Nanofluid stabilizes and enhances convective boiling heat transfer in a single microchannel

The flow boiling heat transfer in a single microchannel was investigated with pure water and nanofluid as the working fluids. The microchannel had a size of 7500 × 100 × 250 μm, which was formed by two pyrex glasses and a silicon wafer. A platinum film with a length of 3500 μm and a width of 80 μm was deposited at the bottom channel surface, acting as the heater and temperature sensor. The nanofluid had a low weight concentration of 0.2%, consisting of de-ionized water and 40 nm Al₂O₃ nanoparticles. The nanoparticle deposition phenomenon was not observed. The boiling flow displays chaotic behavior due to the random bubble coalescence and breakup in the milliseconds timescale at moderate heat fluxes for pure water. The flow instability with large oscillation amplitudes and long cycle periods was observed with further increases in heat fluxes. The flow patterns are switched between the elongated bubbles and isolated miniature bubbles in the timescale of 100 s. It is found that nanofluid significantly mitigate the flow instability without nanoparticle deposition effect. The boiling flow is always stable or quasi-stable with significantly reduced pressure drop and enhanced heat transfer. Miniature bubbles are the major flow pattern in the microchannel. Elongated bubbles temporarily appear in the milliseconds timescale but isolated miniature bubbles will occupy the channel shortly. The decreased surface tension force acting on the bubble accounts for the smaller bubble size before the bubble departure. The inhibition of the dry patch development by the structural disjoining pressure, and the enlarged percentage of liquid film evaporation heat transfer region with nanoparticles, may account for the heat transfer enhancement compared to pure water.     

Microscale heterogeneous boiling on smooth surfaces—from bubble nucleation to bubble dynamics

In this investigation, boiling incipience and bubble dynamics on a microheater with a geometry of 100 μm × 100 μm fabricated with MEMS technology are evaluated using a high-speed digital camera. For the purpose of comparison with conventional boiling heat transfer, boiling incipience and bubble dynamics are also studied on a carefully selected microheater with a fabricated defect (i.e., a microcavity on the heater surface). Of industrial interest are the effects of dissolved gases on boiling incipience and bubble dynamics, which are also discussed in detail. The possible nucleation temperature (or incipience temperature) is analyzed and discussed from the perspective of the measured bulk temperature of the microheater and a 3D heat conduction numerical model. The time-resolved bubble dynamics (i.e., the bubble size evolution, interface velocity and interface acceleration) are all presented along with high-speed digital images. Based upon this investigation, it is clear that explosive boiling can take place on a smooth surface no matter how slow the heating rate, and dissolved gases have a significant influence on the incipience temperature and bubble behavior. Furthermore, this study illustrates that the classical kinetics of boiling can explain the explosive boiling occurring on a smooth surface in principle and can provide a useful guide for the design of microscale heat transfer and/or MEMS devices. Although unexpected, due to the gravitational effects, Marangoni flow on the vapor–liquid interface induced by the temperature gradient was also observed.     

Dynamic characteristics of transient boiling on a square platinum microheater under millisecond pulsed heating

A series of experimental investigations of boiling incipience and bubble dynamics of water under pulsed heating conditions for various pulse durations ranging from 1 ms to 100 ms were conducted. Using a very smooth square platinum microheater, 100 μm on a side, and a high-speed digital camera, the boiling incipience was observed and investigated as a function of the bulk temperature of the microheater, pulse power level, and pulse duration. Given a specific pulse duration, for low pulse power levels, there would be no bubble nucleation or bubble mergence, for moderate pulse power levels, individual bubbles generated on the heater merged to form a single large bubble, while for high pulse power levels, the rapid growth of the individual bubbles and subsequent bubble interaction, resulted in a reduction in bubble coalescence into a single larger bubble, referred to as bubble splash. The transient heat flux range at which bubble coalescence occurs was identified experimentally, along with the temporal variations of bubble size, bubble interface velocity and interface acceleration.     

Pool boiling characteristics of multiwalled carbon nanotube (CNT) based nanofluids over a flat plate heater

This paper is mainly concerned about the pool boiling heat transfer behavior of multi-walled carbon nanotubes (CNTs) suspension in pure water and water containing 9.0% by weight of sodium lauryl sulphate anionic surfactant (SDS). Three different concentrations of 0.25%, 0.5% and 1.0% by volume of CNT dispersed with water and water containing 9.0% by weight of sodium lauryl sulphate anionic surfactant (SDS) were prepared and boiling experiments were conducted over a stainless steel flat plate heater of size 30 mm² and 0.44 mm thickness. The test results exhibit that the addition of carbon nanotubes increases boiling heat transfer coefficients of the base fluids. At a given heat flux of 500 kW/m², the enhancement of heat transfer coefficient was found to be 1.5, 2.6 and 3.0 times of water corresponding to 0.25%, 0.5% and 1.0% concentration of CNT by volume in water, respectively. In water–CNT–surfactant nanofluid, it was found that 0.5% of CNT concentration gives the highest enhancement of 1.7 compared with water. In both water and water–surfactant base fluids, it was observed that the enhancement factor for 0.25% of CNT first increases up to the heat flux of 66 kW/m² and then decreases for higher heat fluxes. Further, the overall heat transfer coefficient enhancement in the water–CNT nanofluids is approximately two times higher than that in the water–CNT–surfactant nanofluids. With increasing heat flux, however, the enhancement was concealed due to vigorous bubble generation for both water–CNT and water–CNT–surfactant nanofluids. Foaming was also observed over the liquid-free surface in water–CNT–surfactant nanofluids during the investigation. No fouling over the test-section surface was observed after experimentation.     

Holographic interferometric study of heat transfer to a sliding vapor bubble

Heat transfer associated with a vapor bubble sliding along a downward-facing inclined heater surface was studied experimentally using holographic interferometry. Volume growth rate of the bubbles as well as the rate of heat transfer along the bubble interface were measured to understand the mechanisms contributing to the enhancement of heat transfer during sliding motion. The heater surface was made of polished silicon wafer (length 185 mm and width 49.5 mm). Experiments were conducted with PF-5060 as test liquid, for liquid subcoolings ranging from 0.2 to 1.2 °C and wall superheats from 0.2 to 0.8 °C. The heater surface had an inclination of 75° to the vertical. Individual vapor bubbles were generated in an artificial cavity at the lower end of the heater surface. High-speed digital photography was used to measure the bubble growth rate. The temperature field around the sliding bubble was measured using holographic interferometry. Heat transfer at the bubble interface was calculated from the measured temperature field. Results show that for the range of parameters considered the bubbles continued to grow, with bubble growth rates decreasing with increasing liquid subcooling. Heat transfer measurements show that condensation occurs on most of the bubble interface away from the wall. For the parameters considered condensation accounted for less than 12% of the rate heat transfer from the bubble base. In this study the heater surface showed no drop in temperature as a result of heat transfer enhancement during bubbles sliding.     

An experimental study of heater size effect on micro bubble generation

An experimental study of the heater size effect on micro boiling is reported in detail. Using a 1.66-ms-wide heating pulse, boiling in subcooled water was investigated on a series of micron/submicron thin film Pt heaters with various feature sizes ranging from 0.5 μm to 70 μm. It was found that there existed a critical heater size (10 μm): single spherical bubble generation with heater’s feature size less than 10 μm; oblate vapor blanket on the heater surface with the size larger than 10 μm. The bubble dynamics was studied by the visualization of the bubble nucleation process with a high-speed CCD. The onset bubble nucleation temperature was measured by using each Pt heater as a resistive temperature sensor. The formation of the oblate vapor blanket was attributed to the condensation effect of the vapor outside the superheated zone. The analysis was further validated by generating spherical bubble on heater with size larger than 10 μm with a longer heating pulse.     

Pool boiling characteristics of nanofluid on flat plate based on heater surface analysis

Nucleate pool boiling of Al₂O₃ based aqueous nanofluid on flat plate heater has been studied experimentally. For boiling of nanofluid (< 0.1 vol.%) on heating surface with ratio of average surface roughness to average diameter of particles much less than unity when boiling continue to CHF, the heat transfer coefficient of nanofluid boiling reduces while critical heat flux (CHF) increases. CHF enhancement increased with volume fraction of nanoparticles. Atomic force microscope (AFM) images from boiling surface showed that after boiling of nanofluid the surface roughness increases or decreases depending on initial condition of heater surface. Changes in boiling surface topology during different regions of boiling, wettability and thermal resistance of heater surface owing to nanoparticles deposition cause to variations in nanofluids boiling performance.     

Experimental investigation of the effect of particle deposition on pool boiling of nanofluids

Research on pool boiling of nanofluids has shown contradicting trends in the heat transfer coefficient (HTC). Such trends have been attributed, in part, to nanoparticle deposition on the heater surface. An experimental investigation of the transient nature of nanoparticle deposition and its effect on the HTC of pool boiling of nanofluids at various concentrations has been carried out. Pool boiling experiments have been conducted on a horizontal flat copper surface for alumina (40–50 nm) water based nanofluids at concentrations of 0.01, 0.1 and 0.5 vol.%. Nanofluids boiling experiments have been followed by pure water boiling experiments on the same nanoparticle-deposited (NPD) surfaces. This technique has been employed in order to separate the effect of nanoparticle deposition from the effect of nanofluids properties on the HTC. Contrary to what was expected, boiling of pure water on the NPD surface produced using the highest concentration nanofluid resulted in the highest HTC. A closer look at the nature of the NPD surfaces explained such trend. A new approach using a transient surface factor in Rohsenow correlation has been proposed to account for the transient nature of nanoparticle deposition. The applicability of such approach at different concentrations has been investigated.     

Effects of electric field on microbubble growth in a microchannel under pulse heating

Effects of imposed DC electric fields on microbubble growth generated from a rectangular Pt micro-heater (140 × 100 μm) fabricated on one wall of the microchannel under pulse heating are investigated experimentally in this paper. Bubble dynamics and surface temperature response of the microheater during pulse heating are observed and recorded using a high speed CCD and data acquisition system. Measurements of nucleation time and nucleation temperature and heat flux at boiling inception are taken at a fixed flow rate of 0.6 ml/min and pulse width of 1 ms, and with the electric field strength gradually increasing from zero. With increasing electric field strength, it is found that heat flux required for boiling inception is increased, boiling nucleation time is delayed, and nucleation temperature is reduced. Bubble growth is suppressed by the inward dielectrophoresis force acting at the vapor/water interface which is induced by the electric field. As a result, the diameter of the bubble becomes smaller, and the interface instability is suppressed during the bubble growth period. In addition, it is found that multiple nucleate sites appear on the surface of the micro-heater at high heat flux when the electric field is increased to a sufficiently high strength. A map showing regimes of single and multi nucleate sites in a plot of heat flux versus electric field strength is obtained.     

Subcooled boiling incipience on a highly smooth microheater

Subcooled boiling incipience on a highly smooth microscale heater (270 μm × 270 μm) submerged in FC-72 liquid is investigated. Using high-speed imaging and a transient heat flux measurement technique, the mechanics of homogeneous nucleation on the heater are elucidated. Bubble incipience on the microheater was observed to be an explosive process. It is found that the superheat limit of boiling liquid is required for bubble incipience. It is concluded that boiling incipience on the microheater is a homogeneous liquid–vapor phase change process. This is in contrast to recent observations of low-superheat heterogeneous nucleation on metallic surfaces of rms roughness ranging from 4 to 28 nm [T.G. Theofanous, J.P. Tu, A.T. Dinh, T.N. Dinh, The boiling crisis phenomenon part I: nucleation and nucleate boiling heat transfer, Exp. Therm. Fluid Sci. 26 (2002) 775–792; Y. Qi, J.F. Klausner, Comparison of gas nucleation and pool boiling site densities, J. Heat Transfer 128 (2005) 13–20; Y. Qi, J.F. Klausner, Heterogeneous nucleation with artificial cavities, J. Heat Transfer 127 (2005) 1189–1196]. Following the explosive bubble incipience, the boiling process on the microheater can be maintained at much lower superheats. This is mainly due to the necking during bubble departure that leaves an embryo from which the next-generation bubbles grow.     

Subcooled flow boiling and microbubble emission boiling phenomena in a partially heated microchannel

A simultaneous visualization and measurement study has been carried out to investigate subcooled flow boiling and microbubble emission boiling (MEB) phenomena of deionized water in a partially heated Pyrex glass microchannel, having a hydraulic diameter of 155 μm, which was integrated with a Platinum microheater. Effects of mass flux, inlet water subcooling and surface condition of the microheater on subcooled flow boiling in microchannels are investigated. It is found that MEB occurred at high inlet subcoolings and at high heat fluxes, where vapor bubbles collapsed into microbubbles after contacting with the surrounding highly subcooled liquid. In the fully-developed MEB regime where the entire microheater was covered by MEB, the mass flux, the inlet water subcooling and the heater surface condition have only small effects on the boiling curves. The occurrence of MEB in microchannel can remove a large amount of heat flux, as high as 14.41 MW/m² at a mass flux of 883.8 kg/m² s, with only a moderate rise in wall temperature. Therefore, MEB is a very promising method for cooling of microelectronic chips. Heat transfer in the fully-developed MEB in the microchannel is presented, which is compared with existing subcooled flow boiling heat transfer correlations for macrochannels.     

Effect of pulse heating parameters on the microscale bubble dynamics at a microheater surface

We study the effects of pulse heating parameters on the micro bubble behavior of a platinum microheater (100 μm×20 μm) immersed in a methanol pool. The experiment covers the heat fluxes of 10–37 MW/m² and pulse frequencies of 25–500 Hz. The boiling incipience is initiated at the superheat limit of methanol, corresponding to the homogeneous nucleation. Three types of micro boiling patterns are identified. The first type is named as the bubble explosion and regrowth, consisting of a violent explosive boiling and shrinking, followed by a slower bubble regrowth and subsequent shrinking, occurring at lower heat fluxes. The second type, named as the bubble breakup and attraction, consists of the violent explosive boiling, bubble breakup and emission, bubble attraction and coalescence process, occurring at higher heat fluxes than those of the first type. The third type, named as the bubble size oscillation and large bubble formation, involves the initial explosive boiling, followed by a short periodic bubble growth and shrinking. Then the bubble continues to increase its size, until a constant bubble size is reached which is larger than the microheater length.     

Pool boiling characteristics of low concentration nanofluids

The pool boiling behavior of low concentration nanofluids (?1 g/l) was experimentally studied over a flat heater at 1 atm. Boiling of nanofluids produces a thin nanoparticle film, on the heater surface, which in turn is believed to increase the critical heat flux. The present study also indicates that the nanoparticle deposition results in transient characteristics in the nucleate boiling heat transfer. Finally, this study investigates possible causes responsible for the deposition of nanoparticle on the heater surface. Experimental evidence shows that microlayer evaporation, during nanofluid boiling, is responsible for the nanoparticle coating formed on the heater surfaces.     

Behavioral study of alumina nanoparticles in pool boiling heat transfer on a vertical surface

Experiments were carried out to investigate the pool boiling of alumina‐water nanofluid at 0.1 g/l to 0.5 g/l of distilled water, and the nucleate pool boiling heat transfer of pure water and nanofluid at different mass concentrations were compared at and above the atmospheric pressure. At atmospheric pressure, different concentrations of nanofluids display different degrees of deterioration in boiling heat transfer. The effect of pressure and concentration of nanoparticles revealed significant enhancement in heat flux and deterioration in pool boiling. The heat transfer coefficient of 0.5 g/l alumina‐water nanofluid was compared with pure water and clearly indicates deterioration. At all pressures the heat transfer coefficients of the nanofluid were lower than those of pure water. Experimental observation revealed particles coating over the heater surface and subsequent SEM inspection of the heater surface showed nanoparticles coating on the surface forming a porous layer. To substantiate the nanoparticle deposition and its effect on heat flux, investigation was done by measuring the surface roughness of the heater surface before and after the experiment. While SEM images of the heater surface revealed nanoparticle deposition, surface roughness of the heater surface confirmed it. Based on the experimental investigations it can be concluded that an optimum thickness of nanoparticles coating favors an increase in heat flux. Higher surface temperature due to the presence of nanoparticles coating results in the deterioration of boiling heat transfer. © 2011 Wiley Periodicals, Inc. Heat Trans Asian Res; Published online in Wiley Online Library ( wileyonlinelibrary.com/journal/htj ). DOI 10.1002/htj.20365     

An experimental investigation on the effects of surfactants on the thermal performance of hybrid nanofluids in helical coil heat exchangers

In the present study, the effects of surfactants on the thermal performance of the hybrid nanofluid (Alumina–Silver) at constant wall temperature and laminar flow have been experimentally studied in a helical coil heat exchanger. Different surfactants such as anionic Sodium Dodecyl Sulfate (SDS) and nonionic Poly Vinyl Pyrrolidone (PVP) in the concentration of range of 0.1–0.4 wt.% are employed. It is found that the thermal performance can be maximized by using the 0.2 vol.% hybrid nanofluid and 0.1 wt.% SDS anionic surfactant in the helical coil. The maximum thermal performance in the presence of hybrid Alumina–Silver nanofluid and SDS anionic surfactant is 16% higher than that of the pure distilled water. The presented results can have potential application in process intensification and optimum design of heat exchangers.     

Effect of nanofluids on reflood heat transfer in a long vertical tube

Experiments were conducted to investigate the effect of nanofluids on reflood heat transfer in a hot vertical tube. The nanofluids, which are produced by dispersing nano-sized particles in traditional base fluids such as water, ethylene glycol, and engine oil, are expected to have a reasonable potential to enhance a heat transfer. 0.1 volume fraction (%) Al₂O₃/water nanofluid was prepared by two-step method and 0.1 volume fraction (%) carbon nano colloid (CNC) was prepared by the process self-dispersing by carboxyl formed particle surface. Transmission electron microscopy (TEM) images are acquired to characterize the shape and size of Al₂O₃ and graphite nanoparticles. The dispersion behavior of nanofluids was investigated with zeta potential values. And then, the reflood tests have been performed using water and nanofluids. We have observed a more enhanced cooling performance in the case of the nanofluid reflood. Consequently, the cooling performance is enhanced more than 13 s and 20 s for Al₂O₃/water nanofluid and CNC.     

An experimental study on the heat transfer performance and pressure drop of TiO2-water nanofluids flowing under a turbulent flow regime

Nanofluid is a new class of heat transfer fluids engineered by dispersing metallic or non-metallic nanoparticles with a typical size of less than 100 nm in the conventional heat transfer fluids. Their use remarkably augments the heat transfer potential of the base liquids. This article presents the heat transfer coefficient and friction factor of the TiO₂-water nanofluids flowing in a horizontal double tube counter-flow heat exchanger under turbulent flow conditions, experimentally. TiO₂ nanoparticles with diameters of 21 nm dispersed in water with volume concentrations of 0.2–2 vol.% are used as the test fluid. The results show that the heat transfer coefficient of nanofluid is higher than that of the base liquid and increased with increasing the Reynolds number and particle concentrations. The heat transfer coefficient of nanofluids was approximately 26% greater than that of pure vol.%, and the results also show that the heat transfer coefficient of the nanofluids at a volume concentration of 2.0 vol.% was approximately 14% lower than that of base fluids for given conditions. For the pressure drop, the results show that the pressure drop of nanofluids was slightly higher than the base fluid and increases with increasing the volume concentrations. Finally, the new correlations were proposed for predicting the Nusselt number and friction factor of the nanofluids, especially.     

Heat transfer and entropy generation for laminar forced convection flow of graphene nanoplatelets nanofluids in a horizontal tube

The results are reported of an investigation of the heat transfer characteristics and entropy generation for a graphene nanoplatelets (GNP) nanofluid with specific surface area of 750 m²/g under laminar forced convection conditions inside a circular stainless steel tube subjected to constant wall heat flux. The analysis considers constant velocity flow and a concentration range from 0.025 wt.% to 0.1 wt.%. The impact of the dispersed nanoparticles concentration on thermal properties, convective heat transfer coefficient, thermal performance factor and entropy generation is investigated. An enhancement in thermal conductivity for GNP of between 12% and 28% is observed relative to the case without nanoparticles. The convective heat transfer coefficient for the GNP nanofluid is found to be up to 15% higher than for the base fluid. The heat transfer rate and thermal performance for 0.1 wt.% of GNP nanofluid is found to increase by a factor of up to 1.15. For constant velocity flow, frictional entropy generation increases and thermal entropy generation decreases with increasing nanoparticle concentration. But, the total entropy generation tends to decrease when nanoparticles are added at constant velocity and to decrease when velocity rises. Finally, it is demonstrated that a GNP nanofluid with a concentration between 0.075 wt.% and 0.1 wt.% is more energy efficient than for other concentrations. It appears that GNP nanofluids can function as working fluids in heat transfer applications and provide good alternatives to conventional working fluids in the thermal fluid systems.     

Laminar convective heat transfer and viscous pressure loss of alumina–water and zirconia–water nanofluids

Laminar convective heat transfer and viscous pressure loss were investigated for alumina–water and zirconia–water nanofluids in a flow loop with a vertical heated tube. The heat transfer coefficients in the entrance region and in the fully developed region are found to increase by 17% and 27%, respectively, for alumina–water nanofluid at 6 vol % with respect to pure water. The zirconia–water nanofluid heat transfer coefficient increases by approximately 2% in the entrance region and 3% in the fully developed region at 1.32 vol %. The measured pressure loss for the nanofluids is in general much higher than for pure water. However, both the measured nanofluid heat transfer coefficient and pressure loss are in good agreement with the traditional model predictions for laminar flow, provided that the loading- and temperature-dependent thermophysical properties of the nanofluids are utilized in the evaluation of the dimensionless numbers. In other words, no abnormal heat transfer enhancement or pressure loss was observed within measurement errors.