Effects of thickness and environmental temperature on fracture behaviour of polyetherimide (PEI)

The fracture behaviour of a polyetherimide (PEI) thermoplastic polymer was studied using compact tension (CT) specimens with a special emphasis on effects of specimen thickness and testing temperatures on the plane strain fracture toughness. The results show that the valid fracture toughness of the critical stress intensity factor, K _IC, and strain energy release rate, G _IC, is independent of the specimen thickness when it is larger than 5 mm at ambient temperature. On the other hand, the fracture toughness is relatively sensitive to testing temperatures. The K _IC value remains almost constant, 3.5 MPa in a temperature range from 25 to 130°C, but the G _IC value slightly increases due to the decrease in Young's modulus and yield stress with increasing temperature. The temperature dependence of the fracture toughness, G _IC, was explained in terms of a plastic deformation zone around the crack tip and fracture surface morphology. It was identified that the larger plastic zone and extensive plastic deformation in the crack initiation region were associated with the enhanced G _IC at elevated temperatures.     

Numerical prediction of notch bluntness effect on fracture resistance of SM490A carbon steel

The present work investigates the notch radius effect on fracture resistance using the finite element (FE) damage analysis based on the multiaxial fracture strain model. The damage model was determined from experimental data of notched bar tensile and fracture toughness test data using a sharp‐cracked compact tension specimen. Then, the FE damage analysis was applied to simulate fracture resistance tests of SM490A carbon steel specimens with different notch radii. Comparison of simulated results with experimental data showed good agreement. Further simulation was then performed to see effects of the specimen size, thickness, and side groove on J‐R curves for different notch radii. It was found that effects of the specimen size and thickness became more pronounced for the larger notch radius. Furthermore, it was found that without side groove, tearing modulus for notched specimens was similar to that for cracked specimens, regardless of the notch radius.     

Effect of geometry on compressive failure of notched composites

The compressive failure of carbon fibre-epoxy laminates is investigated theoretically and experimentally. Panels with a single edge notch, a central notch or a central hole are considered. The failure mechanism is by microbuckling in the 0° plies and is accompanied by delamination and plastic deformation in the off-axis plies [1]. To predict the critical length of the microbuckle and the failure load, the microbuckle is modelled as a cohesive zone. The magnitude of the normal compressive traction across the microbuckle is assumed to decrease linearly with increasing overlap of material on either side of the microbuckle. The relative effect of the specimen size and a bridging length scale is investigated to illustrate the transition between small-scale and large-scale bridging. If the bridging length scale is small compared with the specimen dimensions, the specimen fails when the stress intensity at the notch tip equals a critical compressive stress intensity factorK _IC . When the bridging length scale is not small compared with either the initial defect size or the unnotched ligament length then it is necessary to include the details of the traction across the microbuckle to predict the failure load accurately.     

Thickness effect on the mode III fracture resistance and fracture path of rock using ENDB specimens

Study of the thickness effect in predicting the crack growth behavior and load bearing capacity of rock‐type structures is an important issue for obtaining a relation between the experimental fracture toughness of laboratory subsized samples and the real rock structures with large thickness. The fracture of rock masses or underground rock structures at deep strata may be dominantly governed by the tensile or tear crack growth mechanism. Therefore, in this research, a number of mode I and mode III fracture toughness experiments are conducted on edge notch disc bend (ENDB) specimen made of a kind of marble rock to investigate the effect of specimen thickness on the corresponding K_Ic and K_IIIc values. It is observed that the fracture toughness of both modes I and III are increased by increasing the height of the ENDB specimen. Also, the ratio of K_IIIc/K_Ic obtained from each thickness of the ENDB specimens is compared with those predicted by some fracture criteria, and it was shown that the minimum plastic radius (MPR) criterion is the main suitable criterion for investigating the fracture toughness ratio K_IIIc/K_Ic . Also, the effect of ENDB height on fracture trajectory of tested samples is assessed. It is shown that the crack grows curvilinearly in thicker ENDB samples and cannot extend along the crack front in small specimens.     

Toughness and microscopic fracture mechanisms of unfilled and short-glass-fibre-filled poly(cyano arylether)

Fracture mechanisms of an advanced high-strength thermoplastic poly(cyano arylether) (PCAE) and its short-glass-fibre (SGF)-reinforced composites have been studied in relation to toughnesses K _c and J _c. Test temperatures were 23 and 100 °C. Reflected and transmitted optical observations were combined with scanning electron microscopy for the fractographic investigation. For unreinforced PCAE tested at 100 °C, the damage area in front of a notch becomes fairly large in size and consists of numerous tensile microfailures around the local plastic yielding zone, as compared with that tested at 23 °C. This resulted in a substantial improvement of K _c and a big increase in J _c. Filling fibres, however, produced both toughening and anti-toughening results: effects of fibre spanning, pull-out and bridging across the local plastic failure zone and zigzag propagation of fracture due to fibre filling, improved the toughness. However, adhesive failure at the fibre-matrix interface, tensile microcleavage at the fibre ends and straightforward fracture in the skin layer, considerably diminished the values of K _c and J _c, except for the trend of K _c at 23 °C.     

A fracture mechanics approach to ceramo-metal bond evaluation

The incidence of mechanical failure of cast metal/porcelain dental restorations has promoted a study to develop reliable methods of characterizing and improving bond strengths when produced under standard dental laboratory conditions. Single-edge notch beam specimens were prepared by firing porcelain from a single blended frit to either side of a central metal coupon and subjecting these to four-point bending at 20 ± 2° C and 0.5 mm min^–1 crosshead speed. Specimens of three representative dental alloys and an experimental alloy were prepared in two specimen sizes and three notch widths. The fracture toughness (K _Ic) values were independent of notch width and specimen size over the range of these variables examined and good discrimination was obtained. The fracture toughness of all bonds was improved by a commercial hot isostatic pressure cycle. SEM examination of the fractured surfaces suggested that this improvement was due to the reduction in microporosity at the interface.     

Delamination of multidirectional composite laminates at 0°/θ° ply interfaces

The main objective of this study is to develop a methodology for establishing mixed-mode delamination propagation criteria of non-unidirectional laminates. The crack interface was chosen to be 0°/45° and the effort was mainly focused on obtaining the mode I fracture toughness (G_IC). The widely used DCB test was avoided due to anticipated problems with intralaminar damage developing at the ply interface of interest. The ADCB and AMMF methods were used to determine the mixed-mode fracture toughness with the largest amount of mode I. The selected stacking sequence resulted in desirable crack propagation behavior; there was no change of delamination plane, an acceptable crack front profile, no initial specimen curvature, and no energy dissipation through global specimen damage. Finite element simulation was found to be the only tool capable of analyzing the experimental data.     

Tensile fracture of centre-notched angle ply (0/±45/0)S and (0/90)2S graphite — epoxy composites

The fracture behaviour of centre-notched (0/± 45/0)_S and (0/90)_2S laminates with increasing notch length has been studied. Two test series have been investigated: specimens of constant width (W=20 mm) and small notch length (2a 12 mm), and specimens with various notch lengths (5 2a 35 mm) and a constant relative notch length (2a/W=0.5). An X-ray technique showed that the damage at the notch tip, which is formed at increasing load, consists mainly of subcracks parallel to the fibres of the constituent layers. The damage zone causes the crack opening displacement (COD) to deviate from the original linearity. TheK _R curve concept has been applied assuming that the COD deviation from linearity is completely the result of original crack extension. This approach fails to describe the notch length effect, because a tangent point between theK _R andK curves was not found and because of a strong dependency of the maximum fracture resistanceK _Rmax on notch length. The fracture behaviour of 20 mm wide specimens could be explained with the point and average stress criteria, based on characteristic lengths which are independent of notch length. At various notch lengths at a constant 2a/W=0.5, however, the characteristic lengths increased with increasing notch length.     

Effect of microstructure on elevated-temperature fracture behaviour of two-dimensional carbon/carbon composites

The fracture behaviour of two-dimensional carbon/carbon composites has been studied at temperatures upto 1650°C, using both chevron-and straight-notch single-edge notch beam (SENB) specimens. In all cases, the R-curve behaviour and fracture toughness variations with specimen orientation and temperature are characterized and correlated with the specific microstructure and failure micromechanisms. Higher crack growth resistance and fracture toughness of the longer fibre composite are attributed to the enhanced fibre pull-out and fibre bridging in the following wake region. The relative contribution from the frontal and following wake zone is determined experimentally by the use of renotching methods which demonstrate the effectiveness of the traction zone behind the crack tip. The temperature effects on the toughening mechanisms are examined in terms of crystal structure and fibre matrix interfacial characteristics.     

Fracture mechanics of short glass fibre-reinforced nylon composite

The fracture behaviour of injection-moulded short glass fibre-reinforced, thermoplastic nylon 6.6 plaques has been studied under static loading using compact tension specimens and under impact loading using single-edge notched charpy specimens. The influences of specimen position as taken from the plaque mouldings, notch direction, notch sharpness and the rate of testing on the fracture toughness of this composite system were investigated. Results indicated that the fracture toughness is highest for the cracks perpendicular to the mould fill direction and is lowest for cracks parallel to the mould fill direction. A single fracture parameter, K _c, seems to be inadequate for fracture toughness characterization. Evaluation of the fracture toughness as a function of notch sharpness indicated that for notches perpendicular to the mould fill direction the fracture toughness is not affected by the sharpness of the initial notch. However, for cracks in the mould fill direction, sharpness of the initial notch had a significant effect upon the measured value of the fracture toughness. Results also indicated, that the fracture toughness is rate insensitive over the crosshead speed ranging from 0.5–50 mm min^–1. Finally, the specimen position, as taken from plaque mouldings, had no significant effect on the measured value of the fracture toughness.     

Measurement of the in situ ply fracture toughness associated with mode I fibre tensile failure in FRP. Part II: Size and lay-up effects

The in-plane size, thickness and lay-up effects on the measured fracture toughness associated with fibre tensile failure were investigated for a T300/920 laminated carbon/epoxy material system. Compact tension specimens were tested with scaled in-plane size, increased thickness, and having various proportions of plies orientated at 0° and 90° to the loading direction. No in-plane size effects were discovered; however, testing revealed a thickness dependence. It was found that the ply toughness is significantly dependent on the thickness of the 0° layers. Propagation values of toughness were measured to be 132 kJ/m² for specimens made up of [90/0₂] sub-laminates and between 57 and 69 kJ/m² for all other configurations. Investigation of the fracture surfaces using SEM revealed that the increase in measured toughness for specimens with thicker 0° plies was due to an increase in the amount of pulled-out 0° fibres.     

Translaminar fracture toughness: The critical notch tip radius of 0° plies in CFRP

The relationship between translaminar fracture toughness measured at initiation and specimen initial notch root radius is investigated for the translaminar failure mode of cross-ply IM7/8552 carbon/epoxy laminates. Compact tension specimens with four sizes of notch root radii were tested; the true initiation toughness of the laminate was measured from specimens with notch tip radii of ρ ? 250 μm. Testing of specimens with larger notch root radii, ρ = 750 μm, yielded an apparent toughness that was found to be 30% higher than the true toughness of the laminate. The propagation toughness corresponding to the R-curve plateau was found not to be affected by the initial notch tip radius. Investigation of the fracture surfaces of failed specimens revealed that there is no interaction between the 0° and 90° ply failure mechanisms, and that the critical notch radius is a property intrinsic to the 0° plies of the laminate.     

Damage zone around crack tip and fracture toughness of rubber-modified epoxy resin under mixed-mode conditions

Damage zones that form around crack tips before the onset of fracture provide significant data for evaluating the fracture behavior of polymeric materials. The size of the damage zone correlates closely with the fracture toughness of the resin. In this study, we investigate the relationship between the fracture toughness and damage zone size around crack tips of a rubber-modified epoxy resin under mixed-mode conditions. The fracture toughness, G_C, based on the energy release rate, is measured using an end-notched circle type (ENC) specimen. The deformation of rubber particles in the damage zones is also observed using an optical microscope. The results show that the fracture toughness, G_C, of the rubber-modified epoxy resin is closely related to the area of the damage zone. In the specimen with a loading angle of 30°, the rubber particles were deformed ellipsoidally due to the difference between the first and second principal stresses.     

Fracture toughness of Si3N4 measured with short bar chevron-notched specimens

The short bar chevron-notched specimen was used to measure the plane strain fracture toughness of hot-pressed Si₃N₄. Specimen proportions and chevron-notch angle were varied, thereby varying the amount of crack extension to maximum load (upon which K_ic was based). The measured toughness (4.68 ± 0.19 MN m^3/2) was independent of these variations, inferring that the material has a flat crack growth resistance curve.Nomenclature a crack length - a _A crack length at arrest of unstable crack advance - a ₁ length of chevron notch at specimen surface (distance from line of load application to point of chevron emergence at specimen surface) - a ₀ initial crack length (distance from line of load application to tip of chevron) - a _R crack length at ending of stable crack extension (conversely, crack length at onset of abrupt, unstable crack advance) - B specimen thickness - H specimen half-height - K _1A stress intensity factor at arrest of unstable crack advance - K _IR stress intensity factor at end of stable crack extension (crack growth resistance) - K _IC plane strain fracture toughness - P _max maximum applied load in fracture toughness test - W specimen width - Y ^* dimensionless stress intensity factor coefficient for chevron-notched specimen - Y ^* _m minimum value ofY ^* as a function of - a/W - ₀ a ₀/W - ₁ a ₁/W     

Measurement of Specific Fracture Energy and Surface Tension of Brittle Materials in Powder Form

Studies of the influence of specimen geometry and size–effect on the K _R –curves and the related fracture parameters were carried out by the authors (Kumar and Barai 2008b). The present paper is a supplementary contribution and reports interesting results related to the effect of the loading condition and size–effect studies on the K _R –curves associated with the cohesive stress distribution for complete fracture process, the double–K fracture parameters, the CTOD–curves and the process zone length using two different loading conditions (i.e., three–point bending test and four–point bending test). The laboratory size specimen with initial–notch length/depth ratios 0.3 and 0.5 are considered in the work. The load–crack opening displacement curves for these loading conditions are obtained using well known version of fictitious crack model.     

Fracture of quasi-isotropic composite sheets with sharp notches

Continuous fibre composites are materials that exhibit rather linear elastic deformation behaviour: suggesting brittleness and notch sensitivity. However, notched composites may sustain significant mechanical load. The notch resistance of composites is investigated on quasi-isotropic composite sheets with sharp crack like notches. This allows the use of analytic solutions of the stress field around a crack in a similar way as is used for linear elastic fracture mechanics (LEFM) in homogeneous isotropic solids. Similar to the small scale yielding boundary condition in fracture mechanics, applied on homogeneous isotropic solids, a small-scale non-linear damage condition should be fulfilled for valid LEFM application on quasi-isotropic composites. Indeed, it appeared to be possible to define critical stress intensity factors (K_1c) for the quasi-isotropic composite. Moreover, K_1c values can quantitatively be related to laminate parameters and to the related damage and deformation processes occurring in a small near crack tip zone with intense non-linearity and strain gradients in the thickness direction. Before the final explosive fracture occurred, stable crack growth was observed. This could be described with R-curves, as done for homogeneous metal sheet specimens. Indeed, also in this case, the R-curves were identical, independent of the length of the initial crack-like notch. The R-curves can be estimated adopting a crack-bridging model. Crack growth occurs at the notch tip in the 0° plies. The other plies bridge the fractured 0° plies. The fracture mechanisms, determining the K_1c-values and the shape of the R-curve, are quite different for composites and metals. Yet, the method of fracture mechanics, well established for metals, can obviously also be applied to quasi-isotropic composites.     

Short-rod elastic-plastic fracture toughness test using miniature specimens

The standard ASTM-E399 plane-strain fracture toughness (K _IC) test requires (1) the test specimen dimensions to be greater than a minimum size and, (2) fatigue precracking of the specimen. These criteria render many materials impractical to test. The short-rod elastic-plastic plane-strain fracture toughness test proposed by Barker offers a method of testing not requiring fatigue precracking and furthermore, it appears that test specimens smaller than that stipulated by ASTM can be used to obtain validK _IC values. In this study, the use of a modified miniature short-rod fracture toughness test specimen was investigated. Our miniature short-rod specimen is approximately 7 mm long and 4 mm diameter. These mini specimens are well suited for the purpose of testing biomaterials. The value of the minimum stress intensity factor coefficient (Y _m ^* ) for the mini short-rod specimens was determined experimentally using specimens machined from extruded acrylic rod stock. An elastic-plastic fracture toughness analysis using the mini specimens gave values ofK _IC for extruded acrylic (nominally PMMA) equal to 0.67 ± 0.06 MPa m^1/2. The problem of testing non-flat crack growth resistance curve materials (such as PMMA) using the short-rod fracture toughness test method is discussed. A modification to the test procedure involving the use of aY ^* value corresponding to a short crack length is suggested as a method of overcoming this difficulty.Nomenclature a crack length - a ₀ initial crack length - a ₁ length of the chevron notch on the mini short-rod specimen - a _m critical crack length — crack length atY _m ^* - C specimen compliance - C dimensionless specimen compliance = CED - D mini short-rod specimen diameter - E Young's modulus - K ₁ stress intensity factor - K _1C plane-strain fracture toughness - K _max fracture toughness calculated usingP _max - P load applied to the test specimen during a short-rod fracture toughness test - P _c load applied to the test specimen atY _m ^* - P _max maximum load applied to the specimen during a short-rod fracture toughness test - p plasticity factor - W mini short-rod specimen width - Y ^* stress intensity factor coefficient - Y _m ^* minimum of the stress intensity factor coefficient - dimensionless crack length =a/W - ₀ dimensionless initial crack length = ₀/W - ₁ dimensionless chevron notch length =a ₁/W - _m dimensionless critical crack length =a _m/W     

Notch fracture toughness of high-strength Al alloys

In this study, the notch fracture toughness (NFT) of high-strength Al alloys was examined by a non-standardized procedure. The NFT is defined as the critical notch stress-intensity factor (NSIF) K_ρ,c, which is determined by using several methods of analysis and computing. A set of specimens with different notch root radii made from overaged 7xxx alloy forging was selected. The influence of the notch radius on the fracture toughness of the material was considered. It was found that the notch radius strongly affects the fracture behavior of forged 7xxx alloy in overaged condition. The notch fracture toughness was higher than the fracture toughness of a cracked specimen and increased linearly with notch radius. The critical notch radius was related to the spacing of intermetallic (IM) particles which promote an intergranular or transgranular fracture mechanism according to their size. It appeared that ductile transgranular fracture generated by the formation of dimples around dispersoids and matrix precipitates was predominant which indicates that intense strains are limited to a much smaller zone than the coarse IM particles spacing. This double mechanism is also operate for crack propagation of ductile fatigue. The nature and morphology of IM particles exert significant effects on the rate of fatigue crack growth and fracture toughness properties.     

Fracture Toughness Test with a Sharp Notch Introduced by Focussed Ion Beam

The validity of fracture toughness data obtained from tests with V-notched bending bars is affected by the notch root radius and the presence of R-curve behavior. A macroscopic test specimen has been developed that contains a notch introduced by focused ion beam machining. This produces a notch root radius of less than 0.1 μm, so that notch effects can be ignored for most ceramics. Also, due to the very small notch depths the influence of a rising R-curve should be very close to that of natural cracks. First tests, carried out on a Ce-doped zirconia ceramic resulted in a toughness of K _Ic ≈ 5.9 MPa√m.     

Experimental and numerical investigation of cracked chevron notched Brazilian disc specimen for fracture toughness testing of rock

The cracked chevron notched Brazilian disc (CCNBD) specimen has been suggested by the International Society for Rock Mechanics to quantify mode I fracture toughness (K_Ic) of rock, and it has also been applied to mode II fracture toughness (K_IIc) testing in some research on the basis of some assumptions about the crack growth process in the specimen. However, the K_Ic value measured using the CCNBD specimen is usually conservative, and the assumptions made in the mode II test are rarely assessed. In this study, both laboratory experiments and numerical modeling are performed to study the modes I and II CCNBD tests, and an acoustic emission technique is used to monitor the fracture processes of the specimens. A large fracture process zone and a length of subcritical crack growth are found to be key factors affecting the K_Ic measurement using the CCNBD specimen. For the mode II CCNBD test, the crack growth process is actually quite different from the assumptions often made for determining the fracture toughness. The experimental and numerical results call for more attention on the realistic crack growth processes in rock fracture toughness specimens.