fiber reinforced polymer composites were investigated. Fatigue tests were conducted under fully-reversed (R = −1) and positive stress ratios (R = 0.1 and 0.3) with specimens of different thicknesses, different fiber orientations, and at temperatures of −40 °C, 23 °C, and 125 °C. In samples with 90° fiber orientation angle, considerable effect of thickness on fatigue strength was observed. Effect of mold flow direction was significant at all temperatures and stress ratios and the Tsai–Hill criterion was used to predict off-axis fatigue strengths. Temperature also greatly influenced fatigue strength and a shift factor of Arrhenius type was developed to correlate fatigue data at various temperatures, independent of the mold flow direction and stress ratio. Micromechanisms of fatigue failure at different temperatures were also investigated. Good correlations between fatigue strength and tensile strength were obtained and a method for obtaining strain–life curves from load-controlled fatigue test data is presented. A fatigue life estimation model is also presented which correlates data for different temperatures, fiber orientations, and stress ratios.     

Experimental investigation on low cycle fatigue of DZ125 with film cooling holes in different processes of laser drilling

Due to the different low cycle fatigue (LCF) properties and fatigue fracture behavior around film cooling holes on DZ125, the LCF tests are carried out using tension cycling under stress control conditions (stress ratio R = 0.1) at 900 °C. The specimens were designed as thin-wall plate with single hole and multi holes under picosecond and nanosecond laser drilling processes. Comparative analyses of the differences between fatigue life and microscopic fracture morphology are conducted. It is shown that under the same stress condition, the relationship between fatigue life is as follows: picosecond laser single-holed specimen > nanosecond laser single-holed specimens > picosecond laser multi-holed specimens > nanosecond laser multi-holed specimens. Scanning electron microscope (SEM) analyses of the fracture revealed that the crack initiates from the film cooling holes where fatigue source zone, fatigue crack propagation zone and fatigue fracture zone can be found. However, the different processes lead to slightly different fracture morphology: radial-type ridge centering on the fatigue source zone is more apparent and uniform in picosecond laser drilling specimens than in the nanosecond laser drilling ones. On the other hand, the radial-type ridge is biased toward large-aperture side with nanosecond laser drilling.     

Characteristics of aluminum/CFRP short square hollow section beam under transverse quasi-static loading

Energy absorption capability and bending collapse behavior of an aluminum (Al)/carbon fiber reinforced plastic (CFRP) short square hollow section (SHS) beam were investigated under transverse quasi-static loading. The Al SHS beam was reinforced by CFRP, and the specimen was co-cured via an autoclave curing process. Three-point bending test was performed with five different lay-up sequences and three different laminate thicknesses. Stable bending collapse accompanying plastic hinge was observed in all specimens. Individual bending collapse behaviors were different depending on the lay-up sequences. The specific energy absorbed (SEA) was improved by up to 29.6% in the Al/CFRP SHS beam specimen with a [0/+45°/90°/−45°]_n lay-up sequence and laminate thickness of 1.168 mm (thickness ratio of Al: CFRP = 1: 0.87, 8 plies of prepreg) compared to the Al SHS beam. The SEA was not related with damage area of the Al/CFRP SHS beam. Finite element analysis and theoretical analysis based on Kecman’s model were performed to investigate the effect of reinforcement by CFRP on the Al SHS beam.     

Improved mechanical properties of an epoxy glass–fiber composite reinforced with surface organomodified nanoclays

An organomodified surface nanoclay reinforced epoxy glass-fiber composite is evaluated for properties of mechanical strength, stiffness, ductility and fatigue life, and compared with the pristine or epoxy glass-fiber composite material not reinforced with nanoclays. The results from monotonic tensile tests of the nanoclay reinforced composite material at 60 °C in air showed an average 11.7% improvement in the ultimate tensile strength, 10.6% improvement in tensile modulus, and 10.5% improvement in tensile ductility vs. these mechanical properties obtained for the pristine material. From tension–tension fatigue tests at a stress-ratio = +0.9 and at 60 °C in air, the nanoclay reinforced composite had a 7.9% greater fatigue strength and a fatigue life over a decade longer or 1000% greater than the pristine composite when extrapolated to 10⁹ cycles or a simulated 10-year cyclic life. Electron microscopy and Raman spectroscopy of the fracture and failure modes of the test specimens were used to support the results and conclusions. This nanocomposite could be used as a new and improved material for repair or rehabilitation of external surface wall corrosion or physical damage on piping and vessels found in petrochemical process plants and facilities to extend their operational life.     

Performance of reinforced concrete slabs strengthened with different types and configurations of CFRP

A total of eight reinforced concrete slabs, 2440 × 600 × 125 mm strengthened with different layers and configurations of CFRP sheets were fabricated and tested. In addition, nonlinear finite element analysis (NLFEA) using ANSYS package was used to simulate the behavior of the test specimens. After reasonable validation of NLFEA with the experimental test results of companion slabs, NLFEA was expanded to provide a parametric study of eighteen slabs. The load–deflection, load strain, and failure modes obtained from the experimental test results and the NLFEA evidently confirmed that strengthening of under-reinforced concrete slabs with CFRP improves the flexural strength capacity and reduce the ductility. This was observed for both types of CFRP. The increase in the flexural strength and the reduction in the ductility increased with the increase in the number of CFRP layers. It was concluded that CFRP strengthening of slabs could be categorized as effective, economical, and successful only if substantial increase in the flexural strength capacity is achieved without changing the failure mode to a shear failure mode at the face of the supports or to a compression failure mode. Comparison between the two CFRP types, for almost equivalent applied area of CFRP, showed that the type of CFRP has significant influence on the behavior of the strengthened slabs. The difference is attributed to the difference in the mechanical properties and the bonding quality of the CFRP material.     

Studies on fatigue life enhancement of pre-fatigued spring steel specimens using laser shock peening

SAE 9260 spring steel specimens after enduring 50% of their mean fatigue life were subjected to laser shock peening using an in-house developed 2.5 J/7 ns pulsed Neodymium-doped Yttrium Aluminum Garnet (Nd:YAG) laser for studying their fatigue life enhancement. In the investigated range of process parameters, laser shock peening resulted in the extension of fatigue life of these partly fatigue damaged specimens by more than 15 times. Contributing factors for the enhanced fatigue life of laser peened specimens are: about 400 μm thick compressed surface layer with magnitude of surface stress in the range of −600 to −700 MPa, about 20% increase in surface hardness and unaltered surface finish. For laser peening of ground steel surface, an adhesive-backed black polyvinyl chloride (PVC) tape has been found to be a superior sacrificial coating than conventionally used black paint. The effect of repeated laser peening treatment was studied to repair locally surface melted regions and the treatment has been found to be effective in re-establishing desired compressive stress pattern on the erstwhile tensile-stressed surface.     

Investigation of laser pulse fatigue effect on unpainted and painted CFRP structures

Laser ultrasonic based nondestructive evaluation (NDE) techniques are being increasingly used in aerospace industries. Generally, the service lifetime for an aircraft could be more than 25 years. Thus, the composite structures of the aircraft could be susceptible to laser pulse fatigue damage caused by the laser pulse energy in the long-term repetitive maintenance inspection. In this paper, the effect of repeat laser pulse scanning on the mechanical characteristics of unpainted and painted CFRP specimens (USN175BX Carbon UD prepreg, Bisphenol A epoxy resin) is investigated to verify the reliability regarding the use of laser ultrasonic scanning based NDE techniques on the inspection of the CFRP structure. A high-speed laser ultrasonic scanning system is setup to perform repeat scanning of 1300 times on both CFRP specimens at the five laser pulse energy levels using the 532-nm and 1064-nm Q-switched continuous wave lasers. Elastic modulus assessment based on the ultrasonic Lamb wave pitch–catch method is used and the surface condition of the scanned area is investigated by a microscope. As a result, the laser pulse fluences that is shown in this paper are suitable for the long-term repetitive maintenance inspection in unpainted and painted CFRP structure even if it demonstrates an embrittlement phenomenon similar to the modulus measurement resolution in the unpainted CFRP specimen. In addition, the laser pulse fluence for maximum signal-to-noise ratio without any damage is investigated in both unpainted and painted CFRP specimens. As a result, both 102.45 mJ/cm² in unpainted CFRP specimen and 51 mJ/cm² in painted CFRP specimen can be the laser pulse energy for the maximum signal-to-noise ratio without any damage.