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通过对双宫丝绵纤维的主要物理力学性能及纤维形态进行检测,并与对照组的普通丝绵和蛹衬丝绵的性能进行比较,分析双宫丝绵压缩回弹性优良的原因。测定了双宫丝绵的压缩回弹性和纤维强伸力,结果表明:双宫丝绵的回复率96%,压缩率53%;单丝平均断裂强力4.43 c N,断裂伸长25.42%,这些指标均高于对照组的普通丝绵和蛹衬丝绵,双宫丝绵的回弹性达到了蚕丝被优等品的国家标准。电镜下观察到双宫丝绵的纤维较其他两种丝绵纤维的直径粗、长度长,丝纤维之间形成纵横交错的网络多。测试结果显示双宫丝绵优良的性能与它的结构有关。 相似文献
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由于机制丝绵的劳动生产率高,目前已经成为丝绵生产的主要加工方式,但机制丝绵的加工过程中,一般需要使用双氧水,而双氧水在运输和储存过程中存在易燃易爆等风险。为解决该问题,文章创新性地设计了过碳酸钠或碳酸钠-臭氧联合体系对机制丝绵片脱胶的方法,对两种方法的残胶率、含杂率、压缩率和回复率等丝绵质量指标进行分析,并与使用双氧水加工的商业化优等机制丝绵进行比较。研究表明:在机制丝绵加工过程中,使用过碳酸钠或碳酸钠-臭氧加工得到的丝绵脱胶均匀、纤维表面平整光滑;在残胶率、含杂率、压缩回弹性等方面均达到优等品标准(即残胶率≤5%,含杂率≤0.1%,压缩率≥45%,回复率≥92%);在白度和手感柔软性方面也展现出良好的性能。结果表明:在不用双氧水的条件下,依然可以制备性能优良的机制丝绵,显示了免用双氧水加工机制丝绵的可行性。 相似文献
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针对常规煮绵工艺效率低、能耗大、时间长、脱胶效果差等问题,文章拟采用几种新型、环保、高效的煮绵助剂处理丝绵,并采用扫描电镜、红外光谱仪、X射线衍射仪等对不同工艺处理后的丝绵表面处理效果,丝绵二级结构的情况及其他性能指标进行测试。研究结果表明:与常规工艺处理后的丝绵相比,清丝宝处理后的丝绵手感蓬松、柔软、无异味、光泽较好,其残油率、练减率、煮练温度、煮练时间及白度均有不同程度的改善。因此,在现行的丝绵生产工艺中,采用清丝宝处理丝绵,其实验数据对完善已有成果的煮绵工艺及改善丝绵的内在质量具有一定的实际应用价值。 相似文献
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Silk is a kind of natural fiber with good luster strength elasticity dyeability hygroscopicity and other advantages. Silk products are quite popular to the customers because of their excellent performance such as heat preservation air permeability and so on which make them comfortable to use. Silk floss which is made from pupa lining secondary cocoon etc. can be used as floc and filler materials and is an important part of silk products. According to its production mode silk floss can be divided into manual silk floss and machine-made silk floss and the latter has become the main processing mode of silk floss production due to its high production efficiency. In terms of composition silk flossing generally contains 20% - 30% sericin pupa oil and impurities so in the degumming process in addition to adding sodium carbonate and other degumming agents to remove sericin a large amount of hydrogen peroxide with strong oxidation property is also used to increase the cleanliness and smoothness. Unfortunately hydrogen peroxide is highly flammable and explosive and poses a risk in transportation and storage causing potential safety hazards to the silk processing industry. In order to solve this problem we innovatively propose two hydrogen peroxide-free processing methods of machine-made silk floss by using sodium percarbonate degumming or sodium carbonate-ozone. As an environmentally friendly solid oxidant sodium percarbonate can produce hydrogen peroxide and sodium carbonate after decomposition and is often used to degrade organic harmful substances. Similarly ozone is a common strong oxidant with broad-spectrum antibacterial properties and because ozone can be produced instantly by ozone generators there is no risk of transport and storage. Silk is composed of silk fibroin and sericin. Among them silk fibroin is fibrous protein which will swell in hot water while sericin is globular protein which is easy to dissolve in hot water. As a result in this paper heated sodium percarbonate solution and sodium carbonate-ozone system were used to deglue silk floss. The methods were as follows silk floss was degummed three times in boiling 0. 78 g / L sodium percarbonate solution for 30 minutes each time or was degummed three times in boiled 0. 5 g / L Na2 CO3 solution with ozone continuously flow at a rate of 100 mg / L - h for 30 minutes each time. After cleaning and drying the degummed silk floss can be obtained. After the experiment the apparent morphology sericin residual efficiency impurity rate compression resilience whiteness and other silk floss quality indexes of the two methods were analyzed and compared with superior machine-made silk floss processed by commercial way with hydrogen peroxide. The results show that both two processing methods got uniform degumming effect of silk floss and the surface of the single fiber was smooth and the degumming effect was basically the same as that of commercial products prepared with hydrogen peroxide. The sericin residual rate of silk floss was between 3% - 4% which was in line with the requirements of less than 5% of superior silk floss. There was no significant difference between silk floss obtained and commercial superior products in smoothness and whiteness. In conclusion the performance of silk floss in all aspects has reached the standard of superior products that is the sericin content is not more than 5% the impurity content is not more than 0. 1% the compression rate is not less than 45% and the response rate is not less than 92% . Based on the experimental results and analysis it can be concluded that the machine-made silk floss with good performance can be prepared without hydrogen peroxide showing the feasibility of processing machine-made silk floss without hydrogen peroxide which is of great significance to the research and development of a safe and reliable oxidant system for the removal of impurities in silk floss and to further improve the safety of machine-made silk floss production process. © 2022 China Silk Association. All rights reserved. 相似文献
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采用碱液、超高温和自制柔软剂处理研制高性能丝绵。通过碱液浓度、柔软剂浓度、超高温处理时间和柔软剂处理时间的正交试验设计,对相关指标进行DPS数据分析,发现4因素对丝绵的弹性回复率没有显著的影响,而柔软剂对弹性压缩率和含油率均有显著影响。丝绵的弹性回复率为92.37%~97.66%,弹性压缩率为59.21%~66.77%,均优于行业标准蚕丝绵被特级品的规定。丝绵的含油率为0.28%~1.39%,均优于行业标准蚕丝绵被一级品的规定。丝绵的平均保温率在81.91%~85.24%之间,传热系数的平均值在21.37~27.13 W/(m2.℃)之间。超高温蒸汽处理有利于增加丝绵的弹性和蓬松性。提出了丝绵加工比较适宜的工艺条件组合。 相似文献
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近年来蚕丝被产业保持蓬勃发展的良好势头,但也出现了丝绵增重等不良现象。为解决蚕丝被的相关问题,满足高质量发展的要求,有关方面组织开展了国家标准的修订工作。文章介绍GB/T 24252-2009《蚕丝被》国家标准的修订背景及原则,全面解析标准的主要修订内容,着重强调蚕丝被填充物(蚕丝绵)不允许增重,具体指出标准不足之处,初步提出了标准的实施建议,以便于蚕丝被生产、消费、检验等相关方面更好地理解、领会和应用标准,从而推动提高蚕丝被产品质量、规范蚕丝被市场秩序、维护产销双方合法权益,以及促进行业健康稳定发展。 相似文献
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Maximum mature larval, cocoon and shell weight were observed during winter season followed by spring and autumn seasons of both white and brick red eri cocoons. Cocoon weight and shell weight were found about 40 and 5%, respectively, as compared to mature larval weight. Degumming loss was estimated at about 10% for white eri and 12% for brick red eri cocoons. Weight of silk fibres varies significantly between layers and decreasing trend was noted from outer to inner layers. Similar trend was observed for single fibre denier and it differs significantly between places (ecoraces), seasons and layers of cocoons. Ascending trend for single fibre tenacity was found from floss to pelade layers of both white and brick red eri silk cocoons and significant influence was observed for places, seasons as well as layers whereas no impact was noted in case of single fibre breaking elongation. Regression equations between weight of degummed cocoon fibres, single fibre denier and single fibre tenacity and to its corresponding values for different places (ecoraces), seasons and cocoon layers were established and estimated R2 and ‘t’ values confirmed the significance of these regression equations. 相似文献
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目的 优化调味金枪鱼鱼松配方。方法 对金枪鱼碎肉制作鱼松进行研究。通过L9(34)正交试验设计对其配方进行优化, 以感官评定得分和鱼松疏松度为考核指标, 考察棕榈油、绵白糖、豌豆粉、调味料(生姜粉+五香粉+白酒)添加量对鱼松品质的影响。结果 棕榈油、绵白糖、豌豆粉、调味料的用量为16%、14%、16%、(0.8+0.8+3)%。按此条件生产的鱼松产品呈金黄色, 色泽均匀一致, 呈绒状, 纤维疏松, 口感肉质细腻, 有鱼香味。结论 本研究将金枪鱼下脚料用于鱼松生产, 出品率为72%, 增加了鱼松产品的多样性, 提高了金枪鱼下脚料的附加值。 相似文献