Very high cycle fatigue properties of high‐strength spring steel 60SiCrV7

The very high cycle fatigue properties of spring steel 60SiCrV7 for automotive suspension system with different hydrogen contents were studied by using ultrasonic fatigue testing and fatigue crack growth testing. The results show that the S–N curves exhibit continuous drop of fatigue lives and no obvious horizontal line exists. Similar fracture surface features were observed for all the specimens that failed mainly from internal inclusions with surrounding granular bright facet (GBF). Fatigue strength decreases remarkably with increasing hydrogen content. The applied stress intensity factor range at the periphery of GBF ΔK_GBF is approximately proportional to 1/3 power of the square of GBF area. The average values of ΔK_GBF for uncharged specimens are close to crack growth threshold ΔK_th, which indicates that ΔK_GBF could be regarded as the threshold value governing the beginning of stable fatigue crack propagation. The increase of hydrogen content tends to reduce ΔK_GBF.     

Very high cycle fatigue mechanism of carbide-free bainite/martensite steel micro-alloyed with Nb

In this study, the carbide-free bainite/martensite (CFB/M) steel was micro-alloyed with Nb (CFB/M-Nb). The very high cycle fatigue (VHCF) behaviors of this CFB/M-Nb steel were investigated by ultrasonic fatigue test. Especially, different microstructures of the CFB/M-Nb steel were deliberately designed to disclose the VHCF failure mechanism. In addition, the effect of hydrogen in the formation of the optical dark area (ODA) was analyzed, which was thought to control the formation of ODA by concentrating around interior inclusions. Results show the hydrogen cannot be considered to dominate the formation of ODA. Mostly important, “soft or coarsely soft structure induced fatigue crack” should be responsible for the primary VHCF failure mechanism of CFB/M-Nb steel.     

High‐cycle and very‐high‐cycle fatigue behaviour of a titanium alloy with equiaxed microstructure under different mean stresses

The fatigue behaviour of a titanium alloy Ti‐6Al‐4V with equiaxed microstructure (EM) under different values of tensile mean stress or stress ratio (R) was investigated from high‐cycle fatigue (HCF) to very‐high‐cycle fatigue (VHCF) regimes via ultrasonic axial cycling. The effect of mean stress or R on the fatigue strength of HCF and VHCF was addressed by Goodman, Gerber, and Authors' formula. Three types of crack initiation, namely, surface‐with‐RA (rough area), surface‐without‐RA, and interior‐with‐RA, were classified. The maximum value of stress intensity factor (SIF) at RA boundary for R < 0 keeps constant regardless of R in HCF and VHCF regimes. The SIF range at RA boundary for R > 0 also keeps constant regardless of R in VHCF regime, but this value decreases linearly with the increase of R for surface RA cases. The microstructure observation at RA regions gives a new result of nanograin formation only in the cases of negative stress ratios for the titanium alloy with EM, which is explained by the mechanism of numerous cyclic pressing.     

Very high cycle fatigue of VDSiCr spring steel under torsional and axial loading

Very high cycle fatigue (VHCF) properties of VDSiCr spring steel are investigated with ultrasonic equipment under fully reversed cyclic torsion loading and under cyclic axial loading at load ratios R = –1, R = 0.1 and R = 0.5. Shot‐peened specimens with surface finish similar to valve springs in combustion engines are tested until limiting lifetimes of 10¹⁰ cycles. Under cyclic torsion loading, specimens either fail below 10⁶ cycles with crack initiation at the surface or they do not fail. Under cyclic axial loading, failures above 10⁹ cycles were found for all load ratios with crack initiation at the surface or at internal inclusions. Ratio of mean endurance limit (50% failure probability at 10¹⁰ cycles) under fully reversed cyclic torsion and cyclic tension‐compression loading is 0.86. Cyclic torsion loading slightly below the endurance limit leads to cyclic softening first followed by cyclic hardening whereas cyclic stability is found for tension‐compression loading. Cyclic torsion reduces surface compression stresses whereas they are hardly affected by cyclic tension‐compression loading. Mean endurance limit at 10¹⁰ cycles for R = 0.1 is 61% of the endurance stress amplitude at load ratio R = –1, and for R = 0.5 it is 44% of the tension‐compression endurance limit. Endurance limits for cyclic torsion and cyclic tension‐compression loading are comparable, if effective stress amplitude is used that considers cyclic normal stresses and residual compression stresses at the surface.     

TC4钛合金的超高周疲劳行为及其竞争失效模型构建

针对现有模型对TC4竞争失效预测的不准确性,建立了基于最大应力强度因子的竞争失效模型。在室温以及两种应力比下,针对TC4钛合金进行超高周疲劳试验,通过试验与最弱键竞争失效理论相结合的方法进行评估,研究其超高周疲劳性能。通过对试样断口形貌的观察,可将其失效模式分为如下两类:表面失效以及内部失效。对试样表面缺陷以及内部解理刻面尺寸进行测量,并评估其最大应力强度因子值。进一步通过正态分布得到最大应力强度因子的累计分布函数,基于两参数泊松分布建立了与最大应力强度因子有关的竞争失效模型。通过模型计算结果,可以得出在任一最大应力强度因子下试样发生各种失效模式的概率,且经分析对比,本文中TC4两种疲劳失效模式的失效概率评估结果与试验数据吻合较好,为分析TC4钛合金超高周疲劳状态下的疲劳失效模式提出了新的评估方法。     

Cyclic torsion very high cycle fatigue of VDSiCr spring steel at different load ratios

Cyclic torsion fatigue tests with superimposed static torsion loads are performed with VDSiCr spring steel with shot-peened surface in the high cycle fatigue (HCF) and very high cycle fatigue (VHCF) regime. Fatigue properties are investigated at load ratios R = 0.1, R = 0.35 and R = 0.5 up to limiting lifetimes of 5 × 10⁹ cycles with a newly developed ultrasonic torsion testing method. Increasing the load ratio reduces the shear stress amplitude that the material can withstand without failure. Fatigue cracks are initiated at the surface in the HCF regime. In the VHCF regime, cracks are preferentially initiated internally in the matrix, below the surface layer with compression residual stresses, and less frequently at the surface. Cyclic and mean shear stresses with 50% survival probability in the VHCF regime are presented in a Haigh diagram. Linear line approximation delivers a mean stress sensitivity of M = 0.33 for load ratios between R = −1 and R = 0.5.     

Hydrogen-enhanced cracking of 2205 duplex stainless steel

Tensile and fatigue crack growth tests of 2205 duplex stainless steel (DSS) were performed in laboratory air, gaseous hydrogen at 0.2 MPa and saturated H₂S solution. The longitudinal specimen showed a lesser degradation of tensile properties than the transverse ones in saturated H₂S solution. The orientation of specimens with respect to rolling direction had little influence on the fatigue crack growth rate (FCGR) of the alloy in air. Furthermore, 2205 duplex stainless steel was susceptible to hydrogen‐enhanced fatigue crack growth. Transmission electron micrographs, in addition to X‐ray diffraction, revealed that the strain‐induced austenite to martensite transformation occurred near the crack surface within a rather narrow depth. Fatigue fractography of the specimens tested in air showed mainly transgranular fatigue fracture with a small amount of flat facet fracture. Furthermore, extensive quasi‐cleavage fracture of 2205 duplex stainless steel was associated with the hydrogen‐enhanced crack growth.     

Effect of submillimeter size holes on the fatigue limit of a high strength tool steel

The very high cycle fatigue and small fatigue crack growth behaviour of a generic tool steel material for diesel fuel injector application are described. The small crack growth tests for the tool steel material with and without the hardening heat treatment revealed the mechanisms of crack propagation and threshold behaviour. Based on the small fatigue crack propagation threshold value, an elastic plastic fracture mechanics methodology for the prediction of the endurance limit of specimens with submillimeter holes is proposed. The advantages of the new methodology are discussed in relation to existing methodologies for endurance limit prediction of specimens with small holes.     

Very high cycle fatigue of nitrided 18Ni maraging steel sheet

Thin sheets of nitrided 18Ni maraging steel are tested under cyclic tension (load ratio R = 0.1) in the very high cycle fatigue (VHCF) regime. The ultrasonic fatigue testing method with a cycling frequency of about 20 kHz has been further developed for these experiments. Sheet specimens with 0.35 mm thickness are mounted on a carrier specimen, they are pre-stressed and are forced to vibrate jointly. Between 10⁷ and 10⁹ cycles, fatigue cracks are initiated exclusively at internal TiN inclusions. The areas of the crack initiating inclusions projected perpendicular to the applied tensile stress are evaluated. The square root of inclusion areas, (area_INC)^1/2 lies between 2.5 μm and 5.3 μm. Considering inclusions as cracks, their stress intensity range is between ΔK_INC = 1.3 MPa m^1/2 and 2.4 MPa m^1/2. The sizes of crack initiating inclusions influence fatigue lifetimes. This is considered in a crack propagation model and by presenting lifetimes versus the stress amplitudes multiplied by (area_INC)^1/12. A mean lifetime of 10⁹ cycles is found at a stress amplitude of 22% of the tensile strength, which is comparable to other high strength steels tested under cyclic tension.     

Low cycle fatigue behaviour of dual-phase steel with different volume fractions of martensite

Completely reversed low cycle fatigue tests were carried out at a constant strain rate of 10^?2s^?1 on 3 mm thick sheet specimens of a dual-phase steel treated to give 1.5 to 28% martensite without changing the carbon content. Hysteresis loop shape, stress/strain response and plastic strain energy as a function of applied cycles are analysed for different microstructures. Strain/life and plastic strain energy per cycle ($\text{Δ}\text{W}\text{?}{}_{\mathrm{<mtext>p</mtext>}}$)/life (2N_f) plots are discussed in terms of microstructure. It is shown that during cycling the shape of the hysteresis loop continuously changes at lower volume fractions of martensite whereas it remains more or less constant for microstructures with a higher percentage of martensite. A Coffin-Manson type of plot between log ($\text{Δ}\text{W}\text{?}{}_{\mathrm{<mtext>p</mtext>}}$) and log (2N_f) is found to be applicable to test results of dual-phase steel with a wide range of martensite contents and is thus more versatile than the plot between log (Δ?_p/2) and log (2N_f) for predicting the fatigue life.     

Low cycle fatigue behaviour of a 1Cr-Mo-V steel with bainite and ferrite microstructure

A 1Cr-Mo-V turbine rotor steel forging, heat treated to obtain a bainite-20% ferrite microstructure, has been investigated for low cycle fatigue behaviour at room temperature and 535°C. In addition to establishing life expectancy curves, cyclic stress response and cyclic stress/strain curves were derived and the influence of time-dependent effects on high temperature low cycle fatigue life was also determined by introducing varying hold times at the peak tensile strain level of the fatigue cycle. The life expectancy curve obtained is comparable to that reported for the bainitic structure in this steel. Introduction of a dwell period of 5 min is found to reduce the low cycle fatigue life by a factor of 1.6.     

Effect of corrosive medium on fatigue crack growth behaviour and fracture in high martensite dual phase steel

Fatigue crack growth (FCG) behaviour in both near-threshold and higher stress intensity range (ΔK) in intercritically annealed dual-phase (DP) steel containing martensite between 32% and 76% in ferrite has been studied in 3·5% NaCl solution. It is shown that the amount of martensite content in dual phase steel has a significant effect on threshold (ΔK _th) values and FCG rates. Higher content of martensite in ferrite leads to higher threshold values and lower FCG rates. Further, ΔK _th is much higher in 3·5% NaCl solution as compared to that in laboratory air. Fractography studies reveal that in the near-threshold region, fracture surfaces are characterized mainly by intergranular cracking in corrosive (3·5% NaCl solution) environment. Higher threshold values in 3·5% NaCl solution is attributed to the higher crack closure induced by rougher fracture surface and by the strong wedge effects of corrosion products.     

On the relationship between fatigue limit,threshold and microstructure of a low-carbon Cr-Ni steel

The relationship between the fatigue limit stress range, Δσ_w, the threshold stress intensity factor, ΔK_th, and microstructure of low-carbon 12CrNi3A steel has been investigated. Non-propagating microcracks were observed on the surface of smooth specimens which has been subjected to at least 5 × 10⁶ cycles at the fatigue limit stress. The size of the cracks depended on the characteristic sizes of the microstructure of the material. Scanning electron microscopy showed that the fractographic characteristics in the near-threshold region of fatigue macrocrack growth were similar to those in the fatigue microcrack initiation region. This implies that the fatigue limit and fatigue threshold of the material have a similar physical meaning, both signifying the resistance of the material to the propagation of fatigue cracks. The relationship ΔK_th = 1.12Δσ_W √πα was shown to be valid, where a is a material parameter relating to microstructure, rather than to the length of a macrocrack. The results also showed that the value of a depends on the material and microstructure, and that both Δσ_W and ΔK_th will change if the microstructural characteristics of the material change.     

Morphologies and characteristics of deformation induced martensite during low cycle fatigue behaviour of austenitic stainless steel

Quantification, formation and nucleation micro-mechanisms of deformation induced martensite during low cycle fatigue behaviour of austenitic stainless steel have been investigated at various strain amplitudes tested at ambient temperature. The evolutionary deformation induced martensite has been quantified through magnetic measurement technique. It has been found that as strain amplitude increases, the volume fraction of deformation induced martensite increases. Extensive analytical transmission electron microscopy studies showed more than one nucleation site for martensitic transformation and the transformation micro-mechanisms have been observed to be: γ (fcc) → ? (hcp), γ (fcc) → α′ (bcc), γ (fcc) → deformation twins → α′ (bcc) and γ (fcc) → ? (hcp) → α′ (bcc).     

Deformation and microstructure evolution of a duplex stainless steel under out-of-phase thermo-mechanical fatigue

Abstract

Thermo-mechanical fatigue (TMF) of the duplex stainless steel SAF2205 (X2CrNiMoN22-5-3) was studied in the temperature range of 100–350°C. The tests were carried out on the duplex steel and on single-phase ferritic (X6Cr17, AISI 430) and austenitic steels (X2CrNiMo18-14-3, AISI 316L) similar to the two phases of the duplex steel for comparison. The mechanical behaviour of the three steels is analysed and discussed together with microstructural investigations by scanning electron microscopy, including electron backscatter diffraction and electron channelling contrast imaging.     

Initiation and propagation behaviour of fatigue cracks in hard-shot peened Type 316L steel in high cycle fatigue

Observations of fatigue crack growth behaviour were made during rotating‐bend testing of hard‐shot peened Type 316L steel. From the results of these observations, the crack that developed in the axial direction was observed and the mechanism of the fatigue crack properties was clarified as follows: (1) Small circumferential surface fatigue cracks were detected at 60% of the fatigue lifetime. These cracks propagated very slowly in both the circumferential and radial directions. (2) When a radial crack reached a depth of between 150 and 350 μm, axial fatigue cracks were formed. (3) In the next stage, either the radial or the axial fatigue cracks continued propagating, or an inwards growing radial crack formed from the axial crack. (4) In the final stage, the circumferential surface crack began to grow rapidly and resulted in fracture. (5) The fracture type of hard‐shot peened Type 316L is a particular type of surface fracture.     

Crack growth rates and microstructure feature of initiation region for very‐high‐cycle fatigue of a high‐strength steel

The S‐N data up to very‐high‐cycle fatigue (VHCF) regime for a high‐strength steel were obtained by fatigue tests under constant amplitude and variable amplitude (VA) via rotating bending and electromagnetic resonance cycling. Crack initiation for VHCF was from the interior of specimens, and the initiation region was carefully examined by scanning electron microscopy and transmission electron microscopy. Crack growth traces in the initiation region of fine‐granular‐area (FGA) were the first time captured for the specimens under VA cycling by rotating bending. The obtained crack growth rates in FGA were upwards to connect well with those in fish‐eye region available in the literature and were associated well with the calculated equivalent crack growth rates in FGA. The observations of profile samples revealed that FGA is a nanograin layer for the specimens under VA cycling, which is a new evidence to support the previously proposed “numerous cyclic pressing” model.     

Effect of small scale notches on the very high cycle fatigue of AISI 310 stainless steel

Fatigue behaviour of AISI 310 stainless steel has been investigated up to very high cycles. The fatigue crack initiation sites were found at the surface of the material. Persistent slip bands developed at the surface of the specimens led to the crack initiation. At lower stress levels, shallow persistent slip bands were found at the surface of the specimens, and the fatigue limit was obtained. Notched specimens showed lower fatigue lives. Notched specimens with higher stress concentration factor (K_t) showed higher fatigue strength reduction factor (K_f). It was found that shallow notches of depth ~100 µm may reduce the fatigue life substantially.     

Low cycle fatigue behaviour of duplex stainless steel: influence of isothermal aging treatment

The low‐cycle fatigue behaviour of a duplex stainless steel was comparatively studied in standard heat‐treated and isothermally aged (at 475 °C for 100 h) conditions by mechanical testing, scanning and transmission electron microscopy. It was established that fatigue life is longer in the aged condition as compared to the annealed condition at lower values of total strain amplitude Δ?/2 (Δ?/2 = 4.0 × 10^?3 and 6.0 × 10^?3) and becomes similar in annealed and aged conditions at Δ?/2 = 8.0 × 10^?3. Fatigue resistance of the material converges with increase in Δ?/2 values as a result of rapid cyclic softening of the ferritic phase in the aged condition.