气液固三相循环流化床中气固相含率轴径向的分布

对气液固三相循环流化床中气固相含率沿轴径向的分布进行了实验研究和模拟。实验结果表明：与膨胀床相比，三相循环流化床内的相间接触较为充分；固含率轴向分布的一维沉降－扩散模型模拟值与实验值吻合较好。     

提升管三相流化床内的气液传质系数

采用溶氧电极法测定了以牛顿和非牛顿流体为液相的提升管三相流化床的气液传质系数（ｋｌａ）。证明其值受床层流动特性的影响显著，那些能提供高气含率和增大液体循环速率的操作条件也有助于ｋｌａ的提高。通过引入广义雷诺数得出了计算牛顿和非牛顿流体内ｋｌａ的关联式     

气液固三相流化床反应器测试技术

在简述已有三相流化床测试技术的基础上,着重对近年来开发的测试新技术的基本原理及优缺点进行了分析,包括光纤探头技术、超声探头技术、放射颗粒跟踪技术、X射线颗粒跟踪测试技术、颗粒图像测速技术、电容层析成像技术、激光多普勒测速技术和相多普勒测速技术等,同时,展望了三相流化床测试技术的新方向.     

提升管三相流化床内流动特性研究

在以牛顿和非牛顿流体为液相的提升管三相流化床内研究了粒子循环条件、床层气含率和液体循环速率等变化规律.考察了中心管和环隙气含率的差别及其对液相循环的影响,并引入广义雷诺数,得出计算气含率的关联式.     

气液固三相循环流态化

<正>由于三相流化床反应器在石油化工、湿法冶金、环境工程和煤的液化等工业领域得到越来越广泛的应用,近年来对传统的三相流化床进行了大量的基础研究并取得了很大进展。以往的研究大部分是针对低液速(u_l相似文献   

汽液固三相流化床沸腾传热的研究

对垂直管内汽液固三相流化床沸腾传热特性进行了实验研究和理论分析,建立了沸腾传热的计算方法.实验结果表明,由于固体粒子的存在,强化了沸腾传热.传热系数比汽液两相流提高2倍左右.沸腾过程的稳定性明显提高.     

气液固三相循环流化床气液传质行为

<正>气液固三相流化床反应器在石油化工、湿法冶金、环境工程和煤的液化等工业领域得到了广泛应用,其基础研究也取得了很大进展.但是,传统三相床主要应用于低液速(U_L<     

气—液—固三相磁性流化床混沌特性研究

运用确定性混沌分析技术,研究了气－液＝固三相磁性流化床系统压力波动时间序列的混沌特性。在给定表观气、液速下,非一特征参数如最大李雅谱诺夫指数和Ｋ熵都大于零,并且随磁场强度的增加而减小,表明该系统具有混沌行为：磁场作用使气－液－因三相流动更趋有序。研究还表明,气－液－固三相磁性流化床的三个流区（散流区、链流区及磁聚区）变化可由混沌特征参数值的变化来体现。     

气液固三相分离器的优化设计

将三相分离器的设计与ＵＡＳＢ反应器的工艺条件相结合,建立了一种改进结构的三相分离器的设计模型,可以求得分离器的最佳结构尺寸,为反应器在高负荷一稳定运行提供了依据。     

气液及气液固三相浆态鼓泡塔的气相轴向返混系数

气液及气液固三相浆态鼓泡塔的气相轴向返混系数宋同贵，赵玉龙，苏晓丽，张碧江（中国科学院山西煤炭化学研究所，煤转化国家重点实验室，太原０３０００１）关键词：气液鼓泡塔，浆态鼓泡塔，气相轴向返混１前言在鼓泡塔反应器的设计、放大及数学模拟中，气相轴向返混系...     

RADIAL DISPERSION AND BUBBLE CHARACTERISTICS IN THREE-PHASE FLUIDIZED BEDS

The effects of gas and liquid velocities, liquid viscosity and particle size on the radial dispersion coefficient of liquid phase (D_r) and the bubble properties in three-phase fluidized beds have been determined. A new flow regime map based on the drift flux theory in three-phase fluidized beds has been proposed.

In three-phase fluidized beds, D, increases with increasing gas velocity in the bubble coalescing and in the slug flow regimes, but it decreases in the bubble disintegrating regime. The coefficient exhibits a maximum value in the bed of small particles with increasing liquid velocity at lower gas velocities. However, it increases with increasing liquid velocity at higher gas velocities. In two and three-phase fluidized beds of larger particles (6,8 mm), D_r exhibits a maximum value with an increase in liquid viscosity at lower gas velocities, but it increases at higher gas velocities. The mean bubble chord length and its rising velocity increase with increasing gas velocity and liquid viscosity. However, the bubble chord length decreases with an increase in liquid velocity and it exhibits a maximum value with increasing particle size in the bed. The radial dispersion coefficients in the bubble coalescing and disintegrating regimes of three-phase fluidized beds in terms of the Peclet number in the present and previous studies have been well represented by the correlations based on the concept of isotropic turbulence theory.     

三相外环流反应器的液相返混特性和气液传质特性

主要研究了气速与固相对三相外环流反应器液相返混特性和气液传质特性的影响规律,并用“组合模型”分析了反应器各局部区域的返混情况。实验结果表明:液相返混主要由循环返混所致,约占95%以上;固相的存在对液相返混特性和气液传质特性均有显著的影响。研究结果对开发这类反应器具有重要意义。     

气液固相催化合成甲醇本征动力学

研究了以液体石蜡为液相介质在铜基催化剂上由CO、CO_2与氢气合成甲醇的本征动力学,按CO和CO_2加氢生成甲醇的反应途径,提出了反应机理,建立了6种动力学模型,经参数估值及模型筛选,得出了最终模型,该模型的计算值与实验值吻合很好,对CO及CO_2转化速率的平均偏差分别为3.69%和3.92%。     

气液固三相浆态搅拌反应器中管式内过滤器的过滤特性研究

探讨了在气液固三相浆态搅拌反应器中设置管式内过滤器，以实现气液固三相分离及浆态反应器的连续化。冷模研究表明：在强烈搅拌下，存在一种动态平衡过滤。即在滤饼沉积速率及剥离速率达到平衡条件下，可实现液相进料及滤液排料的连续化。在确定适宜过滤元件结构及过滤介质后研究了搅拌速度 、固含率、体系性质等因素对气液固三相浆态搅拌釜中管式中管式内过滤器的过滤速率的影响。气相按一定比例随液相通过过滤介质 ，其比例大小取决于过滤器的压降大小。实验表明：对颗粒平均直径在（0.8-1.0)10^-4m的α一氧化铝及硅铝氧化物细粒可获得较满意的分离效果。     

PREDICTION OF FLOW REGIME TRANSITIONS IN VERTICAL UPWARD THREE PHASE GAS-LIQUID-SOLID FLOW

The effect of solids concentration on the bubble to bubble-slug, bubble-slug to slug, and slug to churn flow transitions in gas-liquid-solid vertical flow has been studied using air, water, and glass beads in a 5 cm ID plexiglass column. Several simple models to predict the transitions were developed utilizing criteria proposed for gas-liquid vertical flow. These criteria are shown to apply equally well in the absence or presence of the solid phase

With solids present in the flow, the bubble to bubble-slug and bubble-slug to slug flow transitions both occurred at lower superficial gas velocities because of increased bubble coalescence. However, the slug to churn flow transition was unaffected by solids in the range of flow conditions studied.     

变孔径分布板减小液固流化床中液相返混

引言流化床亲合色谱蛋白质分离新方法综合了亲和吸附的快速、高选择性与液固流化床液相负荷大、传质速率高等优点,尤其是生物细胞可随液相穿透空隙率较大的吸附剂颗粒床层,因此该方法是构成连续分离-反应相耦合的蛋白质生产工艺的有效手段．但不足之处是流化床内的液相返混会严重影响分离效率,因此必须采取措施加以抑制．国外有采用磁稳定流化床来减小液相返混,但要添加体积比44％的磁性颗粒且要在75G_s的磁通密度下操作,有可能影响产品的生物活性．鉴于此,可采取不外加场源的稳定化措施来减小液相返混．本文通过对液固流化床液相返…     

HEAT TRANSFER CHARACTERISTICS OF THREE PHASE FLUIDIZED BEDS

Heat transfer characteristics of two (liquid-gas, liquid-solid) and three (liquid-gas-solid) phase fluidized beds have been studied in a 15.2 cm-ID column fitted with an axially mounted cylindrical healer. Effects of gas velocity (0-12 cm/s). liquid velocity (0-16cm/s), particle size (1.7-8.0 mm) and liquid viscosity (0.001-0.039 Pa s) on heat transfer coefficient were determined. The heat transfer coefficient increased with fluid velocities and particle size and it decreased with liquid viscosity in two and three phase fluidized beds. The bed porosity at which the maximum heat transfer occurred decreased with particle size but increased with liquid viscosity. The coefficient were correlated in terms of experimental variables. Modified Nusselt number from the present and previous studies has been correlated with modified Prandtl and Reynolds numbers.     

玻璃钢三相分离器

本文介绍了玻璃钢三相分离器的结构及其优点.