Strength and interface failure mechanism of adhesive joints

Adhesive joints have a wide range of applications in the civil engineering, automotive and aircraft industries. In the present research, we use the finite element method to systematically study the overall strength and interface failure mechanism of single lap joints, which are subjected to tensile loading, focusing on the effects of various system parameters including fracture energy of the adhesive layer, overlap length and adhesive layer thickness on the load-bearing capability of the joints. The results show that the overlap length and the adhesive fracture energy have combined influences on the load-bearing capability. On the other hand, a preliminary damage analysis of the adhesive layer is carried out, considering the situations when the loads arrive to the peak values. Furthermore, the interface behavior is investigated, including the interface stress analysis and interface slip. The rotation of the joint during loading and its influence factors are studied as well. Obtained results suggest that the interface stress distributions are related to the slip and the rotation angle.     

Strength prediction of epoxy adhesively bonded scarf joints of dissimilar adherends

In this study, strength of epoxy adhesively bonded scarf joints of dissimilar adherends, namely SUS304 stainless steel and YH75 aluminum alloy is examined on several scarf angles and various bond thicknesses under uniaxial tensile loading. Scarf angle, θ=45°, 60° and 75° are employed. The bond thickness, t between the dissimilar adherends is controlled to be ranged between 0.1 and 1.2 mm. Finite element (FE) analysis is also executed to investigate the stress distributions in the adhesive layer of scarf joints by ANSYS 11 code. As a result, the apparent Young's modulus of adhesive layer in scarf joints is found to be 1.5-5 times higher than those of bulk epoxy adhesive, which has been obtained from tensile tests. For scarf joint strength prediction, the existing failure criteria (i.e. maximum principal stress and Mises equivalent stress) cannot satisfactorily estimate the present experimental results. Though the measured stress multiaxiality of scarf joints proportionally increases as the scarf angle increases, the experimental results do not agree with the theoretical values. From analytical solutions, stress singularity exists most pronouncedly at the steel/adhesive interface corner of joint having 45-75° scarf angle. The failure surface observations confirm that the failure has always initiated at this apex. This is also in agreement with stress-y distribution obtained within FE analysis. Finally, the strength of scarf joints bonded with brittle adhesive can be best predicted by interface corner toughness, Hc parameter.     

Failure behaviour of the single lap joints of angle-plied composites under three point bending tests

Abstract

In this paper, the response of adhesively-bonded single lap joints (SLJs) with angle-plied composite adherends subjected to flexural loading was investigated. The experiments were carried out for the adherends, glass reinforced polymer matrix, with three kinds of stacking sequence. A three-dimensional finite element (FE) model was developed using ABAQUS/Explicit. The three dimensional Hashin failure criterion with an appropriate damage evolution law was used to characterize the damage inside a ply. Cohesive zone elements were used to model the damage in the adhesive layer (AF163-2K) and the interply failure, that is, the delamination. The developed numerical model was verified with the performed experiments. The SLJs of [±20]_5s and [±45]_5s failed due to failure in the adhesive layer and the delamination between the plies, whereas that of [±10]_5s failed mainly due to the former failure. The intralaminar damage was not noticed for any case. The influence of the fiber angle of plies in the adherends, adherend thickness, overlap length, and the thickness of adhesive layer on the damage in the adhesive layer and the delamination were investigated in terms of the competition between these two failures and activation of different failure modes in each thoroughly.     

Deformation and fracture of adhesive layers constrained by plastically-deforming adherends

The use of an embedded-process zone (EPZ) model to investigate the mode I cohesive parameters for plastically-deforming, adhesively-bonded joints is demonstrated in this paper. It is shown that for the particular systems investigated, the cohesive parameters are consistent with an adhesive layer deforming in accordance with its bulk constitutive properties (as constrained by the adherends). In other words, these systems provide examples where the cohesive tractions exerted by an adhesive layer can be calculated simply from considerations of the constrained deformation of the adhesive. Consistent with such calculations, the peak stress in the adhesive layer decreases as the level of the constraint decreases (either with an increase in the thickness of the adhesive layer or with a decrease in the thickness of the adherends). It is also shown that owing to a compensating effect in which the critical displacement for failure varies with the constraint, the energy absorbed by the adhesive layer (the 'intrinsic' toughness of the joint) is essentially independent of the geometry in these systems.     

Metallic multi-material adhesive joint testing and modeling for vehicle lightweighting

While adhesive bonding has been shown to be a beneficial technique to join multi-material automotive bodies-in-white, quantitatively assessing the effect of adherend response on the ultimate strength of adhesively bonded joints is necessary for accurate joint design.In the current study, thin adherend single lap shear testing was carried out using three sheet metals used to replace mild steel when lightweighting automotive structures: hot stamped Usibor® 1500 AS ultra-high strength steel (UHSS), aluminum (AA5182), and magnesium (ZEK 100). Six combinations of single and multi-material samples were bonded with a one-part toughed structural epoxy adhesive and experimentally tested to measure the force, displacement across the bond line, and joint rotation during loading. Finite element models of each test were analyzed using LS-DYNA to quantitatively assess the effects of the mode mixity on ultimate joint failure. The adherends were modeled with shell elements and a cohesive zone model was implemented using bulk material properties for the adhesive to allow full three-dimensional analysis of the test, while still being computationally efficient.The UHSS-UHSS joint strength (27.2 MPa; SD 0.6 MPa) was significantly higher than all other material combinations, with joint strengths between 17.9 MPa (SD 0.9 MPa) and 23.9 MPa (SD 1.4 MPa). The models predicted the test response (average R2 of 0.86) including the bending deformation of the adherends, which led to mixed mode loading of the adhesive. The critical cohesive element in the UHSS-UHSS simulation predicted 85% Mode II loading at failure while the other material combinations predicted between 41% and 53% Mode II loading at failure, explaining the higher failure strength in the UHSS-UHSS joint.This study presents a computational method to predict adhesive joint response and failure in multi-material structures, and highlights the importance of the adherend bending stiffness and on joint rotation and ultimate joint strength.     

Dynamic strength of single lap joints with similar and dissimilar adherends

The increased use of adhesives for joining structural parts demands a thorough understanding of their load carrying capacity. The strength of the adhesive joints depends on several factors such as the joint geometry, adhesive type, adherend properties and also on the loading conditions. Particularly polymer based adhesives exhibit sensitivity to loading rate and therefore it is important to understand their behavior under impact like situations. The effect of similar versus dissimilar adherends on the dynamic strength of adhesive lap joints is addressed in this study. The dynamic strength is evaluated using the split-cylinder lap joint geometry in a split Hopkinson pressure bar setup. The commercial adhesive Araldite 2014 is used for preparing the joints. The adherend materials considered included steel and aluminum. The results of the study indicated that the dynamic strength of the lap joint is influenced by the adherend material and also by the adherent combination. Even in the case of joints with similar adherends, the strength was affected by the adherend type. The strength of steel–steel joints was higher than that for aluminum–aluminum joints. In the case of dissimilar adherends, the strength was lower than that of the case of similar adherends. The results of this study indicate that the combination of adherend material should also be accounted for while designing lap joints.     

Study on the fatigue strength of AA 6082-T6 adhesive lap joints

A research study on the fatigue behaviour of aluminium alloy adhesive lap joints was carried out to understand the effect of surface pre-treatment and adherends thickness on the fatigue strength of adhesive joints. The adherend material used for the experimental tests was an aluminium alloy 6082-T6 in the form of thin sheets, and the adhesive used was a high strength epoxy (Araldite 420 A/B). The surface preparation included an abrasive preparation (AP joints) and sodium dichromate–sulphuric acid etch (CSA joints).A maximum fatigue strength was obtained for the CSA surface treatment with a 1.0 mm adherends’ thickness. The fastest fatigue damage was related with a high surface roughness and a high stress perpendicular to adhesive surface, which helps to promote the adhesive failure. A numerical analysis was also performed to understand the effect of the adherends thickness on the stress level. Results showed an increase of the out-of-plane peak stresses with the increase of adherends thickness.     

Investigation of optimal surface treatments for carbon/epoxy composite adhesive joints

Although an adhesive joint can distribute the load over a larger area than a mechanical joint, requires no holes, adds very little weight to the structure and has superior fatigue resistance, but it not only requires a careful surface preparation of the adherends but also is affected by service environments. In this paper, suitable conditions for surface treatments such as plasma surface treatment, mechanical abrasion, and sandblast treatment were investigated to enhance the mechanical load capabilities of carbon/epoxy composite adhesive joints. A capacitively coupled radiofrequency plasma system was used for the plasma surface treatment of carbon/epoxy composites and suitable surface treatment conditions were experimentally investigated with respect to gas flow rate, chamber pressure, power intensity, and surface treatment time by measuring the surface free energies of treated specimens. The optimal mechanical abrasion conditions with sandpapers were investigated with respect to the mesh number of sandpaper, and optimal sandblast conditions were investigated with respect to sandblast pressure and particle size by observing geometric shape changes of adherends during sandblast process. Also the failure modes of composite adhesive joints were investigated with respect to surface treatment. From the peel tests on plasma treated composite adhesive joints, it was found that all composite adhesive joints failed cohesively in the adhesive layer when the surface free energy was higher than about 40 mJ/m², because of high adhesion strength between the plasma treated surface and the adhesive. From the peel tests on mechanically abraded composite adhesive joints, it was also found that the optimal surface roughness and adhesive thickness increased as the failure load increased.     

Effect of thermal cycling on tensile properties of degraded FML to metal hybrid joints exposed to sea water

In the present paper, the mechanical properties of hybrid bonded bolted joints between Fiber metal laminate (FML) and stainless steel adherends are investigated using experimental tensile tests. Three and five layered FMLs were fabricated using 430 stainless steel sheets and fiberglass prepreg layers. The adherends were bonded by AD-314 resin mixed with HA-34 hardener as adhesive and steel bolt was used for the mechanical fastening. The specimens were immersed into the sea water for 30 days and degradation of the mechanical strength of the joints was studied. Thermal cycles including heating (40 °C to100 °C) and cryogenic (−100 °C to −40 °C) cycles were applied in order to study their effects on the strength of the degraded joints. The failure mode for the adhesive bond was mixed failure and that of the bolted joint was the net-tension failure. The results showed 52% strength recovery in hybrid joints subjected to heating cycles. Cryogenic cycles also caused a 50% improvement in the tensile strength of the hybrid joints. In addition, the joint stiffness and absorbed energy of the specimens were improved significantly for both heating and cryogenic cycles. Moreover, the effect of FML stacking sequence on the results was also investigated. The results revealed that the mechanical fastening failure load for 5 layered FML joint is more affected by thermal cycles in comparison with 3 layered FML joint.     

Adhesion failure propagation in adhesively-bonded single-lap laminated FRP composite joints

This paper deals with three-dimensional non-linear finite element analyses to study the behaviour of embedded adhesion failure propagation in adhesively-bonded single-lap laminated FRP composite joints clamped at one end and subjected to uniform extension at the other end. Because of loading eccentricity and joint material heterogeneity, the embedded adhesion failure is likely to initiate from the stress singularity points and will propagate from either end of the adhesive layer along the adherend–adhesive interfaces. The effects of interaction of such failures and their propagations along the interfaces of the adherends and adhesive are the main concerns of this paper. The peel and shear stresses have been computed along the mid-surface of the adhesive layer for varying adhesion failure lengths to find out the influence of adhesion failure length on the strength of the joint being analyzed. The concept of fracture mechanics has been used to calculate the strain energy release rate (SERR) as the adhesion failure propagates using the virtual crack closure technique (VCCT). It is seen that mode-II SERR is predominant in the propagation of such adhesion failures. The SERR values computed with respect to the adhesion failure lengths being propagated from the two ends of the adhesive layer are seen to be different.     

Drop weight tensile impact testing of adhesively bonded carbon/epoxy laminate joints

Crashworthiness of composite structures is a key issue for the design of lightweight vehicles. In particular the joined parts of the structures must be able to absorb a high amount of energy in order to protect the passengers. In this paper the dynamic behavior of adhesively bonded carbon/epoxy laminate joints is investigated. The adherends are made of unidirectional plies, whose orientations are carefully chosen in order to assess the influence of the adherend mechanical properties on the joint behavior. A drop weight machine has been modified in order to impact specimens under tension. Single lap joints are tested under impact tension at velocities from 1 to 4 m/s. Results of the impact tests that are compared to reference quasi-static test results emphasize the rate-sensitivity of the joints. The stiffness, the failure load and the absorbed energy all increase with increasing loading rate. One major result is that the joint behavior is qualitatively the same under quasi-static and impact loading: the failure mode and the joint ranking (based on their strength) remain identical. Therefore the impact design of the adhesive joints could be based on a static design at moderate loading rates.     

CRACK GROWTH IN ADHESIVELY BONDED JOINTS SUBJECTED TO VARIABLE FREQUENCY FATIGUE LOADING

The main aim of this article is to investigate the effect of frequency on fatigue crack propagation in adhesively bonded joints. Adhesively bonded double-cantilever beam (DCB) samples were tested in fatigue at various frequencies between 0.1 and 10 Hz. The adhesive used was a toughened epoxy, and the substrates used were a carbon fibre-reinforced polymer (CFRP) and mild steel. Results showed that the crack growth per cycle increases and the fatigue threshold decreases as the test frequency decreases. The locus of failure with the CFRP adherends was predominantly in the adhesive layer, whereas the locus of failure with the steel adherends was in the interfacial region between the steel and the adhesive. The crack growth was faster, for a given strain energy release rate, and the fatigue thresholds lower for the samples with steel adherends. Tests with variable frequency loading were also carried out, and a generalised method of predicting crack growth in samples subjected to a variable frequency loading was introduced. The predicted crack growth using this method agreed well with experimental results.     

Moisture absorption–desorption effects in adhesive joints

This paper presents a study of moisture absorption–desorption effects in single lap adhesive joints. Experiments were carried out to characterise the moisture uptake of the single part epoxide adhesive, FM73. Tensile testing of single lap joints manufactured from aluminium alloy 2024 T3 and O and FM73 adhesive was carried out after the joints were exposed to different conditioning environments. The experimental results revealed that the failure strength of the single lap joints with 2024 T3 adherends progressively degraded with time when conditioned at 50 °C, immersed in water. However, the joint strength almost completely recovered after moisture was desorbed. The single lap joints with 2024 O adherends showed decreased strength for 28 days of conditioning, after which strength recovered, reaching a plateau after 56 days. Again, strength almost completely recovered on desorption of moisture. The strength recovery of the joints, after desorption of moisture, showed that the degradation of the adhesive was largely reversible. Analysis of the failure surfaces revealed that the dry joints failed cohesively in the adhesive layer and that the failure path moved towards the interface after conditioning. The failure mode then reverted back to cohesive failure after moisture desorption.     

Determination of the impact tensile strength of structural adhesive butt joints with a modified split Hopkinson pressure bar

The impact tensile strength of structural adhesive butt joints was determined with a modified split Hopkinson pressure bar using hat-shaped specimens. A typical two-part structural epoxy adhesive (Scotch weld^® DP-460) and two different adherend materials (Al alloy 7075-T6 and commercially pure titanium) were used in the adhesion tests. The impact tensile strength of adhesive butt joints with similar adherends was evaluated from the peak value of the applied tensile stress history. The corresponding static tensile strengths were measured on an Instron testing machine using joint specimens of the same geometry as those used in the impact tests. An axisymmetric finite element analysis was performed to investigate the static elastic stress distributions in the adhesive layer of the joint specimens. The effects of loading rate, adherend material and adhesive thickness on the joint tensile strength were examined. The joint tensile strength was clearly observed to increase with the loading rate up to an order of 10⁶ MPa/s, and decrease gradually with the adhesive thickness up to nearly 180 μm, depending on the adherend materials used. The loading rate dependence of the tensile strength was herein discussed in terms of the dominant failure modes in the joint specimens after static and impact testing.     

Analysis and design of adhesive-bonded tee joints

In this study, the stresses in adhesive-bonded tee joints, in which a right-angled plate is bonded to a rigid plate with an adhesive, have been analysed with a finite element method. It was assumed that the adhesive and adherends had linear elastic properties. The tee joint was analysed under three loading conditions, two linear and one bending moment. The stress distributions in the joint area are given by stress contours and XY plots under the three load conditions. It was found from the results that high stress concentrations occur in the inside corner of the angle plate for loading in the x-direction (P_x) and under bending moment (M), this suggesting that failure would not occur in the bonded joint. However, for loading in the y-direction (P_y), the maximum normal stresses are concentrated at the left free end of the adhesive layer in the joint, and the first failure may be expected at this edge. Since the geometry of the joints affects the analysis and design of such joints, the influences on the stress distributions of the overlap length, adhesive thickness and adherend thickness were investigated. Practical experiments were carried out and it was found that experimental results were in good agreement with those of the finite element analysis.     

Numerical Study of Adhesive Single-Lap Joints with Composite Adherends Subjected to Combined Tension–Torsion Loads

The present investigation focuses on modifying the strength of single-lap adhesively bonded joints under tension–torsion loading with the use of three-dimensional finite element (FE) modeling. A single-lap adhesively bonded joint is reinforced by fibers and analyzed by means of ABAQUS-6.9.1 FE code. The adherends are considered to be made of orthotropic materials, while the adhesive is neat resin or reinforced by various types of fibers. The carbon and glass unidirectional fibers are used for adhesive reinforcement. In the FE modeling, the behavior of all the members is assumed to be linear elastic. The ultimate bond strength is increased as the fiber volume fraction in the adhesive is increased. By changing the properties and the behavior of the adhesive from neat resin (isotropic) to fiber composite adhesive (orthotropic) and with various fiber volume fractions and by changing the orientation of the fibers in the adhesive region with respect to the global axes, the bond strength in tension–torsion loadings are changed. Also, the excessive adhesive layer is modeled and its effect on the joint strength is investigated.     

Crack growth in adhesively bonded joints subjected to variable frequency fatigue loading

The main aim of this article is to investigate the effect of frequency on fatigue crack propagation in adhesively bonded joints. Adhesively bonded double-cantilever beam (DCB) samples were tested in fatigue at various frequencies between 0.1 and 10 Hz. The adhesive used was a toughened epoxy, and the substrates used were a carbon fibre-reinforced polymer (CFRP) and mild steel. Results showed that the crack growth per cycle increases and the fatigue threshold decreases as the test frequency decreases. The locus of failure with the CFRP adherends was predominantly in the adhesive layer, whereas the locus of failure with the steel adherends was in the interfacial region between the steel and the adhesive. The crack growth was faster, for a given strain energy release rate, and the fatigue thresholds lower for the samples with steel adherends. Tests with variable frequency loading were also carried out, and a generalised method of predicting crack growth in samples subjected to a variable frequency loading was introduced. The predicted crack growth using this method agreed well with experimental results.     

Effect of Adhesive Thickness on Joint Strength: A Molecular Dynamics Perspective

Recent studies suggest that adhesion in thin joints depends on several factors including temperature, interface toughness, strain rate, surface roughness of adherends, bondline thickness of adhesives, and many others. Influence of thickness on joint properties is surprising but experimentally well documented without reasonable explanations. In this study, we attempt to address the mechanical behavior of polymer adhesives by molecular dynamics (MD) simulation. We show that interfacial strength of the joints in tensile, shear, or combined loading significantly depends on the coupling strength between adhesives and adherends. Failure of joints is always at the interface when coupling strength is weaker. With stronger interfaces, cohesive failure occurs by cavitation or by bulk shear depending on the loading condition. When joints are loaded in tension, it requires an exceedingly stronger interface to realize pure shear failure, otherwise failure is through interface slip. Under a mixed mode condition, interface slip is difficult to avoid. As long as failure is not at the interface alone, the yield strength of joints improves significantly with the reduction of thickness. Increase in bulk density and change in polymer configurations with the reduction of adhesive thickness are believed to be the two key factors in improving mechanical behavior of adhesives.     

The effects of surface roughness and bond thickness on the fatigue life of adhesively bonded tubular single lap joints

Since the surface roughness of adherends greatly affects the strength of adhesively bonded joints, the effect of surface roughness on the fatigue life of adhesively bonded tubular single lap joints was investigated analytically and experimentally by a fatigue torsion test. The stiffness of the interfacial layer between the adherends and the adhesive was modelled as a normal statistical distribution function of the surface roughness of the adherends. From the investigation, it was found that the optimum surface roughness of the adherends for the fatigue strength of tubular single lap joints was dependent on the bond thickness and applied load.     

Development of a Computer Program for the Design of Adhesive Joints

Adhesive joints are increasingly being used due to their improved mechanical performance and a better understanding of the mechanics of failure. To predict the joint strength, one must have the stress distribution and a suitable failure criterion. The literature contains many closed-form solutions for the stress distribution. However, the models are sometimes difficult to implement and use. The objective of the present work was to compile existing models of increasing complexity into user friendly software. Three main situations were considered: elastic adherends and adhesive, elastic adherends with nonlinear adhesive and nonlinear analyses for both adherends and adhesive. The adherends were both isotropic (metals) and anisotropic (composites). The joints considered are the single and double lap joints for most of the models. However, a sandwich model initially proposed by Crocombe can be used for any type of joint provided the boundary conditions are known. For each model proposed the compatible failure criteria are included to enable the user not only to have the stress distribution but also the failure load for a given joint/load scenario. Experimental tests corresponding to the three cases described above were carried out to validate the models implemented.