Application of two-output port fiber coupler as gasoline level sensor

Detection of gasoline level can be done in a safe and simple way using two output port multimode fiber coupler with a structure of 2 × 2 as a sensor. Two output ports (sensing port) are connected with two reflector displacement device (RDD) and functioned as two probes. These probes are placed on the wall of gasoline tank in a storied and work interchangeably or together depending on setting of these probes. Detection mechanism of the system is based on changes in intensity of reflected light from the reflector RDD that shifts due to changes in level of gasoline (hydrostatic pressure principle). Changes in intensity of light coming into the sensing port are then forwarded to the optical detector. Experiments performed by varying the location of the second probe as 45 cm, 50 cm, and 55 cm above the first probe to detect the level of gasoline in the process of filling and emptying the tank. Experimental results show the process of filling and emptying the tank have small differences of 6% with the dynamic range, the linear region, and resolution are 100 cm, 70 cm, and 0.4 cm respectively. Sensor sensitivity in filling and emptying process of the tank are 2.7 mV/cm and 2.8 mV/cm respectively. These results were the best performance of the sensor, which occurs when the level of the second probe was 55 cm above the first probe.     

Externally pressurized gas journal bearing with slot restrictors arranged in the axial direction

In this study, a novel rectangular slot restriction-type externally pressurized gas journal bearing was developed for use in high-speed rotating machinery, such as medical devices and industrial machines. The proposed bearing has several rectangular slot restrictors arranged in the inner surface of the bearing. To measure the bearing characteristics, a model was developed for the numerical calculation of the pressure distribution in the bearing clearance and the static characteristics of the bearing. The proposed bearing, which consists of two parts, was designed and can be manufactured using appropriate techniques. In this study, a prototype bearing with eight slots in its surface was manufactured as a test piece for fundamental tests. The diameter and length of the test bearing are 30 and 40 mm, respectively. The roundness of the bearing was measured using a three-dimensional coordinate measuring machine, and the results were used in the analysis. The pressure distribution and static characteristics obtained experimentally were found to be in good agreement with the calculated values. In the rotational tests, the rotor speed exceeded 380 Hz (22,800 rpm), and whirl vibration did not occur. During testing, the maximum rotor vibration amplitude was 0.002 mm, corresponding to an eccentricity ratio of 0.3.     

Potential step study of electrooxidation of methanol in 1-butyl-3-methylimidazolium tetrafluoroborate

A potential step method was used to characterize the electrooxidation of methanol on a chemically modified electrode in an ionic liquid solvent. Two major findings were reported from this study. Firstly, the oxidation was dominant 2.2 s after the potential step. Before that, the double layer charging and adsorption were dominant. Therefore, there should be a waiting time of a few seconds if a methanol sensor is developed with a potential step method. Secondly, the oxidation of methanol on the electrode was diffusion controlled. The concentration of methanol affected the diffusion. The diffusion constant D₀ was 8.37 × 10⁻¹⁷ m²/s when the concentration was lower than 0.5 M and was 2.66 × 10⁻¹³ m²/s when the concentration was higher than 1.0 M. This suggests that the methanol concentration should be kept higher than a threshold in an ionic liquid based fuel cell.     

Wear behaviour of dental enamel at the nanoscale with a sharp and blunt indenter tip

Two different diamond nanoindenter tips, a rounded conical (～1200 nm radius) and a sharp cube corner (20–50 nm radius) were used to abrade bovine enamel. Square abraded areas (2 μm × 2 μm, 5 μm × 5 μm, 10 μm × 10 μm) were generated with loads that varied from 50 μN to 500 μN depending on the indenter tip. In addition normal and lateral forces were simultaneously measured along 10 μm single scratched lines with the sharp cube corner tip. SEM (scanning electron microscopy) and TEM (transmission electron microscopy) were also used to characterise the worn areas and debris. Two different wear mechanisms were observed depending on the geometry of the tip. The rounded tip generates a predominantly elastic contact that mainly compresses and plastically deforms the superficial material and generates severe shear deformation within the sub-surface material which, under certain conditions, fractures and removes material from the sample. The sharp tip cuts into and ploughs the enamel creating a wedge or ridge of material ahead of itself which eventually detaches. This sequence is repeated continuously for every passage of the sharp indenter tip. The different mechanisms are discussed in terms of abrading tip contact angle and enamel microstructure.     

Structural inspection and troubleshooting analysis of a lab-scale distillation column using gamma scanning technique in comparison with Monte Carlo simulations

In the present study, structural inspection and troubleshooting analysis of a lab-scale distillation column has been performed using gamma scanning technique and Monte Carlo simulations. MCNP4C Monte Carlo code has been used for simulations of the column and calculation of the computational density profile. The tested column is a one-pass tray type with 51 cm diameter. A Cs-137 sealed source and a 1 × 1 inch NaI (Tl) detector has been used for this gamma scanning process. According to the results, both experimental and simulation results showed the specification of trays and another section of the column accurately. Also, in addition to the flooding and damaged tray in the column, defects such as foaming with the density of 0.17 g/cm³ can be distinguished using this technique. Based on the results, using photopeak count approach the differences in the material attenuations can be better distinguished. The effectiveness of this approach in determination of malfunctions increases with the density of the material between the source and the detector. Analyzing the experimental and simulation results are indicative of the fact that the procedures and methods used in this work are quite suitable for improving the accuracy of the troubleshooting analysis based on gamma scanning technique.     

FEA simulation of thermal processes during the direct metal laser sintering of Ti64 titanium powder

With regard to the fact that laser sintering belongs to the high-temperature processes in which metal particles are sintered by a high-power laser, forming a homogenous structure, it is necessary and important to know the characteristics and the mechanism of these thermal processes. A high-power laser system produces three forms of heat that include convection, conduction, and radiation. These thermal processes affect the formation of internal stresses and tension that lead to deformations and rapidly influence the resulting quality, dimensions, density, micro-structure, and mechanical properties of fabricated parts. In response to this fact, it was important to analyse these heat transfer methods instantly during the direct metal laser sintering (DMLS) process simulation and subsequently monitor the parameters and settings of the sintering equipment in order to obtain acceptable manufacture outputs intended for further use. This work is focused on the creation of a FEA simulation model and the simulation of thermal processes across an object during and after the sintering process in the cooling stage, when it is important to consider a laser beam trajectory, temperatures of individual elements affected by the laser beam, and current laser energy in time. A 3D FEA simulation model was created in order to represent actual behaviour of a part during the sintering process. The simulation model consisted of two sub-models, particularly the building platform model with the dimensions of 250 mm × 250 mm × 22 mm, with stainless steel as the selected material, and the model of individual layers of sintered titanium powder with the dimensions of 10 mm × 10 mm × 0.03 mm. The total number of used layers was 12, which represents the total thickness of 0.36 mm. Applied power was P = 170 W. The simulation as such was carried out using the FEA software, Simulia Abaqus supported on the Windows x86-64 platform, which uses an integrated solver to make thermal and mechanic calculations. The calculations included also the impact of the protective argon atmosphere located in the process chamber. Mutual impact between individual layers was also considered. The simulation results were confronted with the results of already performed experimental studies of other scientific works, with the compliance and confirmation of assumptions being on a very good level.     

AC conduction mechanism and battery discharge characteristics of (PVC/PEO) polyblend films complexed with potassium chloride

New K⁺ ion-conducting polymer blend electrolyte films based on amorphous polymer poly(vinyl chloride) (PVC) and semicrystalline polymer poly(ethylene oxide) (PEO) complexed with KCl salt were prepared using a solution-cast technique. The maximum value of ionic conductivity of a PVC/PEO:KCl (42.5:42.5:15) system is 8.29 × 10⁻⁶ S/cm at 303 K. The absorption edge was found at 4.30 eV for undoped film, while it was observed at 4.03 and 3.93 eV for 10 and 15 wt% KCl doped films, respectively. The direct band gaps for these pure and salt doped PVC/PEO films were found to 4.10, 3.86 and 3.74 eV, respectively, whereas the indirect band gaps were determined as 4.15, 3.72 and 3.64 eV. Transference number values showed that the charge transport in this electrolyte system is predominantly due to ions (t_ion = 0.97). The discharge capacity for PVC/PEO:KCl (42.5:42.5:15) polymer blend electrolyte system is 11 μA/h.     

Nanocomposite polymer electrolyte based on rice starch/ionic liquid/TiO2 nanoparticles for solar cell application

Nanocomposite polymer electrolyte (NCPE) was prepared using solution cast technique. Rice starch (RS), lithium iodide (LiI), 1-methyl-3-propylimidazolium iodide (MPII) as ionic liquid and TiO₂ nanopowder (RS:LiI:MPII:TiO₂) were introduced to prepare the sample. The conductivity of 3.63 × 10⁻⁴ S/cm was achieved by introducing 30 wt.% of 1-methyl-3-propylimidazolium iodide (MPII) as ionic liquid and 2 wt.% of TiO₂. Temperature-dependent conductivity and dielectric behavior were analyzed in this work. Dye sensitized solar cell was fabricated using the nanocomposite film for this sample and analyzed.     

Research on the dynamic characteristics of a turbine flow meter

In the hardware-in-loop simulation of aero-engine control system where the real fuel regulator is engaged, it's crucial to measure the real-time flow rate. In view of this, a flow meter with high precision and fast response is important. In this paper, modeling and experiments are conducted to verify the dynamic characteristics of a turbine flow meter (TFM). For the modeling part, driving torque and resistance torques are analyzed to derive the kinetic equation of TFM. Simulation with the kinetic equation shows good dynamic performance of TFM. In experiments, a workbench is designed to generate step-type flow and sine-type flow for identification in time domain and frequency domain. Results show that the settling time for TFM is no more than 100 ms and its band-with is over 4.61 Hz. Compared with the settling time of a main fuel valve and the band-width of a main fuel control loop, that is, 1.2 s and 2 Hz respectively, TFM is considered to be adaptive to measure the fuel of aero-engine.     

Electrocatalytic determination of captopril using a modified carbon nanotube paste electrode: Application to determination of captopril in pharmaceutical and biological samples

A carbon paste electrode modified with carbon nanotube and benzoylferrocene (BF) was fabricated. The electrochemical study of the modified electrode, as well as its efficiency for electrocatalytic oxidation of captopril (CAP), was described. The electrode was employed to study the electrocatalytic oxidation of CAP, using cyclic voltammetry (CV), chronoamperometry (CHA) and square wave voltammetry (SWV) as diagnostic techniques. It has been found that the oxidation of CAP at the surface of modified electrode occurs at a potential of about 85 mV less positive than that of an unmodified CPE. SWV exhibits a linear dynamic range from 1.0 × 10⁻⁷ to 3.5 × 10⁻⁴ M and a detection limit of 3.0 × 10⁻⁸ M for CAP. Finally the modified electrode was used for determination of CAP in CAP tablet and urine sample.     

Determination of haloperidol drug in ampoules and in urine samples using a potentiometric modified carbon paste electrode

A modified carbon paste electrode for haloperidol drug based on haloperidol-phosphomolybdate (HP-PM) as an ion-exchanger dissolved in plasticizer DBP and its potentiometric characteristics were discussed. The electrode exhibited a good Nernstian slope of 56.9 ± 0.3 mV/decade with a linear concentration range from 3.2 × 10⁻⁶ to 1.0 × 10⁻² M for the haloperidol ion. The limit of detection (LOD) was 1.5 × 10⁻⁶ M. It had response time of 5–8 seconds (s), useable in pH range of 6.2–8.6 and temperature of 20–60 °C. The electrode shows clear discrimination of haloperidol drug from several inorganic ions, sugars and some common drug excipients. The sensor was applied for determination of haloperidol drug in urine and in pharmaceutical formulations using potentiometric determination, standard addition and the calibration curve methods. The results are satisfactory with excellent percentage recovery comparable or better than those obtained by other routine methods.     

Wear of aligned silicon nitride under dry sliding conditions

The wear behaviour of textured silicon nitride (Si₃N₄) ceramics with aligned microstructures was analyzed under abrasive wear conditions. Dry reciprocating self-mated ball-on-flat wear tests were performed to study the influence of different microstructural plane/orientation combinations on the Si₃N₄ tribological behaviour. Textured materials showed superior wear resistance than non-textured reference Si₃N₄ for the whole range of loads and contact pressures, 5–50 N and 1.7–3.6 GPa, respectively, with an increase of about 70% for the maximum applied load. Within textured materials, the plane perpendicular to the extruding direction exhibited a 50% higher wear resistance (4 × 10^?5 mm³ N^?1 m^?1) than the parallel plane where the elongated grains were aligned. The severe wear process involved debonding, fracture and debris formation mechanisms. The progress of this sequence depended on the particular microstructure of each plane/orientation combination. A relationship between abrasive wear resistance and selected microstructural parameters has been established.     

Gasoline level sensor based on displacement sensor using fiber coupler

A simple and fire safe gasoline level sensor has been designed based on displacement sensor using fiber coupler. The sensing principle is to detect displacement of reflector, which is attached to membrane (reflector displacement device), due to the change of gasoline hydrostatic pressure. The displacement of reflector can be detected using fiber coupler from the change of optical power light reflected by the reflector. Three kinds of reflector displacement device used in this experiment are one-layer, two-layer, and three-layer membrane. The experimental results are 0–180 cm of dynamic range, 100–140 cm of linear range, 3.2 mV/cm of sensitivity, and 0.6 cm of resolution for reflector displacement device with one-layer membrane for emptying the tank process. The hysteresis data for emptying and filling the tank process yields the mean of difference 20% for one-layer membrane.     

Development and evaluation of a two-axial shearing force sensor consisting of an optical sensor chip and elastic gum frame

We developed a promising shearing force sensor that is small in size and can measure shearing force along two axes independently. This sensor consists of an elastic gum frame and an optical sensor chip (6 mm × 6 mm × 8 mm). From the experimental results, the resolutions of the sensor along the x- and y-axes are found to be 0.070 N and 0.063 N. We also experimentally demonstrated that the sensor can separately measure shearing force along two axes. Finally, we demonstrated that the scale factor which correspond to resolution and linear portion which correspond to measuring range of the signals can be changed easily by using three types of elastic gum frame. This sensor can be embedded in the finger of a robot hand and use it to not only measure shearing force but also detect the slip phenomenon.     

The design of polyaniline based sensor for the qualitative estimation of malonaldehyde

The detection of contaminated food in every stage of processing required new technology for fast identification and isolation of toxicity in food. Since effect of food contaminant are severe to human health, the need of pioneer technologies also increasing over last few decades. In the current study, MDA was prepared by hydrolysis of 1,1,3,3-tetramethoxypropane in HCl media and used in the electrochemical studies. The electrochemical sensor was fabricated with modified glassy carbon electrode with polyaniline. These sensors were used for detection of sodium salt of malonaldehyde and observed that a high sensitivity in the concentration range ∼1 × 10⁻¹ M and 1 × 10⁻² M. Tafel plots show the variation of over potential from − 1.73 V to − 3.74 V up to 10⁻⁵ mol/L indicating the lower limit of detection of the system.     

Influence of orientation and volume fraction of Aramid fabric on abrasive wear performance of polyethersulfone composites

In case of fabric reinforced composites of specialty polymers influence of orientation of fabric and its volume fraction on tribo-behaviour is sparingly studied. In our earlier work, we have reported on the influence of amount of Aramid fabric (AF) in polyethersulfone (PES) on abrasive wear performance. However, orientation effect of fabric with respect to abrading plane was not investigated. In this work three orientations of composites of PES containing Aramid (Kevlar 29) fabric with three concentrations 64, 72 and 83 wt.% were selected to study the influence on abrasive wear performance. Composites developed by compression molding technique were characterized for their mechanical and physical properties. The abrasive wear performance of the composites was evaluated by abrading 10 mm × 10 mm × 10 mm sample against silicon carbide (SiC) paper under various loads and two grades of abrasive papers. The fabric reinforcement enhanced the abrasive wear resistance of PES significantly (approximately 1.35–9.46 times depending on the operating conditions). It was observed that 83% fabric composite showed the highest resistance to abrasive wear and impact along with the best tensile strength and elongation properties. Its flexural strength and ILSS values, however, were the lowest. Sixty-four percent fabric composite, on the other hand, showed an exactly reverse trend among the three composites. Among the three orientations, fibres in normal and parallel (N–P) and normal and anti-parallel (N–AP) direction with respect to sliding plane proved to impart maximum wear resistance. N–P was best for light loads while N–AP was best for high loading conditions. Orientation parallel and anti-parallel (P–AP) was least beneficial in this respect. Moreover, the extent of improvement very much depended on the operating parameters such as grit size and load. Benefits endowed due to reinforcement were higher at less coarse grade paper. With increase in load, however, wear rate of composites with N–P orientation increased and for other two orientations it decreased. Thus, for severe operating conditions, N–AP orientation proved to be most beneficial. SEM studies proved supporting for understanding the influence of orientation on wear performance.     

Multi-range sensors for the measurement of liquid film thickness distributions based on electrical conductance

The paper presents an approach toward an enhancement of the measuring range of high-speed sensors for the measurement of liquid film thickness distributions based on electrical conductance. This type of sensors consists of electrodes mounted flush to the wall. The sampling of the current generated between a pair of neighboring electrode is used as a measure of the film thickness. Such sensors have a limited measuring range, which is proportional to the lateral distance between the electrodes. The range is therefore coupled to the spatial resolution. The proposed new design allows an extension of the film thickness range by combining electrode matrices of different resolution in one and the same sensor. In this way, a high spatial resolution is reached with a small thickness range, whereas a film thickness that exceeds the range of the high resolution measurement can still be acquired even though on the costs of a lower spatial resolution. A simultaneous signal acquisition with a sampling frequency of 3.2 kHz combines three measuring ranges for the characterization of a two-dimensional film thickness distribution: (1) thickness range 0–600 µm, lateral resolution 2×2 mm², (2) thickness range 400–1300 µm, lateral resolution 4×4 mm², and (3) thickness range 1000–3500 µm, lateral resolution 12×12 mm². The functionality of this concept sensor is demonstrated by tests in a horizontal wavy stratified air–water flow at ambient conditions. Using flexible printed circuit board technology to manufacture the sensor makes it possible to place the sensor at the inner surface of a circular pipe.     

Improved dielectric constant of thermoplastic blend as a function of alumina loading

Polycarbonate (PC) and Poly (methyl methacrylate) blends were prepared by incorporating Al₂O₃ into the polymer matrix using solution blending. The modified blends were characterized by X-ray diffraction, Thermogravimetric analysis, and Scanning electron microscopy. The crystalline to amorphous phase variation was confirmed by XRD with increase in the interplanar distance (d). TGA results indicate that the thermal stability of the modified blend was significantly improved as a function of alumina loading which may be due to interfacial interaction between the alumina particles and the polymers. Scanning electron microscopy studies reveal the presence of alumina particles resulting in plane surface morphology. The modified blends show very high dielectric constant value (10⁵–10⁷) as a function of frequency (in the range 50 Hz–35 MHz) and temperature in the range (40–150 °C). The modified polymer blend demonstrate consistent polarization across the frequency band 50 Hz–10 kHz. The neutral aggregates formation due to higher concentration of alumina loading demonstrated an influence on AC conductivity. This investigation can be feasible for electronic and electrical engineering application as the dielectric medium.     

Effect of various wood preservatives on limiting oxygen index levels of fir wood

Wood preservatives have been widely used to extend the service life of wood. The aim of this study is to evaluate the effects of various wood preservatives with different chemical loadings on fire performance of treated fir wood using by oxygen index test technique (ASTM D 2863-6). The limiting oxygen index (LOI) is the minimum percentage oxygen that is required to continue flaming combustion of a sample under laboratory conditions. For this purpose; wood preservatives commonly used in wood protection industry including amine–copper-quaternary, tanalith-E, wolmanit-CB, imersol aqua, vacsol aqua, timbercare aqua and protim-418 were studied as wood preservative chemicals. Mixture of boric acid + borax was also used as reference sample. The results indicated that LOI levels of all treated fir wood samples were higher than that of control samples except for timbercare aqua and protim-418 treated samples. The highest LOI level was obtained within 5% of wolmanit-CB and 2% of boric acid + borax treated wood samples. It appears that more than 3% concentration of wolmanit-CB treatment may have a potential fire retardant.