A low cost TL–OSL reader dedicated to high temperature studies

In some applications, luminescence dating needs performing studies above 550 °C and conventional or commercial instruments are not always perfectly adapted to this temperature range. We describe here an automated instrument capable of thermoluminescence and optically stimulated luminescence measurements. Main mechanical and digital design is reported showing the technical options leading to both a low cost of fabrication and good high temperature performances. The mechanical design favors simply shaped parts and uses a 3D-CAD software that can drive a numerically controlled milling machine. Besides, electronics is limited to elementary signal conditioning (for photomultiplier and thermocouple) and the more complex functions (as thermal regulation) are performed with softwares running on a standard PC. A fully automated prototype instrument was built using these options. This confirmed the low cost of fabrication and the possibility of measurements up to 800 °C and of withstanding temperatures higher than 600 °C for several minutes.     

Measurement of highly reflective surface shape using wavelength tuning Fizeau interferometer and polynomial window function

In this study, a 5N − 4 phase shifting algorithm comprising a polynomial window function and a discrete Fourier transform is developed to measure interferometrically the surface shape of a silicon wafer, with suppression of the coupling errors between the higher harmonics and the phase shift error. A new polynomial window function is derived on the basis of the characteristic polynomial theory by locating five multiple roots on the characteristic diagram. The characteristics of the 5N − 4 algorithm are estimated with respect to the Fourier representation in the frequency domain. The phase error of the measurements performed using the 5N − 4 algorithm is discussed and compared with those of measurements obtained using other conventional phase shifting algorithms. Finally, the surface shape of a 4-in. silicon wafer is measured using the 5N − 4 algorithm and a wavelength tuning Fizeau interferometer. The accuracy of the measurement is discussed by comparing the amplitudes of the crosstalk noise calculated by other algorithms. The uncertainty of the entire measurement was 34 nm, better than that of any other conventional phase shifting algorithms.     

Development and evaluation of a two-axial shearing force sensor consisting of an optical sensor chip and elastic gum frame

We developed a promising shearing force sensor that is small in size and can measure shearing force along two axes independently. This sensor consists of an elastic gum frame and an optical sensor chip (6 mm × 6 mm × 8 mm). From the experimental results, the resolutions of the sensor along the x- and y-axes are found to be 0.070 N and 0.063 N. We also experimentally demonstrated that the sensor can separately measure shearing force along two axes. Finally, we demonstrated that the scale factor which correspond to resolution and linear portion which correspond to measuring range of the signals can be changed easily by using three types of elastic gum frame. This sensor can be embedded in the finger of a robot hand and use it to not only measure shearing force but also detect the slip phenomenon.     

Direct measurement of bottom shear stress under high-velocity flow conditions

The objectives of the present research are to accurately measure bottom shear stress under high-velocity flow conditions. To achieve high-velocity flow conditions, a laboratory-scale flume has been specially built in which flow velocity can reach over 3 m s⁻¹. Also an instrument that can directly measure bottom shear stress has been developed and validated. Then, the flow resistance has been estimated by simultaneously measuring flow velocity and bottom shear stress. It appears that the shear stress is indeed proportional to velocity squared and also to Reynolds number. On the other hand, Manning's n value and the skin friction factor are more or less uniform across all experimental cases.     

Determination of the thermal conductivity of composted material

The objective of this study was to develop a reliable method for the determination of the thermal conductivity of composted material using the TP08 probe. Study was set out to determine whether the selection of a signal fragment used to establish thermal conductivity (λ), has a significant influence on the results. Also minimum number of measurements was determined for every phase of the composting process. No significant differences were reported between results, but certain changes in the value of λ were noted. In successive stages of the process, thermal conductivity of composted material were: 0.31 ± 0.09, 0.45 ± 0.14, 0.27 ± 0.03 and 0.37 ± 0.17 W m⁻¹ K⁻¹.     

Quasi-constant rotational stiffness characteristic for cross-spring pivots in high precision measurement of unbalance moment

This paper proposes a design method for cross-spring pivots with quasi-constant rotational stiffness in the field of unbalanced moment measurement. To achieve high precision measurement of unbalance moment, the relationship between instrument sensitivity and the rotational stiffness of the cross-spring pivot is revealed. In order to eliminate the impacts of payload changes on instrument sensitivity, the relationship between geometric parameters and the rotational stiffness of the pivot is studied. Further, cross-spring pivots with quasi-constant rotational stiffness are designed as the rotation unit of a static balancing instrument, while the center shift of pivot takes the minimum value. Certain amount of unbalance moments is measured by the instrument. Experimental studies of the instrument show that the maximum measurement errors of unbalance moments 0.162 g mm, 0.319 g mm and 1.300 g mm are 0.068 g mm, 0.086 g mm and 0.053 g mm, respectively, when the payload ranges from 0 g to 7000 g. The instrument can achieve a relatively high precision measurement and the instrument sensitivity is almost not affected by the changes of payloads. The effectiveness of the method and the stiffness property of the pivot are verified by the experiments. So this kind of pivot has good prospects in unbalance moment measurement.     

Refined reconstruction of liquid–gas interface structures for stratified two-phase flow using wire-mesh sensor

Wire-mesh sensors (WMS), developed at HZDR [4], [13], are widely used to visualize two-phase flows and measure flow parameters, such as phase fraction distributions or gas phase velocities quantitatively and with a very high temporal resolution. They have been extensively applied to a wide range of two-phase gas–liquid flow problems with conducting and non-conducting liquids. However, for very low liquid loadings, the state of the art data analysis algorithms for WMS data suffer from the comparably low spatial resolution of measurements and from boundary effects, caused by e.g. flange rings – especially in the case of capacitance type WMS. In the recent past, diverse studies have been performed on two-phase liquid–gas stratified flow with low liquid loading conditions in horizontal pipes at the University of Tulsa. These tests cover oil–air flow in a 6-inch ID pipe and water–air flow in a 3-inch ID pipe employing dual WMS with 32×32 and 16×16 wires, respectively. For oil–air flow experiments, the superficial liquid and gas velocities vary between 9.2 m/s≤ν_SG≤15 m/s and 0.01 m/s≤ν_SL≤0.02 m/s, respectively [2]. In water–air experiments, the superficial liquid and gas velocities vary between 9.1 m/s≤ν_SG≤33.5 m/s and 0.03 m/s≤ν_SL≤0.2 m/s, respectively [17], [18]. In order to understand the stratified wavy structure of the flow, the reconstruction of the liquid–gas interface is essential. Due to the relatively low spatial resolution in the WMS measurements of approximately 5 mm, the liquid–gas interface recognition has always an unknown uncertainty level. In this work, a novel algorithm for refined liquid–gas interface reconstruction is introduced for flow conditions where entrainment is negligible.     

Design and validation of a grinding wheel optical scanner system to repeatedly measure and characterize wheel surface topography

This paper describes the design and validation of an upgraded grinding wheel scanner system that controls the position of a Nanovea CHR-150 Axial Chromatism sensor along the x- and y-directions of the wheel surface to measure and characterize wheel surface topography. The scanner features a novel homing system that enables the wheel to be removed from the scanner, used on a grinding machine and then re-mounted and re-homed so that the same location on the wheel surface can be repeatedly measured and monitored. The average standard deviation for homing was 27.6 μm and 19.3 μm in the x- and y-directions, respectively, which is more than adequate for typical area scans of 25 mm². After homing, the scanner was able to repeatedly measure features that were similar in size to an abrasive grain (∼200 μm diameter) with an average error of 9.3 μm and 5.9 μm in the x- and y-directions, respectively. The resulting topography measurements were compared with Scanning Electron Microscope images to demonstrate the accuracy of the scanner. A custom particle filter was developed to process the resulting data and a novel analysis technique involving the rate of change of measured area was proposed as a method for establishing the reference wheel surface from which desired wheel topography results can be reported such as the number of cutting edges, cutting edge width and cutting edge area as a function of radial depth.     

A signal interpolation method for Fabry–Perot interferometer utilized in mechanical vibration measurement

In this investigation, a self-developed signal processing method for Fabry–Perot interferometer is proposed which can be utilized for high-speed dynamic displacement measurements, e.g. mechanical vibration measurements. The lookup table (LUT) integrated with the interference intensity equation has been employed for the interpolation processing of interference signals. With the aid of this method, the interpolation error has been reduced by 40% in comparison with that resulting from the commercial sinusoidal signal processing module. By operations of Fast Fourier Transform (FFT), the displacement measurement distribution can be converted into the frequency spectrum diagram. The interpolation resolution of the proposed interferometric displacement measurement system is about 0.1 nm. Experimental results demonstrate that this interferometer system is available for measuring frequencies till 2 kHz where its corresponding amplitude is 0.15 μm.     

Ability of different balance tests to discriminate between young and elderly subjects

Different balance tests are used to assess age-related decline of movement function. Good basic metric characteristics are in order for a balance test to become a useful assessment tool for clinical and research practice. By measuring balance of 27 young (22.3 ± 3.6 years) and 23 elderly (82.3 ± 9.6 years) adults discrimination power (ROC curve) of five common and one novel balance test was assessed (maximal lunge, quick step, leaning forwards and backwards, star excursion balance test, forward reach and centre-of-pressure (CoP) tracking, respectively). In all of the tests at least one parameter had high discriminating power (ROC area > 0.8, p < 0.05; d > 0.8). CoP displacement derived parameters in the star excursion balance test had high discrimination power and had the potential to give additional information on balance, besides the outreach distance. The interaction effect between age and direction of reach or lean proved to be insignificant, with the frequency of CoP direction changes in anterior–posterior direction during star excursion balance test being the only exception. The results of this study add to the methodological ground base in clinical balance assessment protocols by identifying parameters with the highest discriminating power of the most commonly applied balance assessment tests.     

Multi-range sensors for the measurement of liquid film thickness distributions based on electrical conductance

The paper presents an approach toward an enhancement of the measuring range of high-speed sensors for the measurement of liquid film thickness distributions based on electrical conductance. This type of sensors consists of electrodes mounted flush to the wall. The sampling of the current generated between a pair of neighboring electrode is used as a measure of the film thickness. Such sensors have a limited measuring range, which is proportional to the lateral distance between the electrodes. The range is therefore coupled to the spatial resolution. The proposed new design allows an extension of the film thickness range by combining electrode matrices of different resolution in one and the same sensor. In this way, a high spatial resolution is reached with a small thickness range, whereas a film thickness that exceeds the range of the high resolution measurement can still be acquired even though on the costs of a lower spatial resolution. A simultaneous signal acquisition with a sampling frequency of 3.2 kHz combines three measuring ranges for the characterization of a two-dimensional film thickness distribution: (1) thickness range 0–600 µm, lateral resolution 2×2 mm², (2) thickness range 400–1300 µm, lateral resolution 4×4 mm², and (3) thickness range 1000–3500 µm, lateral resolution 12×12 mm². The functionality of this concept sensor is demonstrated by tests in a horizontal wavy stratified air–water flow at ambient conditions. Using flexible printed circuit board technology to manufacture the sensor makes it possible to place the sensor at the inner surface of a circular pipe.     

Experimental evaluation of a distributed Brillouin sensing system for measuring extensional and shear deformation in rock

Distributed Brillouin sensing systems (DBSs) have growing applications in engineering and are attracting attention in the field of underground structures, including mining. The capability for continuous measurements of strain over large distances makes DBSs a promising monitoring approach for understanding deformation field evolution within a rock mass, particularly when the sensor is installed away from excavation damaged zone (EDZ). A purpose-built fiber optic sensing cable, a vital component of DBSs, was assessed in laboratory conditions.A test program was performed to observe DBSs response to various perturbations including strain and joint movements, including opening and shearing of joints. These tests included assessment of the strain-free cable response and the application of extensional and lateral displacement to various sensing cable lengths (strained lengths), from 1 m down to 1 cm. Furthermore, tests were done to evaluate the time-dependent behavior of the cable and to observe the effect of strain transfer using a soft host material (e.g. a soft grout) under lateral displacement.The noise level of the DBSs range was ±77 με, determined through repeated measurements on an unstrained cable. Stretching test results showed a clear linear correlation between applied strain and Brillouin frequency shift change for all strained lengths above half the spatial resolution of the DBSs. However, for strained lengths shorter than half the spatial resolution, no strain response was measurable and this is due to the applied internal signal processing of the DBSs to detect peak Brillouin gain spectrum and noise level. The stability with time of the measurements was excellent for test periods up to 15 h.Lateral displacement test results showed a less consistent response compared to tension tests for a given applied displacement. Although the Brillouin frequency shift change is correlated linearly with the applied displacement in tension, it shows a parabolic variation with lateral displacement. Moreover, the registered frequency response (correlated with strain) of the system decreased significantly when the sensing cable was embedded in a sand-filled tube compared with direct cable displacement.     

Design,calibration and tests of versatile low frequency impedance analyser based on ARM microcontroller

Numerous simple impedance analysers based on the microcontroller (μC) and dedicated impedance converter integrated circuits (IC) were reported recently. In many applications sophisticated analogue circuitry has to be appended to enhance the measurement possibilities or to circumvent the limitations. In this paper the impedance analyser IMP-STM32 based solely on the μC and general purpose operational and instrumentation amplifiers is presented. It uses the internal DAC and ADCs in the μC to generate the excitation and to measure the response of the measured object. It also uses the external analogue circuits to condition the excitation signal and measure voltage and current. The magnitudes and phase shifts of voltage and current are evaluated using the three parameter sine fitting algorithm allowing for fast low-frequency impedance measurements. The calibration procedure of completed device is presented as well as the tests of its accuracy. The device allowed for measurements at frequency range between 1 mHz and 100 kHz in 1 Ω to 1 GΩ impedance range with 1% accuracy. IMP-STM32 was also compared to the Agilent 4294A precision impedance analyser. In the middle of the impedance ranges (1 Ω to 300 kΩ) the discrepancies between the two were less than 0.2%.     

High-accuracy displacement metrology and control using a dual Fabry-Perot cavity with an optical frequency comb generator

A displacement metrology and control system using an optical frequency comb generator and a dual Fabry-Perot cavity is developed with sub-nm accuracy. The optical frequency comb generator has expanded the displacement measurement range and the dual cavity system has suppressed the environmental fluctuation. We evaluated the absolute uncertainty of the developed displacement measurement system to be approximately 190 pm for the displacement of 14 μm and the accurate displacement control using a phase-locked loop was demonstrated with a resolution of approximately 24 pm.     

Design and Analysis of MEMS Comb Drive Capacitive Accelerometer for SHM and Seismic Applications

This work presents the design of a MEMS accelerometer that is specifically intended for Structural Health Monitoring (SHM) applications where sensing low frequency low amplitude accelerations with high resolution is essential. The surface micromachined comb drive capacitance accelerometer structure has been considered in this design. The simulation experiments conducted on these devices using IntelliSuite MEMS design tool show that it has excellent displacement sensitivity of 21.39 μm/g, a capacitive sensitivity of 1.22 pF/g and voltage sensitivity of 1783 mV/g/V when it is designed to measure 0–0.1 g. Further, it is seen that it has a very low noise floor of 1.32 μg/√Hz and therefore high resolution. Since the accelerations can be as low as 0.04 g in SHM applications, excellent resolution is the primary goal in this design. Further, one more sensor specifically meant for strong motion seismic application has also been reported. This device has a bandwidth of 0–250 Hz and a noise floor of 5.612 μg/√Hz in addition to a sensor level voltage sensitivity of 97.9 mV/g/V. Finally, the comparison of these results with other similar devices reported in the past clearly illustrates the comparable performance of the present devices. Further, these devices, unlike the commercial low frequency accelerometers and other similar devices reported in the past can be fabricated by surface micromachining and CMOS compatible processes.     

A Pitot tube system for obtaining water velocity profiles with millimeter resolution in devices with limited optical access

An automated, miniature, S-type Pitot tube system was created to obtain fluid velocity profiles at low flows in equipment having limited optical access, which prevents the use of standard imaging techniques. Calibration of this non-standard Pitot tube at small differential pressures with a custom, low-pressure system is also described. Application of this system to a vertical, high-pressure, water tunnel facility (HWTF) is presented. The HWTF uses static flow conditioning elements to stabilize individual gaseous, liquid, or solid particles with water for optical viewing. Stabilization of these particles in the viewing section of the HWTF requires a specific flow field, created by a combination of a radially expanding test section and a special flow conditioner located upstream of the test section. Analysis of the conditioned flow field in the viewing section of the HWTF required measurements across its diameter at three locations at 1 mm spatial resolution. The custom S-type Pitot tube system resolved pressure differences of <100 Pa created by water flowing at 5–30 cm/s while providing a relatively low response time of ~300 s despite the small diameter (<1 mm) and long length (340 mm) of the Pitot tube needed to fit the HWTF geometry. Particle imaging velocimetry measurements in the central, viewable part of the HWTF confirmed the Pitot tube measurements in this region.     

Micro-rotary ratchets driven by migratory phytoplankton with phototactic stimulus

This study proposes micro-rotary ratchets driven by a migratory phytoplankton–Volvox, exhibiting a positive phototaxis. Two types of micro-discs, i.e., ratchet- and starfish-like ratchets are fabricated using conventional photolithography. The ratchet is floated in the center of a Petri dish filled with Volvox suspension under an optical microscope with halogen lamp illumination and is covered by a mask with a small hole so that the microorganisms are concentrated around the micro-ratchets by the phototaxis. Rotations of the ratchets with the same diameter of 0.567 mm were observed through a biological microscope; a rotation speed of 0.86 rpm for the micro-ratchet and 2.01 rpm for the starfish ratchet were obtained for a Volvox density of 1000–3000/mL under an illumination intensity of 0.18 W/cm². As the driving mechanism of the ratchet is based on the microorganisms adhesion to the ratchets surface rather than collision impacts, a gelatin coating on the ratchet was used to enhance the adhered number of Volvox. Although the drag force was increased owing to the larger ratchet diameter, a rotation speed of 0.16 rpm was observed. A particle tracking velocimetry measurement using polystyrene beads was performed to study the fluid flow around the micro-ratchet. A vortex generation by the micro-ratchets was confirmed; this effect may work as a micro-mechanical power booster for microorganisms. This drive system may open the possibility of a solar-power-driven and sustainable micro-mechanism using phytoplankton.     

Electrochemical determination of sulfite and phenol using a carbon paste electrode modified with ionic liquids and graphene nanosheets: Application to determination of sulfite and phenol in real samples

Benzoylferrocene was used to construct a modified-graphene paste electrode. Also, hydrophilic ionic liquid (n-hexyl-3-methylimidazolium hexafluoro phosphate) was used as a binder to prepare the modified electrode. The electro-oxidation of sulfite at the surface of the modified electrode was studied using electrochemical approaches. This modified electrode offers a considerable improvement in voltammetric sensitivity toward sulfite, compared to the bare electrode. Square wave voltammetry (SWV) exhibits a linear dynamic range from 5.0 × 10⁻⁸ to 2.5 × 10⁻⁴ M and a detection limit of 20.0 nM for sulfite. The diffusion coefficient and kinetic parameters (such as electron transfer coefficient and the heterogeneous rate constant) for sulfite oxidation were also determined. The prepared modified electrode exhibits a very good resolution between the voltammetric peaks of sulfite and phenol that makes it suitable for the detection of sulfite in the presence of phenol in real samples.     

1-N-alkyl -3-methylimidazolium ionic liquids as neat lubricants and lubricant additives in steel–aluminium contacts

The influence of the alkyl chain length and of the anion on the lubricating ability has been studied for the room-temperature ionic liquids (IL) 1-n-alkyl-3-methylimidazolium X⁻ [X = PF₆; n = 6 (L-P106). X = BF₄; n = 2 (L102), 6 (L106), 8 (L108). X = CF₃SO₃; n = 2 (L-T102). X = (4-CH3C6H4SO3); n = 2 (L-To102)]. Neat IL have been used for AISI 52100 steel-ASTM 2011 aluminium contacts in pin-on-disk tests under variable sliding speed. While all IL give initial friction values lower than 0.15, real-time sharp friction increments related to tribochemical processes have been observed for L102 and L-P106, at room-temperature and at 100 °C. Electronic microscopy (SEM), energy dispersive (EDS) and X-ray photoelectron (XPS) spectroscopies show that wear scar surfaces are oxidized to Al₂O₃ and wear debris contain aluminium and iron (for L102) fluorides. For L-P106, the steel surface is covered with a P-containing tribolayer. A change of anion (L-T102; L-To102) reduces friction and wear, but the lowest values are obtained by increasing the alkyl chain length (L106; L108). When the more reactive L102 and L-P106 are used as 1 wt.% base oil additives at 25 °C, tribocorrosion processes are not observed and a friction reduction (69–75% for 1 wt.% L102) and a change from severe (10⁻³ mm³ m⁻¹) to mild wear (10⁻⁴ to 10⁻⁶ mm³ m⁻¹) is obtained with respect to the neat IL. 1 wt.% IL additives also show good lubricating performance at 100 °C.