Shrinkage of steel fibre reinforced cement composites

The paper presents results of an experimental investigation on the influence of steel fibres on the free shrinkage of cement-based matrices. Shrinkage tests were carried out on cement paste, mortar and two types of concrete mixes for a period of up to 520 days. Melt extract, crimped and hooked steel fibres were used for reinforcement at volume fractions ranging between 1 and 3%. The results indicate that fibres restrain the shrinkage of the various cement matrices to a significant extent, resulting in reductions of up to 40%. Crimped fibres are the most efficient in providing shrinkage restraint. The paper also presents a theoretical expression and an empirical expression which can be used to predict shrinkage strains of steel fibre reinforced cement matrices. The analysis requires a knowledge of the values of coefficient of friction, μ, at the fibre-matrix interface, which are also derived in this paper. The μ values for steel fibres in normal concrete, mortar and cement paste range between 0.07 and 0.12.     

A simple material model for unidirectionally aligned fibre reinforced composites

A material model for the nonlinear behaviour of composite materials is proposed. The model combines the linear elastic fibre properties with the nonlinear behaviour of the matrix in order to obtain the average properties of the composite. The interaction between the fibre and the matrix is considered using stress partitioning factors, which are based on the experimental behaviour of the material.     

Carbon fibre-cement adhesion in carbon fibre reinforced cement composites

The addition of small amounts of short carbon fibres to cement causes a great increase in the composite material toughness and tensile, flexural, and impact strength. In order to understand how cement properties are improved by carbon fibres and to understand the level of adhesion and interfacial failure mode which are necessary to obtain optimum carbon fibre reinforced cement (CFRC) properties, various admixtures were included in cement and CFRC. Their effects on the carbon fibre-cement adhesion and the composite material properties were determined using fibre pull-out and composite material flexural tests. The addition of latex to CFRC, and hot water curing of CFRC dramatically increase fibre-matrix adhesion. Both latex (with an anti-foam agent) and hot water curing increase flexural strength by 40% over adhesion changes the failure mode from fibre pull-out to fibre rupture. Optimum strength and toughness of CFRC result from an intermediate level of fibre-matrix adhesion.     

Compression creep behaviour of steel fibre reinforced cement composites

The paper presents the results of an experimental investigation to determine the influence of steel fibre reinforcement on the creep of cement matrices under compression. Creep tests were carried out at a number of applied stress-strength ratios ranging between 0.3 to 0.9. Melt extract and hooked steel fibres were used at volume fractions ranging between 0 and 3% by volume of a mix. Three types of cement matrices were used namely cement paste, mortar and two mix proportions of concrete. The results indicate that steel fibres restrain the creep of cement matrices at all stress-strength ratios, the restraint being greater at lower stresses and at higher fibre contents. Steel fibres are effective in restraining only the flow component of creep of cement matrices, the delayed elastic component being unaffected. The reduction in creep of cement pastes, due to fibre reinforcement, is much greater than that for mortar or concrete matrices. Mathematical expressions are given for the creep of steel fibre reinforced cement matrices.

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Résumé Cet article présente les résultats d’une étude expérimentale en vue de déterminer l’influence du renforcement de fibres d’acier sur le fluage de matrices de ciment en compression. On a exécuté les essais de fluage à un certain nombre d’intervalles correspondant à des rapports contrainte/déformation allant de 0,3 à 0,9. On a utilisé des fibres d’acier dans des proportions se situant entre 0 et 3% par volume de mélange, et on s’est servi de trois types de matrices de ciment: pate de ciment, mortier et béton selon deux dosages. Les résultats montrent que les fibres d’acier empêchent le fluage des matrices de ciment dans tous les rapports de contrainte/déformation, l’effet étant plus important pour les contraintes faibles et les teneurs en fibres plus élevées. Les fibres d’acier n’agissent qu’en s’opposant à la déformation plastique des matrices de ciment sans que l’élasticité différée en soit affectée. La diminution du fluage des pates de ciment due au renforcement des fibres est beaucoup plus importante que pour le mortier ou les matrices de béton. On donne des formules mathématiques pour le fluage des matrices de ciment renforcé de fibres d’acier.

     

Investigation of mixed-mode fracture of aligned steel fibre reinforced cementitious composites

International Journal of Fracture - Mixed-mode fracture experiments were conducted on aligned steel fibre reinforced cementitious composite (ASFRC) and ordinary steel fibre reinforced cementitious...     

Plant-based natural fibre reinforced cement composites: A review

The quest for sustainability in construction material usage has made the use of more renewable resources in the construction industry a necessity. Plant-based natural fibres are low cost renewable materials which can be found in abundant supply in many countries. This paper presents a summary of research progress on plant-based natural fibre reinforced cement-based composites. Fibre types, fibre characteristics and their effects on the properties of cement-based materials are reviewed. Factors affecting the fresh and hardened properties of cement-based composites reinforced with plant-based natural fibre are discussed. Measures to enhance the durability properties of cement-based composites containing plant-based natural fibres are appraised. Significant part of the paper is then focused on future trends such as the use of plant-based natural fibres as internal curing agents and durability enhancement materials in cement-based composites. Finally, applications and recommendations for future work are presented.     

Dynamic mechanical properties of short sisal fibre reinforced polypropylene composites

The dynamic mechanical properties of short sisal fibre reinforced polypropylene composites containing both untreated and treated fibres have been studied with reference to fibre loading, fibre length, chemical treatments, frequency and temperature. By the incorporation of short sisal fibre into polypropylene, the storage moduli (E′)and loss moduli (E″) have been found to be increasing whereas the mechanical loss factor (tan δ) decreasing. The storage modulus decreases with increase in temperature. The treated fibre composites show better properties compared to untreated system. The Arrhenius relationship has been used to calculate the activation energy for the glass transition. The use and limitations of various theoretical equations to predict the tan δ and storage modulus of the fibre reinforced plastic composites have been discussed. Cole–Cole analysis has been carried out to understand the phase behaviour of the composite samples. A master curve for the modulus of the blend is drawn by applying the time–temperature super position principle.     

The theoretical prediction of the cracking stress of glass fibre reinforced inorganic cement

Glass fibre-reinforced inorganic cement is increasingly being seen as a promising new building material. For any structural use, its cracking stress will be significant because of its resemblance to the yield point of mild steel. In this paper, the use of fracture mechanics to formulate a prediction of the cracking stress is proposed. Experimental evidence is also presented in support of this theory.     

Crystallization of carbon fibre reinforced polypropylene

Polypropylene (PP) was compounded with carbon fibre of various contents (0, 5, 10, 15, 20 vol%) using a single and a twin screw extruder. The influence of both the carbon fibre content and the compounding method on the thermal behaviour and characteristics of crystallization was studied using differential scanning calorimetry (DSC), polarizing optical microscopy and scanning electron microscopy (SEM). Melting and crystallization temperatures increased with the amount of carbon fibre. Isothermal crystallization was observed using DSC and it was found that crystallization was accelerated by the presence of carbon fibres. Using polarizing optical microscopy, it was found that the nucleation of polypropylene started at the crossing point of two or more fibres.     

Stress-corrosion cracking and its propagation in aligned short-fibre composites

Stress-corrosion tests are conducted on aligned short-fibre composites to assess their performance in both air and 1 N H₂SO₄ environments. The materials used are 3 mm E-glass, AS4 carbon, and their hybrid fibre reinforced epoxy composites. Several crack propagation models are developed to describe different cracking behaviour; the observed composite fracture modes verify these proposed models. Pre-immersion has significant effects onK _l-t _f and crack arrest of hybrid composites. A comparison of theoretical and experimentalK _l-t _f curves indicates good agreement of time to failure. The present research has quantified the susceptibility of these composites to environmental attack.     

Characterisation of interphase nanoscale property variations in glass fibre reinforced polypropylene and epoxy resin composites

The local microstructure can be altered significantly by various fibre surface modifications, causing property differences between the interphase region and the bulk matrix. By using tapping mode phase imaging and nanoindentation tests based on the atomic force microscope (AFM), a comparative study of the sized fibre surface topography and modulus as well as the local mechanical property variation in the interphase of E-glass fibre reinforced epoxy resin and E-glass fibre reinforced modified polypropylene (PPm) matrix composites was conducted. The phase imaging AFM was found a highly useful tool for probing the interphase with much detailed information. Nanoindentation experiments indicated the chemical interaction during processing caused by a gradient profile in the modulus across the interphase region of γ-aminopropyltriethoxy silane (γ-APS) and polyurethane (PU)-sized glass fibre reinforced epoxy composite. The interphase with γ-APS/PU sizing is much softer than the PPm matrix, while the interphase with the γ-APS/PP sizing is apparently harder than the matrix, in which the modulus was constant and independent of distance away from the fibre surface. The interphase thickness varied between less than 100 and ≈300 nm depending on the type of sizing and matrix materials. Based on a careful analysis of ‘boundary effect’, nanoindentation with sufficient small indentation force was found to enable measuring of actual interphase properties within 100 nm region close to the fibre surface. Special emphasis is placed on the effects of interphase modulus on mechanical properties and fracture behaviour. The interphase with higher modulus and transcrystalline microstructure provided simultaneous increase in the tensile strength and the impact toughness of the composites.     

Fibre spacing in steel fibre reinforced composites

A method is presented which makes it possible to evaluate the fibre content or to estimate the distribution of fibres in steel fibre reinforced composite materials from the analysis of X-ray pictures. The basic notion in this method is an apparent fibre spacing defined as the average spacing between the intersections of individual fibre projections upon a certain plane and an arbitrary base line drawn on that plane. Such apparent spacing may be estimated analytically, it may also be measured directly on the radiogram. The comparison of analytical and experimental data shows satisfactory agreement.

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Résumé On présente une méthode qui, par l'analyse des diagrammes de rayons-X, permet d'évaluer la teneur en fibre ou d'estimer leur distribution dans des composites renforcés de fibres d'acier. On suppose que la distribution des fibres est homogène et isotropique, toutes les fibres ayant même longueur et même diamètre. En tant que notion de base de cette méthode, on définit un espacement de fibres apparent comme l'espacement moyen entre d'une part les intersections des projections des fibres individuelles, et d'autre part une ligne de base arbitraire tracée sur le même plan. Un tel espacement apparent (s _{app. anl.} ) peut être évalué analytiquement comme une fonction de la longueur de la fibre (l), du diamètre (d) de la teneur en volume (β) et de l'épaisseur de l'échantillon (w)-équation (7). On peut aussi le mesurer directement sur le radiogramme commes _{app. exp.} [voirfig. 2, équation 12)]. La comparaison des résultats analytiques et expérimentaux (tableau I) montre une bonne concordance. On peut aussi se servir de la méthode pour évaluer l'épaisseur d'échantillons soumis aux rayons-X, ce qui prouverait une bonne lisibilité du radiogramme.

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