自蔓延高温合成技术及发展

自蔓延高温合成（ＳＨＳ）是一项很有希望的制备材料的新技术,与传统工艺相比,自蔓延高温合成具有许多优点。对该合成法的历史发展,应用和理论研究作了简要概括,并全面系统地介绍了ＳＨＳ的工艺技术,其中包括与传统技术相结合的ＳＨＳ技术及在ＳＨＳ基础上的新技术。     

放电等离子烧结制备亚微米LaB6块体材料

采用氢直流电弧等离子体法,以稀土镧块为原料,制备出了平均粒度为20 nm的La纳米粉末.以L丑纳米粉和B纳米粉为原料,采用放电等离子烧结(SPS)技术制备出了LaB6亚微米晶块体材料.通过系统研究各烧结参数对材料结构和性能的影响,得到了最佳的烧结工艺.获得了相对密度高达99.3%的致密烧结体,其维氏硬度达到14.1 GPa.采用XRD,SEM和TEM对材料的相组成和微观组织进行了测试分析.结果表明.SPS烧结LaB6块体的晶粒细小,平均晶粒尺寸为150nm,整体结构均匀致密.实验表明,SPS技术可以实现LaB6细晶块体材料的快速烧结.     

High-Temperature Tensile Properties of Nano-Oxide Dispersion Strengthened Ferritic Steels Produced by Mechanical Alloying and Spark Plasma Sintering

Oxide-dispersion strengthened (ODS) ferritic steels were produced by mechanical alloying and subsequent spark plasma sintering. Very fast heating rates were used to minimize porosity when controlling grain size and precipitation of dispersoids within a compacted material. Sintering cycles performed at 1373 K (1100 °C) induced heterogeneous, but fine grain size distribution and high density of nano-oxides. Yield strengths at room temperature and at 923 K (650 °C) are 975 MPa and 298 MPa, respectively. Furthermore, high-temperature ductility is much increased: total strain of 28 pct at 923 K (650 °C).     

Self-Propagating High-Temperature Synthesis of Silicon Carbide Nanofibers

Russian Journal of Non-Ferrous Metals - The results of investigations into the organization of the synthesis of silicon carbide fibers in the gas phase using silicon powder, an energy additive of...     

Characterization of Oxide Dispersed AlCoCrFe High Entropy Alloy Synthesized by Mechanical Alloying and Spark Plasma Sintering

The present study deals with phase evolution of oxide dispersed AlCoCrFe high entropy alloy during mechanical alloying and spark plasma sintering. Mechanical alloying of AlCoCrFe resulted in a single BCC phase. However, ordering of BCC phase with evolution of chromium carbide and sigma phase were observed after spark plasma sintering. High hardness of 1,050 ± 20 HV₁ and 1,070 ± 20 HV₁ was observed for AlCoCrFe high entropy alloy without and with oxide dispersion, respectively. Significant contribution from solid solution strengthening effect in high entropy alloys appears to have overwhelmed the effect of oxide dispersion on hardness.     

放电等离子烧结技术的发展和应用

放电等离子烧结（SPS）是一种快速，低温，节能，环保的材料制备新技术，本文综述了SPS在国内外的发展和应用，介绍了SPS的原理，特点及在新材料制备加工中的应用。     

放电等离子烧结TbFeCo磁光靶材工艺研究

研究了采用放电等离子烧结技术制备TbFeCo磁光靶材的工艺过程，考察了烧结温度对材料组织均匀性和致密度的影响。利用扫描电子显微镜和能谱分析仪对材料的微观组织形貌及成分进行了分析，同时用阿基米德法测量了材料的密度。结果表明：适当的提高烧结温度可以使材料得到均匀的组织，理想的致密度。但过高的烧结温度会造成材料局部组织的熔化，使材料的组织均匀性变差，l010℃的烧结温度是制备具有均匀组织和理想致密度Tb(Fe，Co)3材料的最佳温度。     

Obtaining of Ligatures from Manganese Production Wastes by Self-Propagating High-Temperature Synthesis

Powder Metallurgy and Metal Ceramics - Ongoing development of manganese ore deposits in various countries and their treatment in special ferroalloys furnaces leads to continued environmental...     

氧化锆基金属陶瓷放电等离子烧结制备与性能研究

氧化锆陶瓷材料的脆性限制了其在某些领域的应用。文章首创在氧化锆粉末中加入316L不锈钢粉,通过放电等离子烧结制备氧化锆基金属陶瓷。试验通过不同的成分配比和不同的烧结温度进行对比研究,采用金相分析、XRD、SEM/EDS等测试方法,对材料的微观结构和宏观性能等进行了表征与分析。并通过断口分析,讨论了Zr O2·316L金属陶瓷的增韧机理。结果表明:采用放电等离子烧结制备出的材料随相组成的成分所占比例的改变,其致密度、弯曲强度、横向断裂强度、断裂韧性都随之呈现出相应的变化规律;316L相以片状均匀分布在氧化锆基体中,在材料断裂时起到了颗粒/纤维增韧的作用。同时氧化锆部分以亚稳相t-Zr O2的形态存在,也起到了相变增韧的作用。     

Spark Plasma Sintering of Magnesium Fluoride Nanopowders

Powder Metallurgy and Metal Ceramics - The densification behavior of nanostructured MgF2 ceramics in the spark plasma sintering process is studied. Nitrate synthesis is employed to produce fine...     

W-Re高比重合金的SPS烧结

采用放电等离子烧结(SPS)设备制备了W-Re高比重合金,烧结温度为1800℃,烧结压力为40MPa,保温时间为5min。对SPS烧结的W-Re合金试样进行了密度、硬度等性能测试。采用金相显微镜观察试样的金相组织、晶粒大小。结果表明:采用SPS烧结,可以在较低的温度下实现W-Re合金的致密化,并能有效控制晶粒长大,提高材料的硬度。     

Study of Molybdenum-Tungsten Powder Compaction Processes by Spark Plasma Sintering

Metallurgist - This paper presents the results of studying the production of molybdenum-tungsten alloys by spark plasma sintering at various process conditions, as well as the processes of material...     

Spark Plasma Sintering of Cryomilled Nanocrystalline Al Alloy - Part I: Microstructure Evolution

Aluminum alloys are widely used because they are lightweight and exhibit high strength. In recent years, spark plasma sintering (SPS) technology has emerged as a viable approach to sinter materials due to its application of rapid heating and high pressure. In this study, SPS was chosen to consolidate dense ultrafine-grained (UFG) bulk samples using cryomilled nanostructured Al 5083 alloy (Al-4.5Mg-0.57Mn-0.25Fe, wt pct) powder. Both bimodal microstructure and banded structure were observed through transmission electron microscopy (TEM) investigation. The evolution of such microstructures can be attributed to the starting powder and the process conditions, which are associated with the thermal, electrical, and pressure fields present during SPS. A finite element method (FEM) was also applied to investigate distributions in temperature, current, and stress between metallic powder particles. The FEM results reveal that the localized heating, deformation, and thermal activation occurring at interparticle regions are associated with the formation of the special microstructure.     

Microstructure,Mechanical Properties,and Sliding Wear Behavior of Oxide-Dispersion-Strengthened FeMnNi Alloy Fabricated by Spark Plasma Sintering

Metallurgical and Materials Transactions A - The face-centered-cubic (fcc) CoCrFeMnNi high-entropy alloy suffers from low strength and wear resistance at ambient temperature. Herein, we developed a...