Development of Micro-SQUID Magnetometers for Investigation of Quantum Tunneling of Magnetization in Nanometer-Size Magnetic Materials

We report development of micro superconducting quantum interference device (μ-SQUID) magnetometers for investigation of quantum tunneling of magnetization in μm- and nm-size magnetic materials. Both high- and low-temperature superconductor (HTS and LTS) based μ-SQUID magnetometers were fabricated and a three dimensional magnetic coil system was constructed for this purpose. The HTS-μ-SQUIDs with a hole of 4×9 μm² work at temperatures between 4.2 and 70 K and in magnetic fields up to 120 mT. A magnetization measurement of a ferrimagnetic micro-crystal was carried out at 35 K with an accuracy of 10^?9 emu. The development of LTS-μ-SQUIDs has been started in order to study much smaller magnetic materials in a mK temperature range. We present a preliminary result on the LTS-μ-SQUID with a hole of 1×1 μm². The critical current as a function of applied magnetic field shows the SQUID modulation at 4.2 K and up to 30 mT. The heat release associated with the present measurement method is estimated to be on the order of several microwatts.     

Role of Coexistence of Superconductivity and Paramagnetism in Magnetostriction of High-T c Superconductors

Total magnetostriction in the superconducting state for high T _c superconductors has been separated into critical state and paramagnetic components in terms of a H(x) dependent magnetic flux density. We show that the paramagnetic part is χ(2+χ)〈H(x)²〉, where χ is paramagnetic susceptibility. We have reproduced successfully ΔL/L−H _a curves measured by de la Fuente et al. (Phys. C 244:214, [1995]), in which they clearly observed coexistence of superconductivity and paramagnetism, employing the concepts presented in this work.      

Modeling of the dynamic characteristics of two‐bolt‐joints

Abstract

In this paper, a method to identify the damping and stiffness properties of bolted joints from a substructure synthesis scheme is presented. The easily measured frequency response functions of substructures and the assembled structure are the only data needed in this method. A synthesis formula used to predict the frequency response functions of two‐bolt‐joint structures is proposed. The formula makes use of the extracted properties of a single‐bolt‐joint. Some experiments with two free‐free steel beams jointed with one or two bolts are made to check this method. The close correlation between predicted and measured results demonstrates that this method is acceptable.     

The design of an intelligent real‐time autonomous vehicle,TAIWAN iTS‐1

Abstract

Developed at National Chiao Tung University, TAIWAN iTS‐1 is the first smart car with active safety systems and comfortable autonomous driving in Taiwan. An adaptive vision‐based lane detection algorithm was proposed to help the lateral control unit to keep the car in its lane safely. It also carries a DSP system to generate warning signals for unintentional roadway departures. A laser radar measures the distance between the preceding car and TAIWAN iTS‐1. With this information, the longitudinal control unit performs intelligent cruise control and stop‐and‐go functions. The remote control function is realized on TAIWAN iTS‐1 for safety testing and military applications. Unlike most smart car studies, this paper considers not only driving safety demands but also non‐driving security. An active mobile surveillance system will inform the car owner when the car is illegally broken into, anytime and anywhere. For drivers and passengers, the perception of comfort is achieved by intelligent vehicle dynamic control. All functions integrated into TAIWAN iTS‐1 have been tested repeatedly on National Highway 3 and Expressway 68 in the Hsinchu area and the system's robustness has been successfully demonstrated in these real‐road experiments.     

Characterization of the Response of CaWO4 on Recoiling Nuclei from Surface Alpha Decays

A potentially harmful background for experiments attempting direct dark matter detection like the CRESST (= Cryogenic Rare Event Search with Superconducting Thermometers) experiment is caused by recoiling nuclei from ²¹⁰Po alpha decays on surfaces close to the detector. In order to characterize this kind of background in CRESST, calibration measurements have been performed at the TU München. A for this purpose an optimized version of the CRESST detector has been developed consisting of a 38 g CaWO₄ crystal and a separate cryogenic light detector, both equipped with Ir/Au transition edge sensors (TESs). The simultaneous measurement of the phonon signal and the scintillation light from the CaWO₄ crystal allows to discriminate between electron and nuclear recoils using their different light outputs. The unexpected results of a first measurement with a ²¹⁰Po source can be understood with the help of a Monte Carlo simulation performed for a similar system.      

Process of Cooling of a High‐Temperature Two‐Phase Flow

A technique and a design of a transducer for measuring the enthalpy of twophase flows using the thinwall method have been developed. Working formulas for calculating the heat capacity and the enthalpy of a gas flow are substantiated. Results of a test of the transducer in hightemperature flows of powder gases, including those after the packing of a coolant, are presented. The results obtained show that cooling of powder gases due to an endothermic reaction makes it possible to decrease the enthalpy flux by a factor of 5 and the temperature by a factor of 2.     

Enhancement of Sudden Death of Entanglement for Driven Qubits

We study the recently discovered phenomena of sudden death of entanglement for a system of two qubits, each of them independently longitudinally damped by a reservoir and subjected to a continuous driving. We show that driving produces, in the interaction picture, an effective bath that has elements amounting to various extra sources of noise (transverse, thermal squeezed, thermal longitudinal). As a result, the time of sudden death decreases due to driving, which we verify as well by direct numerical calculation. We suggest that this phenomenon can be studied systematically using superconducting qubits driven by microwave fields.     

Dispersion-Induced Splitting of the Collective Mode Spectrum in Axial and Planar Phases of Superfluid 3He

The whole collective mode spectrum in axial and planar phases of superfluid ³He with dispersion corrections is calculated for the first time. In axial A-phase the degeneracy of clapping modes depends on the direction of the collective mode momentum k with respect to the vector l (mutual orbital moment of Cooper pairs), namely: the mode degeneracy remains the same as in case of zero momentum k for k‖l only. For any other directions there is a threefold splitting of these modes, which reaches maximum for k ⊥ l. In planar 2D-phase, which exists in the magnetic field (at H>H _C ) we find that for clapping modes the degeneracy depends on the direction of the collective mode momentum k with respect to the external magnetic field H, namely: the mode degeneracy remains the same as in case of zero momentum k for k‖H only. For any other directions different from this one (for example, for k ⊥ H) there is twofold splitting of these modes. The obtained results imply that new interesting features can be observed in ultrasound experiments in axial and planar phases: the change of the number of peaks in ultrasound absorption into clapping mode. One peak, observed for these modes by Ling et al. (J. Low Temp. Phys. 78:187, 1990), will split into two peaks in a planar phase and into three peaks in an axial phase under the change of ultrasound direction with respect to the external magnetic field H in a planar phase and with respect to the vector l in an axial phase. In planar phase, some Goldstone modes in the magnetic field become massive (quasi-Goldstone) and have a similar twofold splitting under the change of ultrasound direction with respect to the external magnetic field H. The obtained results as well will be useful under interpretation of the ultrasound experiments in axial and planar phases of superfluid ³He.     

Theory of Decay of Superfluid Turbulence in the Low-Temperature Limit

We review the theory of relaxational kinetics of superfluid turbulence—a tangle of quantized vortex lines—in the limit of very low temperatures when the motion of vortices is conservative. While certain important aspects of the decay kinetics depend on whether the tangle is non-structured, like the one corresponding to the Kibble-Zurek picture, or essentially polarized, like the one that emulates the Richardson-Kolmogorov regime of classical turbulence, there are common fundamental features. In both cases, there exists an asymptotic range in the wavenumber space where the energy flux is supported by the cascade of Kelvin waves (kelvons)—precessing distortions propagating along the vortex filaments. At large enough wavenumbers, the Kelvin-wave cascade is supported by three-kelvon elastic scattering. At zero temperature, the dissipative cutoff of the Kelvin-wave cascade is due to the emission of phonons, in which an elementary process converts two kelvons with almost opposite momenta into one bulk phonon. Along with the standard set of conservation laws, a crucial role in the theory of low-temperature vortex dynamics is played by the fact of integrability of the local induction approximation (LIA) controlled by the parameter Λ=ln?(λ/a ₀), with λ the characteristic kelvon wavelength and a ₀ the vortex core radius. While excluding a straightforward onset of the pure three-kelvon cascade, the integrability of LIA does not plug the cascade because of the natural availability of the kinetic channels associated with vortex line reconnections. We argue that the crossover from Richardson-Kolmogorov to the Kelvin-wave cascade is due to eventual dominance of local induction of a single line over the collective induction of polarized eddies, which causes the breakdown of classical-fluid regime and gives rise to a reconnection-driven inertial range.     

Application of variable‐structure system in dc‐motor velocity‐control

Abstract

The most important characteristic of variable‐structure system (VSS) is its insensitivity to parameter variations in the sliding mode. In this paper three methods of VSS are used to implement DC‐motor velocity‐control. The conventional VSS uses only a sliding line. The adaptive VSS uses multiple switching lines. The modern method uses a sliding curve. The modern method makes a system trajectory following the sliding curve which has been set up in the controller from the initial state to the origin in the phase plane. Hence it is insensitive to parameter variations from the initial state to the steady state. If parameter variations are the most critical factors, then the modern VSS is the right method to be considered to overcome the problem of parameter variations.     

Widening the Scope of Working of Solid‐State Nd‐Glass Lasers

With the example of the serial model of a pulsed Ndglass laser, it is shown that the use of an unstable resonator with a semireflecting homogeneous exit mirror makes it possible to significantly decrease the laserbeam divergence and increase the uniformity of the radiationintensity distribution in the near zone. We were the first to obtain a laserbeam quality of (40–50) mm·mrad for technological glass lasers and to attain a depth of fusing of of 6.3 mm for steel (aspect ratio 10) for an energy of 23 J. The obtained uniformity of the radiationintensity distribution was estimated at the level of ±10%. The beamquality level attained for the Ndglass laser beam allows us to recommend it for both realization of deepfusion regimes and laser hardening without the use of external integrating optical elements.     

Cytotoxicity of single-walled carbon nanotubes suspended in various surfactants

The cytotoxicity of single-walled carbon nanotubes (SWCNTs) suspended in various surfactants was investigated by phase contrast light microscopy characterization in combination with an absorbance spectroscopy cytotoxicity analysis. Our data indicate that individual SWCNTs suspended in the surfactants, sodium dodecyl sulfate (SDS) and sodium dodecylbenzene sulfonate (SDBS), were toxic to 1321N1 human astrocytoma cells due to the toxicity of SDS and SDBS on the nanotube surfaces. This toxicity was observed when cells were exposed to an SDS or SDBS solution having a concentration as low as 0.05?mg?ml(-1) for 30?min. The proliferation and viability of the cells were not affected by SWCNTs alone or by conjugates of SWCNTs with various concentrations of sodium cholate (SC) or single-stranded DNA. The cells proliferated similarly to untreated cells when surrounded by SWCNTs as they grow, which indicated that the nanotubes did not affect cells adversely. The cytotoxicity of the nanotube-surfactant conjugates was controlled in these experiments by the toxicity of the surfactants. Consequently, when evaluating a surfactant to be used for the dispersion of nanoscale materials in applications such as nanoscale electronics or non-viral biomolecular transporters, the cytotoxicity needs to be evaluated. The methodology proposed in this study can be used to investigate the cytotoxicity of other nanoscale materials suspended in a variety?of?surfactants.     

Investigation of Thermal Processes in Gas‐Thermal Spraying of Metal‐Ceramic Coatings

The features of the thermal regime of gasthermal deposition of metalceramic coatings have been studied. The procedure of calculation of the temperature field of a multicomponent coating throughout the process of formation has been developed. The quantitative dependences of the character of heating of the deposited particles and melting of the substrate on the thermophysical properties and chemical composition of the material, the intensity of heat exchange, and the technological parameters of the process have been established. The thermal conditions of spraying of powder compositions, which ensure improved strength characteristics of the coating–substrate system, have been determined.     

Quasi‐Self‐Similar Description of an Exhaust Jet

The method of construction of an analytical solution for the far field of an exhaust jet on the basis of the quasiselfsimilar solution of Prandtl equations and the turbulence model with one differential equation for the coefficient of kinematic viscosity is described. An exact numerical solution for distances to about 10¹ radii of the nozzle is constructed for the basic version. Then, a numerical solution and its analytical approximation by the quasiselfsimilar solution are constructed. Approximations of the similarity parameters of the selfsimilar problem as functions of the similarity parameters of the initial problem in the form of polynomials allow construction of analytical solutions for different situations, which are in satisfactory agreement with the exact numerical solution at distances of radii.     

The predominant role of collagen in the nucleation, growth, structure and orientation of bone apatite

The involvement of collagen in bone biomineralization is commonly admitted, yet its role remains unclear. Here we show that type I collagen in?vitro can initiate and orientate the growth of carbonated apatite mineral in the absence of any other vertebrate extracellular matrix molecules of calcifying tissues. We also show that the collagen matrix influences the structural characteristics on the atomic scale, and controls the size and the three-dimensional distribution of apatite at larger length scales. These results call into question recent consensus in the literature on the need for Ca-rich non-collagenous proteins for collagen mineralization to occur in vivo. Our model is based on a collagen/apatite self-assembly process that combines the ability to mimic the in vivo extracellular fluid with three major features inherent to living bone tissue, that is, high fibrillar density, monodispersed fibrils and long-range hierarchical organization.     

Norton-Corrected Measurement of Complex Impedances of a Large Format Bolometer Array

We report on our efforts to measure simultaneously a well-calibrated complex impedance of a large number of detectors in a long wavelength bolometer array. The array is described in other presentations. A method for correcting the complex impedance measurements of bolometers and calorimeters has been presented by Lindeman et al. (Rev. Sci. Instrum. 78:043105, [2007]) using a Thévenin equivalent circuit to represent the bias network. We have built on this method for superconducting bolometers with a Norton equivalent circuit and have used it to improve our impedance data. We further describe our method for extracting a Norton-corrected complex impedance as a function of frequency from a stream of multiplexed time-ordered data. This method is well-suited to producing simultaneous complex impedance measurements for a large number of detectors.      

Properties of Tungsten Thin Films Produced with the RF-Sputtering Technique

For the purpose of building very sensitive light and phonon detectors, as e.g. applied in the Dark Matter (DM) experiment CRESST (Cryogenic Rare Event Search with Superconducting Thermometers), transition edge sensors (TESs) in combination with a massive absorber crystal are used. To ensure high sensitivity of the detectors, low heat capacities, i.e. low working temperatures of about 10 mK are aimed at. Therefore, TESs made of tungsten thin films exhibiting the alpha-tungsten (α-W) phase with transition temperatures of T _c =10–15 mK are required. We have produced tungsten thin films with T _c in the range of 25–55 mK by rf-sputtering. To decouple the thermometer production from the choice of the target material and to avoid heating cycles of the absorber crystal, a composite design for detector production is applied. The composite design includes fabrication of the TES on a separate substrate and then attaching of this separate TES to a massive absorber crystal by gluing. For this purpose small sapphire substrates are used for the deposition of the TES. Properties of tungsten thin films grown with the rf-sputtering technique as well as first results of composite detectors built with these films acting as TESs will be presented.      

Detector Development for the Next Phases of the Cryogenic Dark Matter Search: Results from 1 Inch Ge and Si Detectors

The Cryogenic Dark Matter Search (CDMS) experiment is searching for Weakly Interacting Massive Particles (WIMPs) using detectors with the ability to discriminate between candidate (nuclear recoil) and background (electron recoil) events by measuring both phonon and ionization signals from recoils in the detector crystals. As CDMS scales up to greater WIMP sensitivity, it is necessary to increase the detector mass and further improve background discrimination. CDMS is engaged in ongoing fabrication and development of new detector designs in order to meet these criteria for the proposed SuperCDMS experiment. Thicker detector prototypes have been produced with new photolithographic masks. These masks have greater surface coverage of the quasi particle trap and transition edge sensor system to provide superior athermal phonon collection. Results from continuing laboratory tests are presented which already indicate improvement in discrimination parameters.      

Dynamic J-R curves and tension-impact properties of AISI 308 stainless steel weld

In this paper, instrumented tension-impact (dynamic tensile) and instrumented Charpy impact test results for AISI 308 stainless steel welds at room temperature are reported. A few Charpy specimens precracked to a/W (crack length to width ratio) ratios of 0.42 to 0.59 were also tested. Dynamic yield strength obtained from tension-impact test agrees well with that from Charpy V-notch specimens. The strain rates obtained during the tension-impact test are compared with the various estimates of strain rates for V-notch and precracked Charpy specimens. A variation of the compliance changing rate method was necessary for determining the crack initiation point while crack growth was determined by power law key-curve procedure. J-R curves thus obtained from Charpy (precracked and V-notch) specimens are compared with those computed using handbook procedures using dynamic tensile results. Key words: Tension-impact testing, 308 stainless steel weld, Charpy V-notch, dynamic fracture toughness, dynamic yield strength, J-R curve, strain rate, key-curve.