Compressive response and failure of fiber reinforced unidirectional composites

The compressive response of polymer matrix fiber reinforced unidirectional composites (PMC's) is investigated via a combination of experiment and analysis. The study accounts for the nonlinear constitutive response of the polymer matrix material and examines the effect of fiber geometric imperfections, fiber mechanical properties and fiber volume fraction on the measured compressive strength and compressive failure mechanism.Glass and carbon fiber reinforced unidirectional composite specimens are manufactured in-house with fiber volume fractions ranging over 1060 percent. Compression test results with these specimens show that carbon fiber composites have lower compressive strengths than glass fiber composites. Glass fiber composites demonstrate a splitting failure mode for a range of low fiber volume fractions and a simultaneous splitting/kink banding failure mode for high fiber volume fractions. Carbon fiber composites show kink banding throughout the range of fiber volume fractions examined. Nonlinear material properties of the matrix, orthotropic material properties of the carbon fiber, initial geometric fiber imperfections and nonuniform fiber volume fraction are all included in an appropriate finite element analysis to explain some of the observed experimental results. A new analytical model predictionof the splitting failure mode shows that this failure mode is favorable for glass fiber composites, which is in agreement with test results. Furthermore, this modelis able to show the influence of fiber mechanical properties, fiber volume fraction and fiber geometry on the splitting failure mode.     

Fatigue-life distributions and failure probability for glass-fiber reinforced polymeric composites

There has been an upsurge in the application of composite materials in the last few decades, due to high demands on material performance placed by advanced technologies. Most of these applications include the situations where degradation of strength and life by fatigue process is most likely. In this investigation, rotating bending fatigue tests have been conducted on two types of unidirectional glass-fiber reinforced polymeric composites, having vinylester and Epoxy as matrix materials. It has been observed that the probabilistic distribution of fatigue-life of these glass-fiber reinforced composites, at a particular stress level, can be modeled by two-parameter Weibull distribution, with statistical co-relation coefficient values exceeding 0.90. Various methods have been used to obtain the parameters of Weibull distribution. Kolmogorov–Smirnov goodness-of-fit test has also been used to reinforce the above findings. The two-parameter Weibull distribution has also been employed to incorporate failure probability into S–N relationships.     

Compressive behaviour of unidirectional flax fibre reinforced composites

The compressive strength of unidirectional flax fibre epoxy composites was studied. The compressive strength is influenced negatively by the presence of kink bands in the flax fibres. Improvement of the adhesion between the fibres and the epoxy resin can be achieved easily by removing the thin wax layer which covers the surface of the flax fibres. However, improving the adhesion between fibres and matrix only improves the compressive strength to a very limited extent. Stabilisation of the kink bands present in the fibres and improvement of the compressive properties of the fibres can be achieved by impregnating the fibres with melamine formaldehyde (MF) resin. This results in a large increase in the compressive strength of the resulting composite. The increase in compressive strength is proportional to the amount of MF resin present in the composite. However, the presence of the resin in the fibres lowers their tensile strength, and subsequently the tensile strength of the resulting composite.     

Mode I delamination fatigue crack growth in unidirectional fiber reinforced composites: Development of a standardized test procedure

Selected mode I fatigue data from five different types of fiber-reinforced, polymer–matrix composites tested in two round robins organized by the American Society for Testing and Materials subcommittee D30.06 and European Structural Integrity Society Technical Committee 4, respectively, are analyzed and discussed. The focus is on experimental scatter (in-laboratory and inter-laboratory) and on schemes for quantitative data analysis. It is shown that in spite of considerable scatter different composites can be distinguished and, under certain assumptions, a relative ranking be established. Further, effects from limited experimental measurement resolution are noted and implications for the test procedure and use of the test data in design of composite structures discussed. For comparative purposes, a rough ranking of different composites is feasible with test data generated within 24 h per specimen in an industrial test environment.     

Compressive failure of hybrid multidirectional fibre-reinforced composites

In this paper, the hybridisation of multidirectional carbon fibre-reinforced composites as a means of improving the compressive performance is studied. The aim is to thoroughly investigate how hybridisation influences the laminate behaviour under different compression conditions and thus provide an explanation of the “hybrid effect”. The chosen approach was to compare the compressive performance of two monolithic carbon fibre/epoxy systems, CYTEC HTS/MTM44-1 and IMS/MTM44-1, with that of their respective hybrids. This was done by keeping the same layup throughout ((0/90/45/−45)_2S) while replacing the angle plies in one case or the orthogonal plies in the other case with the second material, thus producing two hybrid systems. To investigate the compressive performance of these configurations, compact and plain compression test methods were employed which also allowed studying the sensitivity of compressive failure to specimen geometry and loading conditions. The experimental results and the subsequent fractographic analysis revealed that the hybridisation of selective ply interfaces influenced the location and severity of the failure mechanisms. Finally, in light of this knowledge, an update of the generic sequence of events, previously suggested by the authors, which lead to global fracture in multidirectional fibre-reinforced composites under compression is presented.     

A novel processing technique for thermoplastic manufacturing of unidirectional composites reinforced with jute yarns

This paper primarily investigates the fabrication process of long-fibre reinforced unidirectional thermoplastic composites made using jute yarns (both untreated and treated). Tubular braiding technique was used to produce an intermediate material called “microbraid yarn” (MBY) with jute yarn as the straightly inserted axial reinforcement fibre and polymer matrix fibre being braided around the reinforcing jute yarns. Microbraid yarns were then wound in a parallel configuration onto a metallic frame and compression molded to fabricate unidirectional composite specimens. In this study, two types of polymeric materials (biodegradable poly(lactic) acid and non-biodegradable homo-polypropylene) were used as matrix fibres. Basic static mechanical properties were evaluated from tensile and 3 point bending tests. Test results were analyzed to investigate the effects of molding temperature and pressure on the mechanical and interfacial behaviour. For the unidirectional jute fibre/poly(lactic) acid (PLA) composites, the results indicated that the molding condition at 175 °C and 2.7 MPa pressure was more suitable to obtain optimized properties. Improved wettability due to proper matrix fusion facilitated thorough impregnation, which contributed positively to the fibre/matrix interfacial interactions leading to effective stress transfer from matrix to fibre and improved reinforcing effects of jute yarns. For the jute/PP unidirectional composites, specimens with only 20% of jute fibre content have shown remarkable improvement in tensile and bending properties when compared to those of the virgin PP specimens. The improvements in the mechanical properties are broadly related to various factors, such as the wettability of resin melts into fibre bundles, interfacial adhesion, orientation and uniform distribution of matrix-fibres and the lack of fibre attrition and attenuation during tubular braiding process.     

Effects of interphase material properties in unidirectional fibre reinforced composites

A three-dimensional (3D) micromechanical study has been performed in order to investigate local damage in unidirectional (UD) composite materials with epoxy resin under transverse tensile loading. In particular the effect of different mechanical properties of a 3D interphase within the hexagonal array RVE have been considered and effects of thermal residual stress arising during the curing process have been accounted for in this study. To examine the effect of interphase properties and residual stress on failure, a study based on the temperature-dependent properties of matrix and interphase and a stiffness degradation technique has been used for damage analysis of the unit cell subjected to mechanical loading. Results indicate a strong dependence of damage onset and its evolution from the different interphase properties within the RVE (representative volume element). Moreover, predicted mechanical properties, damage initiation and evolution are also clearly influenced by the presence of residual stress. Numerical results and experimental data (in the literature) have also shown an interesting agreement.     

Compressive splitting failure of composites using modified shear lag theory

The shear lag model has been used in conjunction with the 3D elasticity equations to determine the stress state in a fiber/matrix system containing an interface crack. The use of a shear lag model to capture the stress state at the crack tip and the modelling of the region away from the crack tip by the elasticity equations leads to a simple analytical expression which can be used to determine the compliance changes for both unsteady crack growth as well as steady state crack propagation under compressive loading. Certain modifications to the assumptions used in the classical shear lag model have been made to increase the accuracy of the predictions for the rate of change of compliance with respect to crack length, dc/dl. The present approach leads to closed form expressions for the compressive strength of unidirectional fiber reinforced composites.     

Fracture characterisation of short bamboo fibre reinforced polyester composites

In the study, fracture behaviour of short bamboo fibre reinforced polyester composites is investigated. The matrix is reinforced with fibres ranging from 10 to 50, 30 to 50 and 30 to 60 vol.% at increments of 10 vol.% for bamboo fibres at 4, 7 and 10 mm lengths respectively. The results reveal that at 4 mm of fibre length, the increment in fibre content deteriorates the fracture toughness. As for 7 and 10 mm fibre lengths, positive effect of fibre reinforcement is observed. The optimum fibre content is found to be at 40 vol.% for 7 mm fibre and 50 vol.% for 10 mm fibre. The highest fracture toughness is achieved at 10 mm/50 vol.% fibre reinforced composite, with 340% of improvement compared to neat polyester. Fractured surfaces investigated through the Scanning Electron Microscopy (SEM) describing different failure mechanisms are also reported.     

Surface and sub-surface degradation of unidirectional carbon fiber reinforced epoxy composites under dry and wet reciprocating sliding

The role of water on the sub-surface degradation of unidirectional carbon fiber reinforced epoxy composite is examined. The correlation between the debonding of carbon fibers at the fiber–epoxy interface, and the wear behavior of the carbon fiber composite are discussed based on an in-depth analysis of the worn surfaces. We demonstrate that a reciprocating sliding performed along an anti-parallel direction to the fiber orientation under dry conditions results in a large degradation by debonding and breaking of the carbon fibers compared to sliding in parallel and perpendicular directions. Immersion in water has a harmful effect on the wear resistance of the carbon fiber composite. The competition between crack growth and the wear rate of epoxy matrix and/or carbon fibers in the sliding track determines the level of material loss of the composite in both test environments.     

Local stress concentration and the prediction of tensile failure in unidirectional composites

The aim of this paper is to present a new representation of the tensile failure of a composite material which accounts for the normal stress supported by the matrix and allows a study of the influence of constituent material properties and fibre volume fraction on the stress-concentration factors. This is done by micromechanical analysis which allows the stress and strain in the fibres and the matrix to be related to the applied stress or strain on the composite. Stress-concentration factors are calculated in the composite transverse section and are found to be smaller than previously published analytical solutions. The difference is essentially due to the normal stress supported by the matrix which is neglected by the shear-lag analysis but is taken into account in our model. The tensile strength is calculated firstly by numerical simulations and secondly by Batdorf's methodology which addresses the formation and propagation of fibre fractures. Comparisons with experimental measures are satisfactory.     

Micromechanical modeling of damage and fracture of unidirectional fiber reinforced composites: A review

An overview of methods of the mathematical modeling of deformation, damage and fracture in fiber reinforced composites is presented. The models are classified into five main groups: shear lag-based, analytical models, fiber bundle model and its generalizations, fracture mechanics based and continuum damage mechanics based models and numerical continuum mechanical models. Advantages, limitations and perspectives of different approaches to the simulation of deformation, damage and fracture of fiber reinforced composites are analyzed.     

Moisture absorption of unidirectional hybrid composites

Unidirectional hybrid composite rods were conditioned in humid air to investigate the sorption kinetics and the effects of moisture on mechanical and physical properties. Sorption curves were obtained for both hybrid and non-hybrid composite rods to determine characteristic parameters, including the diffusion coefficient (D) and the maximum moisture uptake (M_∞). The moisture uptake for the hybrid composites generally exhibited Fickian behavior (no hybridization effects), behaving much like non-hybrid composites. A two-dimensional diffusion model was employed to calculate moisture diffusivities in the longitudinal direction. Interfaces and thermally-induced residual stresses affected the moisture diffusion. In addition, the effect of hygrothermal aging on glass transition temperature (T_g), short beam shear strength (SBS), and tensile strength was determined for hygrothermal exposure at 60 °C and 85% relative humidity (RH). Property retention and reversibility of property degradation were also measured. Microscopic inspection revealed no evidence of damage.     

Nonlinear response in glass fibre non-crimp fabric reinforced vinylester composites

This paper addresses the nonlinear stress-strain response in glass fibre non-crimp fabric reinforced vinylester composite laminates subjected to in-plane tensile loading. The nonlinearity is shown to be a combination of brittle and plastic failure. It is argued that the shift from plastic to brittle behaviour in the vinylester is caused by the state of stress triaxiality caused by the interaction between fibre and vinylester. A model combining damage and plasticity is calibrated and evaluated using data from extensive experimental testing. The onset of damage is predicted using the Puck failure criterion, and the evolution of damage is calibrated from the observed softening in plies loaded in transverse tension. Shear loading beyond linear elastic response is observed to result in irreversible strains. A yield criterion is implemented for shear deformation. A strain hardening law is fitted to the stress-strain response observed in shear loaded plies. Experimental results from a selection of laminates with different layups are used to verify the numerical models. A complete set of model parameters for predicting elastic behaviour, strength and post failure softening is presented for glass fibre non-crimped fabric reinforced vinylester. The predicted behaviour from using these model parameters are shown to be in good agreement with experimental results.     

Effect of basalt fibre hybridisation on post-impact mechanical behaviour of hemp fibre reinforced composites

A major limitation to the spreading of natural fibre reinforced composites in semi-structural components is their unsatisfactory impact performance. As a potential solution, the production of synthetic/plant fibre hybrid laminates has been explored, trying to obtain materials with sufficient impact properties, while retaining a reduced cost and a substantial environmental gain. This study explores the effects of hybridisation of basalt fibre on post-impact behaviour and damage tolerance capability of hemp fibre reinforced composites. All reinforced laminates were impacted in a range of energies (3, 6, and 9 J) and subjected to both quasi-static and cyclic flexural tests with a step loading procedure. The tests have also been monitored by acoustic emission (AE), which has confirmed the existence of severe limitations to the use of natural fibre reinforced composites even when impacted at energies not so close to penetration and the enhanced damage tolerance offered by the hybridisation with basalt fibers.     

Nonlinear transient analysis of reinforced concrete slabs subjected to blast loading and retrofitted with CFRP composites

Computational models using the finite element method for nonlinear transient analysis of reinforced concrete (RC) two-way slabs subjected to blast loading are presented. Both as-built and retrofitted slabs with carbon fiber reinforced polymer (CFRP) composite strips are analyzed. The models are used to investigate different parameters including (a) loading duration, and (b) effect of CFRP retrofit on damage accumulation. In this study, damage is globally quantified by the amount of reduction of the first two vibrational frequencies of the slabs. Local representation of damage in terms of reinforcing steel strains is also discussed. The computational models for both the as-built and the retrofitted slabs are verified using experimental results. In these experiments, a slowly increasing uniform pressure is applied to the bottom surface of large-scale RC slab specimens using high-pressure water bag. Experimental results showed that an increase up to 200% in the load carrying capacity is achieved when using the CFRP composite retrofit system. Transient nonlinear analysis results proved the efficiency of the CFRP composite retrofit in improving the slab behavior under blast loading for different loading durations, i.e. for small, medium, and large charge weights at the same applied maximum pressure. In particular, less than 50% reduction of the fundamental frequency due to concrete damage is obtained for the retrofitted slab compared to more than 85% reduction for the as-built slab. Moreover, the maximum displacement is reduced by 40–70% with the CFRP retrofit compared to the as-built slab. As for reinforcing steel strains, the application of CFRP retrofit significantly limited the spread of yielding in time and space. The improved slab behavior with CFRP is best when retrofitting is applied to both sides of the slab.     

An analytical method for predicting cutting forces in orthogonal machining of unidirectional composites

Since the chip-formation mechanism in orthogonal machining of composites is different from that of metals, the cutting theories developed for metals cannot be directly used for orthogonal machining of composites. The objective of this research was to develop a new analytical method using energy method to predict the machining forces for orthogonal machining of unidirectional polymer–matrix composites (PMCs) for fiber orientations ranging from 90° to 180° Experiments were conducted to verify the validity of the proposed model using tools with rake angles of 5°, 10°, 15°, and 20°.     

Synchronous effects of multiscale reinforced and toughened CFRP composites by MWNTs-EP/PSF hybrid nanofibers with preferred orientation

MWNTs-EP/PSF (polysulfone) hybrid nanofibers with preferred orientation were directly electrospun onto carbon fiber/epoxy prepregs and interlaminar synchronously reinforced and toughened CFRP composites were successfully fabricated. With MWNTs-EP loading increasing, the oriented nanofibers were obtained accompanying with enhanced alignment of inner MWNTs-EP. Flexural properties and interlaminar shear strength of composites were improved with increasing MWNTs-EP loadings, whereas fracture toughness attained maximum at 10 wt% MWNTs-EP loading and then decreased. Based on these results, multiscale schematic modeling and mechanism schematic of hybrid nanofibers reinforced and toughened composites were suggested. Due to the preferred orientation of nanofibers, MWNTs-EP was inclined to align vertically to carbon fiber direction along the in-plane of interface layer. The proposed network structures, containing four correlative phases of MWNTs-EP/PSF sphere/carbon fiber/epoxy matrix, contributed to simultaneous improvement of strength and toughness of composites, which was realized by crack pinning, crack deflection, crack bridging and effective load transfer.     

Surface damage of unidirectional carbon fiber reinforced epoxy composites under reciprocating sliding in ambient air

For many technical applications friction and wear are critical issues. Reinforced polymer-matrix composites are widely used under vibrating contact condition in various automotive and aerospace applications as well as in structural engineering. In this paper, the friction and wear of bulk epoxy and unidirectional carbon fiber reinforced epoxy composite have been investigated under reciprocating sliding against either alumina or stainless steel balls in ambient air. The effect of sliding direction with respect to the long and unidirectional carbon fibers has been studied. We demonstrate that the carbon fiber reinforcement greatly improves the tribological properties of the thermoset epoxy: it reduces the coefficient of friction and the debris formation. It was found that on sliding in the anti-parallel direction a more significant degradation takes place than in the parallel direction. The coefficient of friction measured on bulk epoxy sliding against either stainless steel or alumina is around 0.65, whereas the coefficient of friction measured on epoxy reinforced with carbon fibers is significantly lower, namely down to 0.11. It was found that sliding with a stainless steel ball in a direction parallel to the fiber orientation results in a lower coefficient of friction than sliding in anti-parallel direction. The reduced coefficient of friction is largely influenced by the carbon fiber reinforcement due to the auto-protecting film formed as a paste in the contact area and along the wear track edges. The relationship between friction and degradation of the composite material including surface wear and debris formation are discussed based on an in-depth analysis of the worn surfaces by optical and scanning electron microscopy, micro-Raman spectroscopy, and white light interferometry.     

Compressive failure of finite size unidirectional composite laminates with a region of fibre waviness

The compressive behaviour of finite unidirectional composites with a region of misaligned reinforcement is investigated via finite element analyses. Models with and without fibre bending stiffness are compared, confirming that compressive strength is accurately predicted without modelling fibre bending stiffness for real composite components which typically have waviness defects of several millimetres wavelength. Various defect parameters are investigated. Results confirm the well-known sensitivity of compressive strength to misalignment angle, and also show that compressive strength falls rapidly with the proportion of laminate width covered by the wavy region. A simple empirical equation is proposed to model the effect of a single patch of waviness in finite specimens. Other parameters such as length and position of the wavy region are found to have a smaller effect on compressive strength. The modelling approach is finally adapted to model distributed waviness and thus determine the compressive strength of composites with realistic waviness defects.