Effects of Preform Shear on Tensile Properties of a Woven C/SiC Composite

This article addresses effects of weave defects in an angle‐interlock C‐fiber preform on the tensile properties of the resulting fully processed C‐fiber/SiC‐matrix composite. For this purpose, a preform was intentionally sheared in a controlled manner after weaving. The resulting distortions were quantified by analyzing high‐resolution images of the preform surface after the first step of matrix processing, while the tows were still clearly visible. Comparisons are made of tensile test results on specimens cut from this composite panel and from a pristine panel in select loading orientations. Strain maps obtained by digital image correlation are used to identify local strain variations that are attributable to weave defects. The results are discussed in terms of: (i) the shear‐normal coupling that arises in loading orientations of present interest, and (ii) the geometric effects of tow misalignment on tow continuity along the specimen gauge length. The composite is found to perform in a robust manner, in the sense that the tensile properties are not sensitive to the presence of the defects.     

Analysis of SiC/SiC composites for energy applications at ambient conditions

Plain weave planar and biaxially braided tubular SiC/SiC CMCs are evaluated in tension and four-point bending, respectively, at ambient conditions. Custom-designed fixtures for CMC testing are developed for each loading mode and are coupled with three-dimensional digital image correlation. Stereoscopic image correlation analysis reveals crack initiation and failure sites to provide insight into stress redistribution mechanisms. Scanning electron microscopy is performed postmortem to determine the influence of microstructural features on crack initiation and failure. Crack spacing is measured in situ by stereoscopic image correlation and confirmed by SEM measurements to relate to underlying tow-tow crossing points. Triangulated surface heights of plain weave tow architecture are used to determine that subtle differences in neighboring transverse tow angle, which vary within a range of ±4° from horizontal, have no significant effect on final fracture location. The results presented reaffirm the state of current SiC/SiC CMCs developed for energy applications and will help to further improve SiC/SiC and other CMCs.     

Changes in tow geometry of plain‐weave carbon/epoxy fabrics draped onto compliant hemisphere molds

In this study, draping of carbon/epoxy fabrics (Plain weave, 3k) onto hemisphere molds is studied to understand the deformation behavior of fabrics during thermoforming. In order to characterize the local deformation of fabrics draped onto hemisphere molds, specimens are selected and prepared for microscopic observation. Several tow parameters such as crimp angle and tow amplitude are investigated to determine the effect of forming conditions and material properties of molds on the microstructures of fabrics during draping and forming. The measured parameters were normalized with respect to an undeformed specimen to facilitate a comparison between specimens. Hemisphere molds made of aluminum and PVC foam are used to observe the effect of mold compliance on microstructural changes during forming. The stress–strain behavior of the foams are measured to correlate the behavior of micro‐tow structures with the foam properties. It is found that some of the tow deformation during shearing is significantly altered when using the compliant foam mold. Polym. Compos. 27:111–118, 2006. © 2006 Society of Plastics Engineers.     

基于深度学习的平纹Cf/SiC复合材料原位拉伸损伤演化与断裂分析

为揭示平纹C_f/SiC复合材料的拉伸损伤演化及失效机理,开展了X射线CT原位拉伸试验,获得材料的三维重构图像,利用深度学习的图像分割方法,准确识别出拉伸裂纹并实现其三维可视化。分析了平纹C_f/SiC复合材料损伤演化与失效机理,基于裂纹的三维可视化结果对材料损伤进行了定量表征。结果表明:平纹C_f/SiC复合材料的拉伸力学行为呈现非线性,拉伸过程中主要出现基体开裂、界面脱黏、纤维断裂及纤维拔出等损伤;初始缺陷易引起材料损伤,孔隙多的部位裂纹数量也多;纤维束外基体裂纹可扩展至纤维束内部,并发生裂纹偏转。基于深度学习的智能图像分割方法为定量评估陶瓷基复合材料损伤演化与失效机理提供了有效分析手段。     

Prediction of orthotropic mechanical properties of plain‐weave composites with matrix voids using unit cells at multi‐scales

A numerical procedure for predicting the orthotropic mechanical properties of plain‐weave composites with matrix voids through a combined approach of the representative volume element method and finite element analyses is presented. The representative volume element method was implemented using two unit cells established at different length scales with equation boundary conditions. By considering the presence of randomly scattered voids throughout the matrix induced during the manufacturing process, it was assumed in the simulation that the spatial distribution of matrix voids is completely random. The procedure was exemplified with a glass fiber‐reinforced (plain‐weave fabric) epoxy composite with matrix voids. Sensitivity studies were conducted to quantify the influence of fiber volume fraction and mechanical properties of the constituent phases on the orthotropic mechanical properties of the composite. The numerical procedure, which can be implemented in ABAQUS, is an efficient tool for guiding the design of plain‐weave composites at materials level and also provides effective properties of such composites for the design optimization of engineering structures made of such composite materials. © 2012 Society of Chemical Industry     

Effects of Tow‐Scale Holes on the Mechanical Performance of a 3D Woven C/SiC Composite

This article addresses the effects of small holes (1–2 mm in diameter) on the tensile properties of a woven C/SiC composite. Holes are introduced by one of two methods: by insertion of fugitive rods into the woven preform before adding the matrix or by drilling after panel fabrication. The tensile strength exhibits only a weak sensitivity to the presence of holes, regardless of the manner in which the holes are introduced. Nevertheless, woven holes appear to be somewhat less detrimental to strength. The effects are attributed to the fact that the tows in specimens with woven holes are locally intact and thus contribute to load‐bearing. Full‐field strain maps reveal strong spatial periodicity, reflecting the underlying crack pattern and weave geometry. Even when averaged over lengths equal to the unit cell dimensions, the strains exhibit periodicity, with a wavelength dictated by the unit cell dimensions. When holes are present, the strain patterns reflect a convolution of the effects of weave geometry and strain concentrations near the holes. The results have implications for development of high‐fidelity models for these composites: notably, in selection of a suitable representative volume element and for modeling schemes that capture the stochastic nature of cracking.     

Shear properties of three‐dimensional woven composite reinforcements

This paper presents a comprehensive experimental study and detailed mechanistic interpretations of the shear deformation of three‐dimensional (3D) reinforcements. Six types of 3D angle interlock glass fiber preforms (3DAP) were fabricated using a range of weave parameters including the fabric density, fabric layer, and yarn linear density. A modified picture frame was developed to ensure a pure shear load during the test. Through a series of comprehensive tests, our results demonstrated that the fabric density played a key role in the mechanical properties of 3DAP and that the reinforcements with low fabric density and yarn linear density were easy to shear. The shear deformation mechanism was analyzed based on the meso‐structure. It is expected that this research will provide preliminary work for building a theoretical model of 3D woven preform. POLYM. COMPOS., 38:244–251, 2017. © 2015 Society of Plastics Engineers     

间位芳纶基导电纤维多功能织物的开发与研究

采用自纺的含间位芳纶基导电纤维的纱线,通过正交试验,从织物密度、组织和嵌织间距等方面出发,设计出不同规格的织物,并对织物进行阻燃、抗静电等功能性测试。在此基础上,对正交结果进行分析,确定出最佳的织物密度、组织和嵌织间距来保证织物具有最优的功能性,从而为织物的功能性整理做准备。     

Scalable measurements of tow architecture variability in braided ceramic composite tubes

The performance of braided ceramic matrix composites has been shown to depend on the spatial arrangement of tows; therefore, a new class of tools is required to measure irregularities in the composite architecture for components with intricate geometries. We report a scalable and robust reconstruction technique built upon stereoscopic digital image correlation that is able to efficiently measure the position of tows in arbitrarily shaped composites. This method was applied to triaxially braided ceramic matrix composite tubes intended for use as nuclear fuel cladding, which revealed both long‐range “systematic” tow packing defects associated with the manufacturing process and short‐range “intrinsic” defects due to the braid architecture. These findings suggested that the character of tow spacing variation in braided composite tubes was substantially more complex than in planar woven composites. These measurements are expected to lead to improved processing of braided composites and to facilitate the design of statistically representative virtual specimens for finite element modeling.     

凉感纤维织物导热系数影响因素的探讨

采用普通涤纶、含1%云母颗粒的涤纶(1%云母/涤纶)以及含5%云母颗粒的涤纶(5%云母/涤纶)三种材质,上机纬密采用200根/10 cm、300根/10 cm、400根/10 cm,组织采用平纹、斜纹、缎纹试织试样。通过Hot Disk热常数分析仪,采用正交试验及极差、方差分析,研究了纤维材质、上机纬密、组织对凉感纤维织物导热系数的影响。结果表明:在试验设置变量范围内,纤维材质对导热系数的影响显著,上机纬密、组织对导热系数的影响高度显著,影响因素从大到小顺序为上机纬密>组织>纤维材质。     

Characterizing Weave Geometry in Textile Ceramic Composites Using Digital Image Correlation

Techniques for characterizing tow architectures and defects in woven ceramic composites are required for generating high‐fidelity geometric models and subsequently probing effects of defects on composite performance. Although X‐ray computed tomography (CT) has been shown to provide the requisite information with potentially sub‐μm resolution, the technique is inherently limited to probing only small volumes: on the order of a few unit cells of typical weaves. Here, we present an assessment of the efficacy of a complementary 2D technique, based on surface topography mapping via 3‐D (three‐dimensional) digital image correlation (DIC), with potential for ascertaining long‐range features in weaves and defects that cannot be gleaned from CT imaging alone. Upon comparing surfaces reconstructed from CT and DIC data, we find that DIC is capable of resolving surface heights with a root mean square(RMS) error of ~10 μm (about twice the CT voxel size, 4.4 μm) and a spatial resolution of ~20 μm over areas of several cm². Achieving this level of resolution requires use of sufficiently small speckles (~50 μm) and small subset size (~300 μm) relative to the characteristic tow dimensions (~1 mm). The error is somewhat higher (about 20 μm) in areas where surface discontinuities or rapid changes in topography exist (e.g., at tow boundaries).     

Elektrophoretische Abscheidung zur Herstellung von faserverstärkten Keramik‐ und Glasmatrix‐Verbundwerkstoffen — Eine Übersicht

In this paper, we review the application of the electrophoretic deposition (EPD) technique in the fabrication of fibre reinforced composites, with particular emphasis on composites with glass and ceramic matrices containing metallic or ceramic fibre fabric reinforcement. The review covers research published in the last 10 years. EPD has been used to infiltrate preforms with tight fibre weave architectures using different nano‐sized ceramic particles, including silica and boehmite sols, as well as dual‐component sols of mullite composition. The principles of the EPD technique are briefly explained and various factors affecting the EPD behaviour of ceramic sols and their optimisation to obtain high infiltration of the fibre preforms are considered. Overall, the analysis of the published data and our own results demonstrate that EPD, being simple and inexpensive, provides an attractive alternative for ceramic infiltration and coating of fiber fabrics, even if they exhibit tight fibre weave architectures.     

Surface quality prediction of thermoset composite structures using geometric simulation tools

Abstract

The surface quality of polymer composite laminates was examined via geometric modelling techniques and compared to experimental data. TexGen software provided the platform for the development of a surface roughness simulation tool which accounted for textile architecture and specific cure kinetics of the matrix. The study focused on the influence of thermal and chemical shrinkage during cure and the change in localised volume fraction across the surface of a unit cell. A one-dimensional analysis was used to determine proportional dimensional changes to the matrix region, with the results stitched together to form a three-dimensional topological plot. Three demonstrator geometric models were developed to represent a carbon 2 × 2 twill weave fabric with 3000, 6000 or 12 000 tows. These models were analysed with low and high shrink resin properties. Optical microscopy was used to determine accurate tow forms for compacted tows which aided the development of the geometric model. Simulated profiles, topography and surface roughness measures were compared to experimental data which demonstrated the significance of matrix contraction and fabric architecture on the final surface quality. The simulations were shown to represent experimental data typically within 6%.     

Pattern‐driven color pattern recognition for printed fabric motif design

Pattern‐driven design method is an important data‐driven design method for printed fabric motif design in textiles and clothing industry. We introduce a novel framework for automatic design of color patterns in real‐world fabric motif images. The novelty of our work is to formulate the recognition of an underlying color pattern element as a spatial, multi‐target tracking, classification, segmentation and similarity association process using a new and efficient color feature encoding method. The proposed design method is based on pattern‐driven color pattern recognition and indexing from the element image database. A series of color pattern recognition algorithms are used for color and pattern feature extraction. The local statistical corner features and Markov random field model are used for motif unit tiling detection and conversion. The color feature encoding problem is modeled in a gray‐scale color difference optimization problem, which can be solved quickly by existing algorithms. Color pattern feature matching, segmentation and indexing techniques are then used to locate and replace the elements in the motif unit image with similar elements in the database. Experiments show that the approach proposed in this study is effective for color pattern recognition and printed fabric motif design.     

Using textile topography to analyze X‐ray CT data of composite microstructure

The 3‐dimensional yarn architecture in a 2‐dimensional woven fabric reinforced composite is nonuniform. Many structural features appear that are not obvious from consideration only of the yarn architecture in the single layer textile fabric. A complete set of 3‐dimensional image data was acquired for a representative volume of the composite using X‐ray micro‐computed tomography. Extensive image analysis was, however, necessary to reveal the yarn architecture due to relatively low signal‐to‐noise ratio and contrast levels relative to optical microscopy of polished cross sections.     

Assessment of uniformity of fibre coloration in Tencel woven fabrics dyed using reactive dyes

Weave structure and fabric density has an influence on dye penetration. The uniformity of dyeing, expressed as the uniformity of fibre coloration, of Tencel woven fabrics comprised of different weave structures, was assessed. The fabrics were dyed by exhaust and continuous dyeing methods using selected reactive dyes. Cross‐sectional images were captured and then given a rating 1–5 with respect to the depth of the fibre filaments of the yarn of the woven fabric. The images were assessed both subjectively and objectively. The uniformity of fibre coloration was expressed in terms of the standard deviation, mean value and histogram analysis such as dispersion and bandwidth. Objective assessment of uniformity of fibre coloration is a more accurate and quicker method than visual assessment and can be used to assess the uniformity of fibre coloration of woven and knitted fabrics dyed by any class of dyes. Improvement of the uniformity of fibre coloration of Tencel fabrics of various weave structures by causticisation of the fabrics and by modification to the padding process was investigated.     

A novel method for fabric color transfer

Fabric color design is a complex process in textiles and clothing industry. A new method for fabric color selection and transferring is proposed in this study. An automatic way to select the colors from the natural images is developed for fabric color design. Based on these colors, a fabric image is then used for color transferring. The fabric image is processed by a bias field estimation operation, and the membership function of the color deviations of the image has been obtained. According to the selected colors and the color membership function, the fabric image colors can be changed and transferred to a new image that preserves the similar texture appearance but with significantly different color effects. The experimental results confirm the effectiveness of the proposed method. © 2014 Wiley Periodicals, Inc. Col Res Appl, 40, 304–310, 2015     

The large deformation elastic response of woven kevlar fabric

The large deformation elastic response of a plane woven Kevlar fabric is investigated analytically and experimentally. The analysis assumes the undeformed geometry to be a sequence of interlaced arcs of circles that reverse at each yarn midpoint, and each yarn is modeled as an extensible elastica subject to certain compatibility conditions. Deflection-force relations for the fabric are determined in terms of the initial weave geometry and the elastic properties of the individual yarns. The theoretical results agree well with the results of experiments performed on a fabric woven from 400 denier Kevlar yarns under conditions of uniaxial loading in both warp and fill directions.     

Mechanical behavior of textile composite materials using a hybrid finite element approach

A novel analytical solution is presented to describe the mechanical behavior and failure of textile reinforced composites. This solution is constructed from two parts. First a geometrical model, based on a processing science approach coupled with graphical rendering, is utilized to quantify the spatial characteristics of the fabric preform inside the composite. A 3-D iterative hybrid finite element analysis is then used, utilizing data acquired from the geometrical model, to predict the stressstrain behavior of the composite. Inelastic behavior is modeled using an expanded Hahn and Tsai model and maximum stress criterion is used to predict initial failure. Damage progression is predicted based on a stiffness reduction approach. AS4 carbon/epoxy plain weave composite laminates, with a range of fiber volume fractions, have been tested. A 3-D woven E-glass/poly-vinyl-ester (PVE) angle interlock composite was also tested. Analytical results are compared with results from this experiment as well as other analytical models and experimental data in the literature. Theoretical model predictions are in agreement with most experimental data.