Drying Characteristics of Porous Materials in a Fluidized Bed under Reduced Pressure

Abstract

The drying of porous materials immersed in the fluidized bed under reduced pressure was performed, and the results were compared with those of hot air drying. The pressure in drying chamber was changed (5.0–101.3 kPa) and the effect of it was examined.

The temperature of the sample center becomes lower as the pressure in drying chamber decreases, and the temperature in fluidized-bed drying is higher than that in hot air drying at the same pressure. The effect of pressure in drying chamber on the sample temperature is significant for different temperatures of drying gas.     

Effect of Fluidizing Particle on Drying Characteristics of Porous Materials in Superheated Steam Fluidized Bed under Reduced Pressure

The hygroscopic porous particle was used as the fluidizing particle for the superheated steam fluidized bed drying under reduced pressure. A relatively large material was immersed in the fluidized bed as the drying sample. The drying characteristics of the sample were examined experimentally and the results were compared with those in the case of inert particle fluidized bed.

The water transfer from the sample to the fluidizing particle bed in the case of hygroscopic porous particle facilitated the drying regardless of pressure and temperature in the drying chamber. The increment degree of the sample temperature at the earlier period of drying was smaller in the case of hygroscopic porous particle than in the case of inert particle, and the phenomenon was more remarkable in the case of superheated steam than in the case of hot air.     

Effect of Fluidizing Particle on Drying Characteristics of Porous Materials in Superheated Steam Fluidized Bed under Reduced Pressure

The hygroscopic porous particle was used as the fluidizing particle for the superheated steam fluidized bed drying under reduced pressure. A relatively large material was immersed in the fluidized bed as the drying sample. The drying characteristics of the sample were examined experimentally and the results were compared with those in the case of inert particle fluidized bed.

The water transfer from the sample to the fluidizing particle bed in the case of hygroscopic porous particle facilitated the drying regardless of pressure and temperature in the drying chamber. The increment degree of the sample temperature at the earlier period of drying was smaller in the case of hygroscopic porous particle than in the case of inert particle, and the phenomenon was more remarkable in the case of superheated steam than in the case of hot air.     

Drying Characteristics of Carrots Immersed in a Fluidized Bed of Fluidizing Particles Under Reduced Pressure

The drying characteristics and properties (color and shrinkage) of carrots (as a representative agricultural product) were experimentally examined in a fluidized bed under reduced pressure. Dry hot air and superheated steam were used as the drying gases. Rice and carrot powders (0.125–0.355 mm in diameter) were used as the fluidizing particles, in addition to glass beads (0.12 mm in diameter).

It was confirmed that the drying rate using a fluidized bed was much higher than without a fluidized bed (hot-air drying), regardless of the type of fluidizing particles used. Under reduced pressure, both with and without a fluidized bed, the drying rate was higher than that at atmospheric pressure using hot air. The drying rate was sufficiently high for fluidized-bed drying with superheated steam, though the drying rate was higher with hot air than with superheated steam. As the drying temperature increased, the volume ratio (befor/after drying) of the sample increased. At high drying temperatures (373 and 423 K in the present study), the color of the sample changed; in other words, a heat-induced change in the properties of the carrot was observed. At a low drying temperature (333 K in the present study), the drying method did not affect the color of the carrot; i.e., the color of the dried material was maintained even in a fluidized bed under reduced pressure when the drying rate was higher.     

Effect of Humidity on Drying of Porous Materials in Fluidized Bed under Reduced Pressure

For fluidized bed drying under a reduced pressure, the effect of the humidity of the drying gas on the drying characteristics of porous materials immersed in the bed was examined experimentally and theoretically. The temperature at the sample center increased with the humidity at relatively high pressures in the drying chamber (101.3 and 50 kPa), and the degree of the increment in the temperature with the humidity increased with the chamber pressure. The effect of the humidity on the temperature at the sample center and the drying time was insignificant at a relatively low chamber pressure (20 kPa).     

Drying Suspensions in a Pulsed Fluidized Bed of Inert Particles

The drying of carbohydrate suspensions on polypropylene particles in a pulsed fluidized bed was studied by means of a 2⁵ experimental design, to determine the effect of the air flow and temperature, suspension flow rate, and free section and rotating speed of the rotary plate on the Nusselt number, the moisture content of the product, and the percentage of solids retained inside the bed (which were minimized to 4.9 and 14.4%, respectively) with an air flow of 600 m³/h at 90°C and 720 mmHg, a suspension flow rate of 6 L/h, and a plate with 6% free section, rotating at 50 rpm.

Additionally, the effects of temperature, air flow, and suspension flow rate on the residence time distribution (RTD) were determined, using the stimulus-response methodology. The RTD was represented by 1.1 to 2 tanks in series, according to this model. The mean residence time of the dried carbohydrate particles was between 5.4 and 8.2 min.

Finally, an egg suspension could be dried at 4 L/h, with air at 90°C, with a mean residence time about 50% longer that that found for drying carbohydrate suspensions.     

Drying Suspensions in a Pulsed Fluidized Bed of Inert Particles

The drying of carbohydrate suspensions on polypropylene particles in a pulsed fluidized bed was studied by means of a 2⁵ experimental design, to determine the effect of the air flow and temperature, suspension flow rate, and free section and rotating speed of the rotary plate on the Nusselt number, the moisture content of the product, and the percentage of solids retained inside the bed (which were minimized to 4.9 and 14.4%, respectively) with an air flow of 600 m³/h at 90°C and 720 mmHg, a suspension flow rate of 6 L/h, and a plate with 6% free section, rotating at 50 rpm.

Additionally, the effects of temperature, air flow, and suspension flow rate on the residence time distribution (RTD) were determined, using the stimulus-response methodology. The RTD was represented by 1.1 to 2 tanks in series, according to this model. The mean residence time of the dried carbohydrate particles was between 5.4 and 8.2 min.

Finally, an egg suspension could be dried at 4 L/h, with air at 90°C, with a mean residence time about 50% longer that that found for drying carbohydrate suspensions.     

Drying Characteristics In Superheated Steam Drying at Reduced Pressure

Abstract

The superheated steam drying at reduced pressure is performed, and the effects of operational conditions such as drying pressure and temperature on the drying characteristics are examined. In order to obtain the basic guideline for the design of the superheated steam dryer at reduced pressure, the heat flux to sample was calculated and the optimal conditions were estimated.

After the sample temperature reached at the boiling point, the temperature was maintained at the boiling point and the drying rate became almost constant. Once the sample was dried out, the temperature suddenly increased up to the drying gas temperature. From the calculation of combined heat flux, the followings were found. The contribution of radiative heat transfer to the combined heat flux became larger as the drying pressure was lower. The combined heat flux had a maximum value against the drying pressure. The optimum drying pressure, which gave the maximum heat flux, became lower as the drying gas temperature decreased. It was found that reduction in the drying pressure is effective for the enhancement in drying performance.     

Drying Characteristics In Superheated Steam Drying at Reduced Pressure

The superheated steam drying at reduced pressure is performed, and the effects of operational conditions such as drying pressure and temperature on the drying characteristics are examined. In order to obtain the basic guideline for the design of the superheated steam dryer at reduced pressure, the heat flux to sample was calculated and the optimal conditions were estimated.

After the sample temperature reached at the boiling point, the temperature was maintained at the boiling point and the drying rate became almost constant. Once the sample was dried out, the temperature suddenly increased up to the drying gas temperature. From the calculation of combined heat flux, the followings were found. The contribution of radiative heat transfer to the combined heat flux became larger as the drying pressure was lower. The combined heat flux had a maximum value against the drying pressure. The optimum drying pressure, which gave the maximum heat flux, became lower as the drying gas temperature decreased. It was found that reduction in the drying pressure is effective for the enhancement in drying performance.     

Drying Characteristics of Coriander Seed Particles in a Reduced Pressure Superheated Steam Fluidized Bed

Drying characteristics of coriander seed particles were experimentally analyzed in a reduced pressure superheated steam fluidized bed. The typical moisture gain, reported in some other studies during the warm-up period of the process, was reduced in most of the cases by supplying additional heat into the column. The experimental results demonstrated that the drying rate increases and the equilibrium moisture content decreases by increasing the operating temperature. However, variation of the operating pressure (40–67 kPa) and the superficial steam velocity (2.3–4.0 m/s) did not present significant effects on the moisture contents. The degree of superheating was found to be the most important parameter for the process. The experiments also showed that the equilibrium moisture content decreases upon increasing the degree of superheating. Finally, employing a reduced pressure superheated steam fluidized bed appears as an option to carry out drying processes at relatively lower temperatures.     

Mathematical Modeling of the Fluidized Bed Drying of Cubic Materials

The unsteady‐state simultaneous heat and mass transfer between gas and potato cubes during the drying process in a batch fluidized bed was described by a mathematical model. Mass transfer was considered to occur in three dimensions whereas heat transfer between the gas and dried material was assumed to be lumped. It was found that the model could describe the drying process with acceptable accuracy. The moisture profile inside the material at any cross‐section and at any time can be predicted by the model.     

Drying and Heat Transfer Characteristics for a Novel Fluidized Bed Dryer

Abstract

The use of a fluidized bed dryer with a lateral air flow and mechanical agitation to the drying of sludge from a wastewater treatment plant was investigated. Experimental curves of moisture content vs. drying time, as well as heat transfer coefficients and the size characteristics of the products, were determined at temperatures between 80°C and 110°C, a stirring rate of 55 rpm and air velocity of 0.9 m/s for 3 kg sludge batches with initial moisture contents of 0.55 and 0.65 (d.b.). Experimental drying kinetics were compared with values derived from three models based on Fick's second law, namely: the constant diffusivity model, the simplified variable diffusivity model, and the modified quasi-stationary model.     

Drying Efficiency of Indonesian Lignite in a Batch-Circulating Fluidized Bed Dryer

This research explores the production of low-moisture, high-rank coal using a batch-type, laboratory-scale, circulating fluidized bed to dry low-rank Indonesian coal with a high moisture content of 35 wt%. The operation was performed using air as a fluidization gas in a riser (a 4-m-tall pipe with an inner diameter of 0.04 m) at a gas velocity ranging from 2.0 to 2.7 m/s and a riser temperature of 80 to 150°C. The electric heaters were installed in the upper part of a downcomer to prevent the condensation of the evaporated moist- ure. The drying rate of the coal was investigated in terms of the inlet gas temperature, the gas velocity, and the drying time in order to determine the optimum operating conditions. Changes in the moist- ure content of the coal, before and after the experiments, were char- acterized by a proximate analysis, an ultimate analysis, the higher heating value (HHV), the lower heating value (LHV), a particle size analysis, and by the equilibrium moisture content. The results show that 70 to 80 wt% (wet basis, wb) of the total moisture can be reduced when the gas velocity of the riser is 2.0 m/s and the gas temperature is 150°C. In experiments, a simple mathematical model based on the heat and mass balances and a thin-layer drying model were simul- taneously used to predict the drying behavior of coal under the given operating conditions. The results of the model are similar to those of the experiment.     

Batch Drying Kinetics in a Two-Zone Bubbling Fluidized Bed

This article deals with investigation and modeling of batch drying process of solids in fluidized bed apparatus. There has been used model of fluidized bed drying, which consists two zones: emulsion zone and bubbling zone with taking into consideration the presence of solid particles in the bubbles. The results of theoretical expectations that arise from simulation calculations have been verified with experimental data obtained with the use of fluidized bed dryer 0.225 m in diameter. A drying process of silica gel, sand, and ammonium sulfate has been tested. To verify the model, the concept of a generalized drying curve has also been employed.     

Drying of Suspensions in a Fluidized Bed of Inert Particles Under Reduced Pressure

A drying method in which a heat-sensitive material is immersed in a fluidized bed under reduced pressure was used to continuously obtain dispersed, dry, fine powders of that material from a dilute suspension or solution at a low temperature with a high drying rate. The mass velocities of the drying gas, sample flow rate, and chamber pressure were varied, and the effects of these variations on the corresponding drying characteristics were examined.

The fluidization state of a fluidized bed of inert particles strongly affects the drying rate in the bed and has a greater effect than the chamber pressure on the corresponding drying characteristics. In other words, it is important to maintain a vigorous fluidization state to achieve a high drying rate. Although the maximum drying rate is independent of the chamber pressure, it can be achieved at a low mass velocity of the drying gas under reduced pressure. That is, at a low chamber pressure a high drying rate can be achieved, even at a relatively low mass velocity of the drying gas. The bed temperature at the time of drying is strongly influenced by the drying rate and decreases linearly with an increase in the maximum drying rate when the sample flow rate is equal to the drying rate.     

Vacuum Drying of Porous Solids under Supercooling

Vacuum drying of sintered glass beads, cemented glass balloons, and baked clay was investigated under supercooling. Glass beads and glass balloons, which were made of a common glass material, were used for comparison. Concerning sintered glass beads, there was no effect of supercooling on drying rates at a pressure of 0.93 kPa. In cemented glass balloons as well as in baked clay, however, a prominent peak of drying rates emerged in drying rate curves and at the same time, a stepwise increase in the surface temperature appeared under supercooling at a pressure of 1.19 kPa; no peak of drying rates emerged in drying rate curves of sintered glass beads. The total amount of latent heat of vaporization and sensible heat generated at the peak of drying rates was 39–59% of the latent heat of solidification. A part of the latent heat of solidification evaporated the water in the sample, producing a peak of drying rates as well as a stepwise increase in the surface temperature of the sample.     

Vacuum Drying of Porous Solids under Supercooling

Vacuum drying of sintered glass beads, cemented glass balloons, and baked clay was investigated under supercooling. Glass beads and glass balloons, which were made of a common glass material, were used for comparison. Concerning sintered glass beads, there was no effect of supercooling on drying rates at a pressure of 0.93 kPa. In cemented glass balloons as well as in baked clay, however, a prominent peak of drying rates emerged in drying rate curves and at the same time, a stepwise increase in the surface temperature appeared under supercooling at a pressure of 1.19 kPa; no peak of drying rates emerged in drying rate curves of sintered glass beads. The total amount of latent heat of vaporization and sensible heat generated at the peak of drying rates was 39-59% of the latent heat of solidification. A part of the latent heat of solidification evaporated the water in the sample, producing a peak of drying rates as well as a stepwise increase in the surface temperature of the sample.     

Drying of Potato Slices in a Pulsed Fluidized Bed

This article presents experimental and modeled drying kinetics of potato slices of the Desiree variety (9 × 9 × 3 mm³) in a pulsed fluid bed as a function of the air velocity, air temperature, and rotating disk velocity of the pulse generator. A statistical multifactor experimental design (2³) was applied to analyze the drying process with two levels each of drying temperature, air velocity, and rotating disk velocity. The results showed that the significant factors were air temperature, air velocity, rotating disk velocity, and the binary interactions of air velocity with both the temperature and the rotating disk velocity. The simplified variable diffusivity model (SVDM) gave the least deviation for the experimental data. The effective diffusivity values determined in this work are similar to those reported in the literature.     

Drying of Potato Slices in a Pulsed Fluidized Bed

This article presents experimental and modeled drying kinetics of potato slices of the Desiree variety (9 × 9 × 3 mm³) in a pulsed fluid bed as a function of the air velocity, air temperature, and rotating disk velocity of the pulse generator. A statistical multifactor experimental design (2³) was applied to analyze the drying process with two levels each of drying temperature, air velocity, and rotating disk velocity. The results showed that the significant factors were air temperature, air velocity, rotating disk velocity, and the binary interactions of air velocity with both the temperature and the rotating disk velocity. The simplified variable diffusivity model (SVDM) gave the least deviation for the experimental data. The effective diffusivity values determined in this work are similar to those reported in the literature.     

Plasma Nitriding of Titanium Particles in a Fluidized Bed Reactor at a Reduced Pressure

A fluidized bed reactor operated at a reduced pressure is used to modify the surface property of particles. Titanium particles of 46- to 74-μm diameter are fluidized by a nitrogen gas flow of 0.35 cm³-std/s at a pressure of about 100 Pa, and a nitride layer is formed with the assistance of a radio-frequency plasma discharge. Modified particles are characterized with elementary analysis and XPS. The nitriding rate is enhanced by the presence of the nitrogen plasma, and the kinetics obey a parabolic law.