An investigation into the damage development and residual strengths of open-hole specimens in fatigue

An extensive experimental program was carried out to investigate and understand the sequence of damage development throughout the life of open-hole composite laminates loaded in tension–tension fatigue. Quasi-isotropic carbon/epoxy laminates, with stacking sequence [45₂/90₂/−45₂/0₂]_S, [45/90/−45/0]_2S and [45/90/−45/0]_4S were examined. These were selected on the basis that under quasi-static loading the [45₂/90₂/−45₂/0₂]_S configuration exhibited a delamination dominated mode of failure whilst the [45/90/−45/0]_2S and [45/90/−45/0]_4S configurations showed a fibre dominated failure mode, previously described as “pull-out” and “brittle” respectively. Specimens were fatigue loaded to 1 × 10⁶ cycles or catastrophic failure, which ever occurred first. A number of tests were interrupted at various points as the stiffness dropped with increasing cycles, which were inspected using X-ray computed tomography (CT) scanning. A static residual strength program was carried out for run-out specimens of each configuration.     

Bridging effect on mode I fatigue delamination behavior in composite laminates

This paper discusses the bridging effect of fibres on mode I fatigue delamination growth in unidirectional and multidirectional polymer composite laminates based on a series of double cantilever beam (DCB) tests. From the results, there is sufficient evidence that fibre bridging can decrease the crack growth rate da/dN significantly, and using only one fatigue resistance curve to determine the delamination behavior in composite materials with large-scale fibre bridging may be inadequate. The bridging created in fatigue delamination is different from that of quasi-static delamination at the same crack length. So it is incorrect to use the resistance curve (R-curve) from quasi-static delamination tests to normalize fatigue delamination results.     

Quantification of flexural fatigue life and 3D damage in carbon fibre reinforced polymer laminates

Carbon fibre reinforced polymer (CFRP) laminated composites have become attractive in the application of wind turbine blade structures. The cyclic load in the blades necessitates the investigation on the flexural fatigue behaviour of CFRP laminates. In this study, the flexural fatigue life of the [+45/−45/0]_2s CFRP laminates was determined and then analysed statistically. X-ray microtomography was conducted to quantitatively characterise the 3D fatigue damage. It was found that the fatigue life data can be well represented by the two-parameter Weibull distribution; the life can be reliably predicted as a function of applied deflections by the combined Weibull and Sigmodal models. The delamination at the interfaces in the 1st ply group is the major failure mode for the flexural fatigue damage in the CFRP laminate. The calculated delamination area is larger at the interfaces adjacent to the 0 ply. The delamination propagation mechanism is primarily matrix/fibre debonding and secondarily matrix cracking.     

An experimental study on the effects of matrix cracking to the stiffness of glass/epoxy cross plied laminates

Three independent measurement techniques are applied to characterize glass fiber laminates. The effects of distributed fatigue damage to the stiffness related behavior of cross plied laminates are quantified. Tensile and flexural stiffness reduction is obtained from quasi-static testing. Vibration testing shows the degradation of flexural and in-plane shear stiffnesses. The reduction of the phase velocity of symmetric S₀ mode is observed from the experimental dispersion curves of Lamb waves. However, the mutual agreement of these results is less satisfactory than was earlier seen for virgin laminates. The phenomena causing the discrepancies are proposed and discussed.     

Intralaminar fatigue crack growth properties of conventional and interlayer toughened CFRP laminate under mode I loading

Intralaminar and interlaminar fatigue crack growth behaviours under mode I loading were investigated with conventional and interlayer toughened unidirectional CFRP laminates. For intralaminar crack growth tests, initial defects were introduced using “intralaminar film insertion method”, in which a release film is inserted inside a single lamina prepreg. A fatigue test under a constant maximum energy release rate, G_max, was carried out using DCB specimens. It was found that the intralaminar fatigue crack growth property of the interlayer toughened CFRP laminates was the same as that of the conventional CFRP laminates. For the interlayer toughened CFRP laminates, the G_max with a given crack growth rate, da/dN, was much lower for intralaminar crack growth than for interlaminar crack growth. The da/dN-G_max curve at zero crack extension, Δa = 0, which was estimated by extrapolating the da/dN-Δa relationship, was not affected by bridging fibres, and most conservative for the interlayer toughened CFRP laminates.     

Effect of temperature on low velocity impact damage and post-impact flexural strength of CFRP assessed using ultrasonic C-scan and micro-focus computed tomography

The effect of temperature on the low velocity impact resistance properties and on the post-impact flexural performance of CFRP laminates were studied. With this aim, 150 × 75 mm cross-ply carbon fibre/epoxy laminates with a [0/90/90/0]_2s layup, therefore with a total of sixteen layers, were impacted at ambient temperature (30 °C) and at elevated temperatures (55, 75 and 90 °C) at a velocity of 2 m/s using a drop weight impact tower. This was followed by flexural tests carried out at ambient temperature using a three-point bending rig. Damage assessment of impact and post-impact behaviour were carried out using ultrasonic C-scan and microfocus X-ray computed tomography (μCT). Interrupted flexural tests using μCT allowed delamination propagation to be observed. In general, lower projected damage was observed at elevated temperatures, which resulted also in a possible hindrance to delamination and shear cracks propagation during impact and in a greater amount of retained flexural strength after impact.     

3D damage characterisation and the role of voids in the fatigue of wind turbine blade materials

The fatigue mechanisms of Glass Fibre Reinforced Polymer (GFRP) used in wind turbine blades were examined using computed tomography (CT). Prior to mechanical testing, as-manufactured [+45/−45/0]_3,s glass/epoxy specimens were CT scanned to provide 3-dimensional images of their internal microstructure, including voids. Voids were segmented and extracted, and individual characteristics and volumetric distributions were quantified. The coupons were then fatigue tested in uniaxial loading at R = −1% to 40% of the nominal tensile failure stress. Some tests were conducted to failure for correlation with the initial void analysis and to establish failure modes. Other tests were stopped at various life fractions and examined using CT to identify key damage mechanisms. These scans revealed transverse matrix cracking in the surface layer, occurring predominantly at free edges. These free-edge cracks then appeared to facilitate edge delamination at the 45/−45° interface. Propagation from sub-critical, surface ply damage to critical, inner ply damage was identified with either a −45/0° delamination, or a 0° fibre tow failure allowing a crack to propagate into the specimen bulk. Final failure occurred in compression and was characterised by total delamination between all the 45/−45° plies. A quantitative void analysis, taken from the pre-test CT scans, was also performed and compared against the specimens’ fatigue lives. This analysis, to the authors’ knowledge the first of its kind, measured and plotted approximately 10,000 voids within the gauge length of each specimen. The global void measurement parameters and distributions showed no correlation with fatigue life. A local ply-level investigation revealed a significant correlation between the largest void and fatigue life in the region of the laminate associated with the crack propagation from sub-critical to critical damage.     

Cure cycle effect on impact resistance under elevated temperatures in carbon prepreg laminates investigated using acoustic emission

Voids in composites have been a perennial problem, since the amount of porosities is deemed to bear a strong relation with the degradation of service performance of laminates. On the other side, the effect of porosity on impact resistance of laminates is often dependant on their distribution in the material, especially with respect to the location and severity of impact damage in it. In this study, the influence of void content percentage on the residual flexural strength of CFRP laminates impacted at very low energy, in the region of 1 J, at different temperatures was investigated. Laminates were fabricated using 16 layers of Cycom 977-2 prepreg material in a [0/90/90/0]_2S layup with different void contents in the range from 1 to 7% by varying cure conditions. Low velocity impact tests were conducted on three categories of laminates, defined as high pressure cured, low pressure debulked and low pressure non debulked respectively, each of these at ambient temperature (30 °C) and elevated temperatures of 50, 70 and 90 °C. Post-impact residual flexural strength of the laminates was measured by three-point bending tests followed in real time by acoustic emission (AE) monitoring. From the separation of frequency bands and of their amplitude levels, identification of the different failure modes, such as matrix cracking, delamination and fibre failure, was performed. The results indicated that in the case of very low impact energy high porosity laminates, such as non debulked ones, may possess slightly higher residual flexural strength and an enhanced delamination resistance with respect to debulked ones.     

Open hole fatigue characteristics and damage growth of stitched plain weave carbon/epoxy laminates

Fatigue response of stitched plain weave carbon/epoxy laminates containing circular holes is experimentally investigated. Two carbon/epoxy laminates of cross-ply [(0/90)]₂₀ and quasi-isotropic [(±45)(0/90)₂(±45)₂(0/90)₂(±45)₂(0/90)]_s are reinforced using Kevlar-29® yarns in through-thickness direction. The laminates are drilled to produce a circular hole with diameter of 5.7 mm. Stitch configuration for cross-ply laminates is round stitch and parallel stitch, while that for quasi-isotropic laminates is parallel stitch only. For round stitch configuration, the hole is surrounded by circular stitch line of 7-mm diameter. For parallel stitch, the distance between two stitch lines (spacing) is 15 mm. In all, three independent cases are presented in this paper: Case 1 (cross-ply laminates, round stitch, tension–tension fatigue); Case 2 (cross-ply laminates, parallel stitch, tension–tension fatigue); Case 3 (quasi-isotropic laminates, parallel stitch, compression–compression fatigue). In each case, comparison with unstitched laminates is made. Case 1 shows that round stitch reduces tension fatigue curve of carbon/epoxy laminates. Round stitch seems to aggravate the damage, which is emanating from the hole rim of laminates. It gradually diverts the damage towards the edge of the specimen and causes premature fatigue failure. Case 2 shows that although parallel stitch generally does not influence the fatigue life of laminates, the damage growth due to parallel stitch is apparently unstable after 8 million cycles. As a result, laminates with parallel stitch eventually fail before reaching 10 million cycles. In contrast, unstitched laminates are able to sustain fatigue load for more than 10 million cycles. Case 3 shows that under compression fatigue load, fatigue limit of stitched plain weave laminates is better than that of the unstitched ones due to damage redistribution along the stitch lines.     

Temperature effects on mixed mode I/II delamination under quasi-static and fatigue loading of a carbon/epoxy composite

This paper addresses the effect of temperature on the mixed-mode interlaminar fracture toughness and fatigue delamination growth rate of a carbon-fibre/epoxy material, namely IM7/8552. Quasi-static and fatigue characterisation tests were carried out at −50 °C, 20 °C, 50 °C and 80 °C, using asymmetric cut-ply coupons. The experimental results show that temperature may have an accelerating or delaying effect on delamination growth, depending on the loading regime, i.e. either quasi-static or fatigue. Fractographic examinations were also carried out in order to assist the interpretation of the experimental data. A semi-empirical equation is introduced to describe the experimentally observed fatigue delamination growth rates at elevated temperatures.     

低速冲击后复合材料层合板的压缩破坏行为

对缝纫层合板和无缝纫层合板进行低速冲击后压缩破坏实验,以研究低速冲击后层合板的压缩破坏机理。采用C扫描、X射线、热揭层等技术对层合板内的损伤进行测量和对比。结果表明,界面不是很强的碳纤维增强复合材料层合板低速冲击后受压时,层合板非冲击面的子层屈曲及其扩展是导致层合板冲击后压缩强度下降的重要因素,而且子层屈曲主要是沿垂直载荷的方向(90°)扩展;对于准各向同性板,屈曲子层中与母层相邻的铺层的方向一般为90°。层合板的剩余压缩强度与板的冲击损伤面积无直接关系。      

Scaling of fracture response in Over-height Compact Tension tests

An experimental investigation into in-plane scaled Over-height Compact Tension (OCT) [45/90/−45/0]_4s carbon/epoxy laminates was carried out to study the scaling of fracture response. The dimensions of the baseline specimens were scaled up and down by a factor of 2. Interrupted tests were carried out for specimens of each size in which the tests were stopped after certain load drops in order to study the failure mechanisms. X-ray Computed Tomography (CT) scanning was applied after the interrupted tests to examine the damage development and its effect on the fracture response. The test results showed that the scaling of the initial propagation of fracture follows Linear Elastic Fracture Mechanics (LEFM), but the development of the damage process zone differs with specimen sizes. The OCT specimens were found to be not large enough to generate a self-similar damage zone during propagation, and so no conclusions could be drawn regarding the R-curve effect.     

Damage development in carbon fibre-reinforced polyimides in fatigue loading as a function of stress ratio

Carbon fibre-reinforced polyimide laminates of lay-up (O₂/±45/O₂/ ±45/90)_s have been fatigue tested at stress ratios of 0.1 and −1. Damage propagation was monitored by recording the storage modulus and rate and amplitude of acoustic emission events. The results of these tests, along with X-ray and optical photographs of damaged specimens, indicate that damage propagates in three stages: the formation of transverse cracks on 45° and 90° plies, delamination from the transverse cracks and sample failure.     

A comparative study of fatigue behaviour of flax/epoxy and glass/epoxy composites

Experimental investigations on flax and glass fabrics reinforced epoxy specimens, i.e. FFRE and GFRE, submitted to fatigue tests are presented in this paper. Samples having [0/90]_3S and [±45]_3S stacking sequences, with similar fibre volume fractions have been tested under tension–tension fatigue loading. The specific stress-number of cycles to failure (S–N) curves, show that for the [0/90]_3S specimens, FFRE have lower fatigue endurance than GFRE, but the [±45]_3S FFRE specimens offer better specific fatigue endurance than similar GFRE, in the studied life range (<2 × 10⁶). Overall, the three-stage stiffness degradation is observed in all cases except for [0/90]_3S FFRE specimens, which present a stiffening phenomenon of around 2–3% which could be related to the straightening of the microfibrils.     

Fatigue residual strength of circular laminate graphite–epoxy composite plates damaged by transverse load

The research dealt with the relation between damage and tension–tension fatigue residual strength (FRS) in a quasi-isotropic carbon fibre reinforced epoxy resin laminate. The work was organized in two phases: during the first one, composite laminates were damaged by means of an out-of-plane quasi-static load that was supposed to simulate a low velocity impact; in the second phase, fatigue tests were performed on damaged and undamaged specimens obtained from the original composite laminates. During the quasi-static transverse loading phase, damage progression was monitored by means of acoustic emission (AE) technique. The measurement of the strain energy accumulated in the specimens and of the acoustic energy released by fracture events made it possible to estimate the amount of induced damage and evaluate the quasi-static residual tensile strength of the specimens. A probabilistic failure analysis of the fatigue data, reduced by the relative residual strength values, made it possible to relate the FRS of damaged specimens with the fatigue strength of undamaged ones.     

High temperature fatigue deformation behaviors of thermally sprayed steel measured with electronic speckle pattern interferometry method

High temperature fatigue (R=0) damage and deformation behaviors of SUS304 steel thermally sprayed with Al₂O₃/NiCr coating were investigated using an electronic speckle pattern interferometry (ESPI) method. Surface cracks and delamination occurred after 1×10⁵ cycles test when σ_max was 202 MPa at 873 K. The lengths and number of cracks and delamination largely decreased when σ_max or temperature decreased to 115 MPa or 573 K, respectively. Strain values along cracks measured with the ESPI method were much larger than other areas due to crack opening under the tensile load. The positions of strain concentration zones on strain distribution figures by ESPI method were well corresponded to those of cracks on sprayed coatings. Strain values decreased largely where local delamination occurred.     

Compression fatigue failure of CFRP laminates with impact damage

The objective of this study is to investigate failure mechanisms of impact-damaged CFRP laminates subjected to compression fatigue. Two kinds of composite materials, UT500/Epoxy and AS4/PEEK, were used to examine the dependence of failure behavior on the material properties such as interlaminar toughness. Impact-induced delaminations in the UT500/Epoxy specimen were considerably larger than those in the AS4/PEEK specimen. The S–N curves for the UT500/Epoxy specimens with impact damage exhibited a similar tendency to those without impact. The impact-induced delamination in the UT500/Epoxy specimen grew widthwise to the free edge on the rear side of the specimen during the fatigue test. On the other hand, the AS4/PEEK specimens without impact exhibited a more steeply declining S–N curve than those with impact damage. The delaminations in the impacted AS4/PEEK specimen did not reach the free edge before the fatigue fracture.     

Investigation of the response to low velocity impact and quasi-static indentation loading of particle-toughened carbon-fibre composite materials

This work investigates damage caused by low velocity impact and quasi-static indentation loading in four different particle-toughened composite systems, and one untoughened system. For impact tests, a range of energies were used between 25 and 50 J. For QSI, coupons were interrupted at increasing loading point displacement levels from 2 to 5 mm to allow for monitoring of damage initiation and propagation. In both loading cases, non-destructive inspection techniques were used, consisting of ultrasonic C-scan and X-ray micro-focus computed tomography. These techniques are complemented with instrumentation to capture force–displacement data, whereby load-drops are associated with observed damage modes. Key results from this work highlight particular issues regarding strain-rate sensitivity of delamination development and an earlier onset of fibre fracture associated with particle-toughened systems. These issues, in addition to observations on the role of micro-scale events on damage morphology, are discussed with a focus on material development and material testing practices.     

Progressive damage assessment of centrally notched composite specimens in fatigue

The aim of this study is to assess the residual properties and the corresponding damage states within centrally notched quasi-isotropic [0/−45/+45/90]_S T650/F584 (Hexcel) carbon-fiber/epoxy composites subjected to fatigue loading using Digital Image Correlation (DIC), radiography, and a non-contact vibration measurement technique. Quasi-static tests were performed on virgin samples using DIC to determine the full-field in-plane strains at different applied load levels. Fatigue tests were interrupted during the fatigue lifetimes in order to perform quasi-static tests with DIC measurements. Non-contact vibration measurements were performed to investigate the effect of fatigue damage on residual frequency responses. X-ray computed tomography was used to determine the type, location, and extent of fatigue damage development. The results provide an important step in the validation of DIC and vibration response as a powerful combined non-destructive evaluation tool for monitoring the development of fatigue damage as well as predicting the damage level of notched composite materials.