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1.
研究了煤、煤灰、煤渣和土壤样品中^210Pb的测定方法,分析程序主要包括HCl浸取,阴离子交换分离,PbS沉淀纯化和^210Bi测量。分析10g煤时,检测限为7.6×10^-4Bq/g;分析5g煤灰,煤渣或土壤时,检测限均为1.5×10^-3Bq/g。测得煤、煤灰、煤渣和土壤样品中^210Pb含量分别为0.0316±0.0097、0.0712±0.0760、0.0109±0.0035和0.0355  相似文献   

2.
EDXRF法测定人发中Ca,Fe,Cu和Zn的含量   总被引:3,自引:1,他引:3  
本文介绍了国产管激发能量色散X射线荧光分析仪同时测定人发中Ca、Fe、Cu和Zn的分析方法。该方法采用在人发样品中加入内标元素Y,用化学法溶解人发,制成分析试样,用X射线荧光分析仪测定试样中的上述元素。此方法对这4种元素的检测限依次为7×l0 ̄(-6)、l×10 ̄(-6)、4×10 ̄(-6)和3×10 ̄(-6),其变异系数分别为6%、l%、2%和2%。  相似文献   

3.
费浩  唐邦福 《核动力工程》1994,15(4):357-360
本文介绍了电感合等离子体原子发射光谱法测定氧化钆中18种元素,经对元素光谱干扰和基体效应的探讨发现,当溶液中氧化钆浓度为5mg·mL^-1时,本法测定下限在6×10^-5~1×10^-3μg(g·Gd2O3)^-1之间。加入回收率在82%-109%之间;相对标准偏差优于±6.9%。  相似文献   

4.
在铜-邻菲罗啉-乙醇水溶液中,采用单纯形最优化方法选择出偶氮氯膦Ⅲ与钇的最佳显色条件。在实验条件下,钇的摩尔吸收系数为1.06×10^4m^2mol,且在0-0.6mg/l范围内服从比尔定律,变异系数为0.87%。用此方法测定了中子活化岩石样品^88Y的化学回收率。  相似文献   

5.
纪刚  郭勇 《辐射防护》1998,18(1):18-23
本文利用^60Coγ放射源和72cm×72cm×90cm(长×宽×高)体模,在大射野(10.0cm×10.0cm~50.cm×50.0cm)和大深度d(10.0~70.0cm)照射条件下实测的组织-空气比数据,按Melski计算^60Coγ射线组织-空气比深度函数公式,Ae^Bd+Ce^Dd,利用高斯-牛顿逐次逼近的计算方法,拟合出该公式参数A,B,C和D的最佳估计值,5组数据的残差平方和小于1.  相似文献   

6.
新丰中子核素^185Hf的研究:Ⅰ.合成,分离和鉴别   总被引:1,自引:1,他引:0  
用(n,2p)反应和快化分离法首次合成和鉴别了新丰中子同位素^185Hf。其半衰期为3.5±0.6min。另外,还观察到一条能量为164.5±0.5keV、半衰期为4.3±0.9min的属于^185Hf衰变的r射线。  相似文献   

7.
姜山  黄麒 《核技术》1993,16(12):720-725
描述了中国原子能科学研究院的基于HI-13串列加速器建立的加速器质谱计装置和测定^36Cl的实验方法。利用这台加速器质谱计测定^36Cl/Cl同位素原子比值的灵敏度已好于3×10×-15,对地下水,盐湖和铀矿石样品中的^31Cl进行了测定,这些样品的^36Cl/Cl同位素比为1.2×10×-12-2.2×10^-14。  相似文献   

8.
研究了煤、煤灰、煤渣和土壤样品中 ̄210pb的测定方法,分析程序主要包括HCl浸取、阴离子交换分离、PbS沉淀纯化和 ̄210Bi测量。分析10g煤时,检测限为7.6×10 ̄( ̄4)Bq/g;分析5g煤灰、煤渣或土壤时,检测限均为1.5×10 ̄( ̄3)Bq/g。测得煤、煤灰、煤渣和土壤样品中 ̄210pb含量分别为0.0316±0.0097、0.0712±0.0760、0.0109±0.0035和0.0355±0.0173Bq/g,对应的化学回收率依次为95.1%±2.5%、97.2%±2.0%、93.5%±1.6%和95.7%±1.5%。和煤中 ̄210pb含量相比,煤灰中 ̄210pb的浓集因子在1.60-11.8的范围。  相似文献   

9.
韦伦存  丁富荣 《核技术》1994,17(3):140-144
在本征型GaAs中注入2.0MeV(剂量1.0×10^15/cm^2)+2.9MeV(剂量1.1×10^15/cm^2)的^16O,使氧在约1.5-2.5μm之间形成均匀分布。注入样品分别经400-800℃、15min热退火后的电阻率测量表明,经500℃和600℃退火后的样品具有高的电阻率(~10^8Ω·cm);而当退火温度进一步升高时,其电阻率逐渐下降,并具有p型导电行为。沟道RBS分析表明,当  相似文献   

10.
同位素稀释质谱法测定气体样品中微量氦氖氩   总被引:2,自引:1,他引:1  
介绍了同位素稀释质谱法(IDMS)定量分析地下气体样品中的微量氦氖氩。介绍了稀释剂配制、标定、稀释剂与待测样品混合和同位素比值测量技术并进行了实验结果的误差分析。结果表明:体积分数为10 ̄(-6)、10 ̄(-5)、10 ̄(-4)时,不确定度分别约为±3%、±2%、±2%。  相似文献   

11.
The stopping powers of Be, Al, Ti, V, Fe, Co, Ni, Cu, Zn, Mo, Rh, Ag, Sn, Ta, Pt and Au for 6.5 MeV have been measured using a surface barrier silicon detector. The accuracy of the results is ± 0.3%. The detail of the experimental procedures is described. The results have been compared with the Risø data and the Aarhus data of Andersen et al. The present results for Al, Cu and Ag agree very well with the Aarhus results at 6.5 MeV. The mean excitation energy has been extracted from the present results using the Bonderup shell correction, the Barkas correction and the Bloch correction. The parameters x and b which appear in the Bonderup shell correction and the Barkas correction have been newly determined as x = 1.358 and b = 1.3. The present mean excitation energy agrees very well with the I values obtained by other authors. It has been confirmed that the Bonderup shell correction is quantitatively correct for 6.5 MeV protons.  相似文献   

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Wavelengths, transition probabilities, and oscillator strengths have been calculated for M-shell electric dipole transitions in Co-, Ni-, Cu-, Zn-, Ga-, Ge-, and Se-like Au ions. The fully relativistic multiconfiguration Dirac–Fock method, taking quantum electrodynamical effects and the Breit correction into account, was used in the calculations. Calculated energy levels of M-shell excited states for Cu-, Zn-, Ga-, Ge-, and Se-like Au ions from the method were compared with available theoretical and experimental results, and good agreement with them was achieved.  相似文献   

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19.
The results of calculations of the level constants in the elements Pd, Os, Ir, Mo, I, In, Ta, Th, U238 are presented; the cross sections for these elements have been published earlier. New measurements for the cross sections in Ir, Th, U238 are cited. The measurements were made with a mechanical-chopper spectrometer with a resolution of 0.08 sec/m in the energy region from 4.5 to 10,000 ev. The integrated and differential curves for the distribution of neutron widths in these elements are plotted.Presented at the International Conference on Nuclear Reactions in Amsterdam (June 1956).The authors take this opportunity to express their gratitude to U. Chi-Kwa and Suan Chi-Ling for their assistance in the mathematical analysis of the experimental results, G. M. Kukavadze for the mass-spectro-graphic analyses of the samples, V. N. Bovinoi and M. P. Anikinoi for providing the chemical analyses and A. I. Ermakov, N. S. Rezvyakov, G. V. Rukolaine and K. A. Trostinoi for help in building the analyzer and in carrying out the measurements.  相似文献   

20.
Currently, thirty-one dysprosium, thirty-two holmium, thirty-two erbium, thirty-three thulium, and thirty-one ytterbium isotopes have been observed and the discovery of these isotopes is described here. For each isotope a brief synopsis of the first refereed publication, including the production and identification method, is presented.  相似文献   

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