共查询到18条相似文献,搜索用时 62 毫秒
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采用三氧化二铟和真空蒸发法制得的纳米锡粉为原料,溶解在一定浓度的氢氧化钠溶液中,水热条件下成功的合成了纳米级的铟锡氧化物粒子,通过粉末X射线衍射(XRD),场发射扫描电子显微镜(FE-SEM),透射电子显微镜(TEM)和紫外可见光光吸收光谱(Uv-Vis)等手段对所得产物进行表征。讨论了反应时间、pH值因素对产物成分和形貌的影响。结果表明:在温度为180℃,10mol/L NaOH溶液的条件下,水热反应36h得到比较均一的产物In1.94Sn0.06O3,产物形貌为均匀的六面体,大小在100nm左右,且对波长在200-400nm的光有强烈的吸收。 相似文献
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以InCl_3·4H_2O和SnCl_2·2H_2O为原料,水为溶剂溶解作为前驱体溶液,采用微波管式炉加热联合超声波喷雾热解法制备得到ITO粉体。实验研究了不同微波热解温度和添加柠檬酸对ITO产品的微观形貌的影响,利用TG-DSC、XRD、SEM、EDS、TEM对样品的结构特征和微观形貌进行了表征分析。研究结果表明,前驱液浓度、温度和添加剂是影响氧化铟锡(ITO)粉体形貌的关键因素。得到粒径较小、分散性好和形貌呈球形的超细粉体的最佳条件为:温度650℃,前驱体原溶液浓度0.01mol/L,柠檬酸浓度0.004mol/L,载气速率0.6L/min,加入200目滤网。 相似文献
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利用微波辅助-水相共沉淀法,在InCl3和SnCl4混和溶液中添加PEG-6000,并滴加体积比1∶4浓度的氨水,并在不同反应温度(35~75℃)下制备了ITO前驱体,在温度800℃煅烧1h后得到纳米ITO粉体。利用SEM对纳米ITO粉体的形貌进行表征,用XRD对其结构、晶粒度和堆垛层数进行了表征,同时用纳米粒度Zeta电位分析仪对相应颗粒度进行了测试。讨论了微波辅助下不同反应体系温度对制备的纳米ITO粉体的形貌和尺寸的影响,并探讨了其机理,研究结果表明,随着反应体系温度的上升,纳米ITO粉体形貌由球形转为棒形,其晶体结构不变,晶粒粒径和颗粒度随着增大;反应体系温度的升高使纳米ITO晶粒不同晶面的晶粒度不同程度地增大,以及不同晶面垂直方向晶面不同程度地增多,是球形ITO晶粒成为棒形ITO晶粒的基础。 相似文献
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以Zn(NO3)2.6H2O、NaOH和聚乙二醇(PEG,Mn=2000)为原料,采用微波水热法制备了结晶性能良好的ZnO纳米棒及其3D组装结构。利用EDS、XPS、SEM、TEM、FTIR对样品进行了表征,结合光致发光(PL)谱研究了样品的PL性能,并对ZnO纳米棒及其3D组装结构的生长机理进行了简要分析。结果表明,ZnO纳米棒的直径约为300nm,长径比约为3,3D组装结构的直径约为2μm,ZnO纳米棒及其3D组装结构的生长可能与PEG模板的导向作用有关。PL谱表明样品在413~464nm内有很强的蓝光发射特性,这与样品的微观结构有很大关系。 相似文献
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采用微波水热法合成了纳米晶钛酸锶钡(Ba0.5Sr0.5TiO3)粉体,通过XRD、TEM、SEM等分析手段表征粉体,研究了微波水热合成反应温度、时间和前驱物浓度对反应产物形貌、粒度的影响,获得了制备纳米晶钛酸锶钡粉体的最优工艺参数.实验结果表明:在微波水热反应温度为195℃、反应时间20~30min、前驱物浓度为0.16mol/L时获得的粉体粒径小而且均匀,粉体平均粒度为60nm. 相似文献
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由近零介电常数材料构成的纳米天线,其折射率具有强度依赖性,可以用来调控远场辐射模式。因此,提出了基于氧化铟锡(ITO)的混合光学天线,以光学方式调控远场辐射角的偏转。并且,基于ITO和线性介电材料(nL)的混合结构天线可实现在近红外波段(1 000 nm~1 600 nm)偏转角的调控。随着入射光强度的增加,远场辐射角度最大可达到21.6°。基于混合结构,通过改变光学强度和波段进而影响辐射模式,最终调控偏转角度,这为进一步研究和应用于光束转向和光学调制奠定了基础。 相似文献
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Previously we reported the synthesis of novel organic-inorganic composite indium tin oxide (ITO) foam precursor leading to the formation of “sponge-like” ITO by burning away the organics. This newly made sponge-like ITO possesses relatively high electrical conductivity due to phonon confinement with reasonable pore structure and may have potential application as functional materials in semiconducting dye absorbing layer in dye-sensitized solar cell (DSSC) and also as the receptor of electrons injected from the quantum dots (QDs) of organic--inorganic hybrid QD based solar cell. This report is a short review of “sponge-like” ITO described as a lecture note on its future use as an alternative new prospective material for photoanode of solar cell in the domain of sustainable energy. 相似文献
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Low temperature processing of hybrid nanoparticulate Indium Tin Oxide (ITO) polymer layers and application in large scale lighting devices 总被引:1,自引:0,他引:1
Ilja MaksimenkoPeter Wellmann 《Thin solid films》2011,519(17):5744-5747
We report on transparent conductive indium tin oxide (In2O3:Sn; ITO) nanoparticle films processed at a low temperature of 130 °C for the application in lighting devices using spin coating and doctor blading techniques. Major emphasis is put on the beneficial application of the particular transparent electrode material for the fabrication of patterned large area electroluminescence lamps. In order to improve film properties like adhesion and conductivity, hybrid nanoparticle-polymer blends out of ITO particles and organic film-forming agent polyvinylpyrrolidone (PVP) and the organofunctional coupling agent 3-methacryloxypropyltrimethoxysilane (MPTS) have been developed. The layers were cured by UV-irradiation, which was also used for lateral structuring of the transparent, conductive electrode. Additional low-temperature heat treatment (T = 130 °C) in air and forming gas improved the electronic properties. While pure ITO nanoparticulate layers processed at 130 °C exhibited conductance of up to 3.1 Ω− 1 cm− 1, the nanocomposite coatings showed a conductance of up to 9.8 Ω− 1 cm− 1. Corresponding layers with a sheet resistance of 750 Ω/□ were applied in electroluminescent lamps. 相似文献
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Youn J. Kim Su B. Jin Sung I. Kim Yoon S. Choi In S. Choi Jeon G. Han 《Thin solid films》2010,518(22):6241-6244
Tin-doped indium oxide (ITO) thin films were deposited on glass substrates at various oxygen flow rates using a planar magnetron sputtering system with facing targets. In this system, the strong internal magnets inside the target holders confine the plasma between the targets. High resolution transmission electron microscopy revealed a combination of amorphous and crystalline phases on the glass substrate. X-ray photoelectron spectroscopy suggested that the decrease in carrier concentration and increase in mobility were caused by a decrease in the concentration of Sn4+ states. The electrical and optical properties of the ITO films were examined by Hall measurements and UV-visible spectroscopy, which showed a film resistivity and transmittance of 4.26 × l0−4 Ω cm, and > 80% in the visible region, respectively. 相似文献
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铟锡氧化物(Indium tin oxide)是一种优良的透明导电氧化物材料。叙述并对比了目前制备ITO粉体的几种方法的优缺点。对其中的化学共沉淀法和化学滴定法,讨论了从铟锡化合物的物理化学性质来选择原料和沉淀剂,分析了制备过程中各种离子的浓度、沉淀时的温度、终点pH值、煅烧温度的范围及时间、分散剂等影响因素。 相似文献
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Indium tin oxide (ITO) films are widely used for a transparent electrode of organic light emitting devices (OLEDs) because of its excellent conductivity and transparency. Two types of ITO substrates with different surface roughness were selected to use as anode of OLEDs. In addition, two types of etching process of ITO substrate, particularly the etching time, were also carried out. It was found that the surface roughness and/or the etching process of ITO substrate strongly influenced on an edge of ITO surface, further affected the operating characteristics and reliability of devices. 相似文献