基于品评小组可靠性筛选葡萄酒的香气描述符

利用定量描述性分析（0～5标度法）评价9 款国产‘赤霞珠’干红葡萄酒的香气特性,结合方差分析和多元统计分析方法,评估品评小组可靠性和规范葡萄酒香气特性感官描述符的筛选方法。结果表明,利用平均重现性指数Ri、检验统计量F值、均方误差（mean-square error,MSE）值和Manhattan图等能够有效评估品评员的重现性、辨别能力、可重复性以及品评小组的一致性。以可靠品评小组的感官数据为原始变量,通过几何平均值（M值）计算和排序,结合主成分分析（principal component analysis,PCA）和聚类分析（cluster analysis,CA）,规范了葡萄酒特征香气描述符的科学筛选方法,明确了实验‘赤霞珠’干红葡萄酒的香气特征：以黑醋栗、红醋栗等果香为主,有突出的焦糖、烟熏等焙烤类香气,兼有胡椒等佐料香气。     

Consumer acceptability,sensory properties and expert quality judgements of Australian Cabernet Sauvignon and Shiraz wines

Background and Aims: This study aimed to determine what sensory attributes most drive consumer and expert acceptance for Cabernet Sauvignon and Shiraz wines. Methods and Results: The sensory attributes of a set of commercial wines were quantified by a trained panel. A subset was assessed blind for liking by 203 consumers and for quality by 67 winemakers. For the total group of consumers, wines with low levels of ‘bitterness’, ‘hotness’, ‘metallic’, ‘smoky’ and ‘pepper’ were preferred. In addition, four consumer clusters were identified, each with different sensory drivers of preference, with the attributes ‘red berry’, ‘floral’, ‘caramel’ and ‘vanilla’ aroma, ‘acidity’, ‘green’ flavour and astringency being of importance in distinguishing the different clusters' acceptance scores. The winemakers' quality scores had little relationship with consumer response, although both groups gave low ratings to wines with Brettanomyces-related flavour. Conclusions: A relatively small set of sensory attributes were of greatest importance to consumer liking, and these generally dominate varietal differences. Winemakers' quality concepts do not closely align with those of the consumers. Significance of the Study: This study identifies sensory properties of red wines which could be maximised as well as those which should be reduced, allowing producers to better meet consumers' preferences.     

Wine produced by immobilized cells on dried raisin berries in sensory evaluation comparison with commercial products

Comparative sensory evaluation of wines produced by immobilized cells of Uvaferme 299 on dried raisin berries and free cells using the Saint Denis grape variety and of commercial Greek products (‘Biblia Chora’ rosé wine produced from the Syrah grape variety, ‘Palivos’ and ‘Strofilia’ rosé wines both produced from the Agiorgitiko grape variety) was carried out. Sensory evaluation was conducted twice by 11 tasters previously trained and a method for panel validation was proposed. Subsequently, the wines were evaluated for their aroma intension, aroma complexity, aroma elegance and overall quality. Duncan's multiple range test clearly showed that there were statistically significant differences between wines produced using different grape varieties and fermentation conditions. Linear regression analysis of the results was performed in order to investigate which sensory parameter had a significant effect on the overall quality and it revealed that only aroma elegance affected significantly the overall quality. Wine produced by immobilized cells scored a statistically higher value for its overall quality than the wine produced by free cells. Finally, discriminant sensory evaluation revealed a gooseberry, cherry, mint aroma for ‘Biblia Chora’ wine and a citrus, rose aroma for ‘Strofilia’ and ‘Palivos’ wines. Wines produced using immobilized and free cells were characterized by a fruity, banana‐like aroma, and a herbaceous note was predominant. Copyright © 2005 Society of Chemical Industry     

Volatile aroma and sensory analysis of black raspberry wines fermented by different yeast strains

Robus coreanus Miquel is a small berry fruit used for Korean black raspberry (KBR) wine‐making. Twelve different yeast strains were investigated by laboratory‐scale fermentation to develop a wine with a high flavour quality. Volatile aroma compounds from the wines were analysed using headspace–solid phase microextraction–gas chromatography–mass spectrometry and sensory evaluation was performed to evaluate the flavour characteristics. The volatile aroma compounds that mostly contributed to the flavour of KBR wines were those related to fruity (esters) and floral (terpenes) aromas. Fifteen out of the 67 identified volatile compounds showed higher odour activity values than other compounds in the wines, and these compounds were considered as important contributors to the final aromas of the wine. Additionally, the KBR wine fermented by the M1 yeast strain had the highest sensory preference because of higher fruity and floral aroma characters compared with other wines. In addition to the M1 strain, the other yeast strains that produced favourable sensory characteristics included Enoferm CSM, Uvaferm VRB, Lalvin ICV GRE, Lalvin ICV Opale and LevureSeche Active. Of these strains, the M1 strain produced a particularly excellent black raspberry wine, and thus could be applied for further large‐scale production of black raspberry wines. It is also expected that this work will expedite research on the production of high‐quality black raspberry wines with beneficial physicochemical properties, functionality and good sensory characteristics. Copyright © 2015 The Institute of Brewing & Distilling     

黑米酒挥发性成分分析及其变化规律研究

以不同酿造工艺制得的3种黑米酒为实验对象,采用顶空固相微萃取结合气相色谱-质谱联用（HS-SPME-GC-MS）技术分析黑米酒中的挥发性成分,并对贮藏期间3种黑米酒香气成分的变化规律进行了研究。结果表明,3种黑米酒共鉴定出66种香气成分,其中10°半干黑谷酒46种、传统型黑米酒51种、12°干红黑谷酒36种,挥发性物质主要包括醇类、酯类、醛酮类、酚类以及酸类物质等（醇类最高,酯类次之）。随着贮藏时间的延长,3种黑米酒香气成分含量均呈下降趋势,传统型黑米酒挥发性成分相对丰富且较为稳定,而采用现代新技术生产的12°干红黑谷酒风味物质变化最大且不稳定。     

Amelioration of smoke taint in wine by reverse osmosis and solid phase adsorption

Background and Aims: Wines made from grapes harvested from vineyards exposed to bushfire smoke can exhibit objectionable ‘smoky’, ‘cold ash’, ‘medicinal’ and ‘ashy’ aroma and flavour characters. This study evaluated a combined reverse osmosis and solid phase adsorption process as a potential amelioration method for the treatment of smoke‐tainted wines. Methods and Results: Smoke‐tainted wines were treated using either pilot or commercial scale reverse osmosis systems and the chemical composition and sensory properties of wine compared before and after treatment. The concentrations of smoke‐derived volatile phenols, including marker compounds, guaiacol and 4‐methylguaiacol, decreased significantly with treatment. As a consequence, diminished smoke‐related sensory attributes enabled treated wines to be readily differentiated from untreated wines. However, the taint was found to slowly return with time, likely because of hydrolysis of glycoconjugate precursors, which were not removed during the treatment process. Conclusions: Reverse osmosis and solid phase adsorption reduced the concentration of smoked‐derived volatile phenols and improved the sensory attributes of smoke‐tainted wines. Significance of the Study: This is the first study to evaluate the amelioration of smoke taint in wine using reverse osmosis and solid phase adsorption.     

Alcohol,Tannins, and Mannoprotein and their Interactions Influence the Sensory Properties of Selected Commercial Merlot Wines: A Preliminary Study

The objective of this study was to assess the influence of the interaction among alcohol, tannins, and mannoproteins on the aroma, flavor, taste, and mouthfeel characteristics of selected commercial Merlot wines. Merlot wines (n = 61) were characterized for wine chemistry parameters, including pH, titratable acidity, alcohol, glucose, fructose, tannin profile, total proteins, and mannoprotein content. Agglomerative clustering of these physicochemical characteristics revealed 6 groups of wines. Two wines were selected from each group (n = 12) and profiled by a trained sensory evaluation panel. One wine from each group was evaluated using the electronic tongue (e‐tongue). Sensory evaluation results showed complex effects among tannins, alcohol, and mannoproteins on the perception of most aromas, flavors, tastes, and mouthfeel attributes (P < 0.05). The e‐tongue showed distinct differences among the taste attributes of the 6 groups of wines as indicated by a high discrimination index (DI = 95). Strong correlations (r² > 0.930) were reported between the e‐tongue and sensory perception of sweet, sour, bitter, burning, astringent, and metallic. This study showed that interactions among wine matrix components influence the resulting sensory perceptions. The strong correlation between the e‐tongue and trained panel evaluations indicated the e‐tongue can complement sensory evaluations to improve wine quality assessment.     

The evaluation of remedial treatments for wine affected by Harmonia axyridis

This study evaluated the efficacy of a range of commercially available fining agents and other interventions on reducing 2‐isopropyl‐3‐methoxypyrazine (IPMP) concentration and taint characteristics of white and red wine affected by Harmonia axyridis (HA). Wines fermented in the presence of HA beetles were treated with bentonite, activated charcoal, oak chips, deodorized oak chips and either ultraviolet (red wine) or visible (white wine) light. IPMP concentrations were lowered by activated charcoal in white wine and deodorized oak in red wine. Treatment with oak chips reduced the intensity of HA‐associated sensory attributes (‘ladybug taint’) in both white and red wines, while other applications generally had no effect on white wine and limited effect on red wines.     

黑果腺肋花楸酒与赤霞珠葡萄酒香气物质对比分析

以赤霞珠葡萄酒为参照分析黑果腺肋花楸发酵酒的香气物质组成并进行感官品评,评价其酿酒潜质,为开发适宜消费者口味的黑果腺肋花楸酒提供参考。采用顶空固相微萃取结合气相色谱-质谱分析酒的香气物质成分。结果显示：黑果腺肋花楸酒香气物质含量为赤霞珠葡萄酒的2.73 倍,香气物质种类分别为41 种和40 种,其中共有的18 种。醇类物质含量最高,分别占总香气的62.11%和73.87%。依据香气活度值,酯类物质对酒的香气贡献最大,分别为36.57%和22.04%。黑果腺肋花楸酒的主体香气物质是大马士酮、辛酸乙酯、正己酸乙酯和乙酸异戊酯,而赤霞珠葡萄酒则为α-紫罗酮、辛酸乙酯、正己酸乙酯和苯乙醛。2 款酒中共有香气物质对香气贡献占比分别为34.20%和21.81%,说明具有一定的相似性,而大马士酮和α-紫罗酮对酒香气值的贡献分别为63.22%和76.36%,形成了各自酒的特色。经感官品评,黑果腺肋花楸酒比赤霞珠葡萄酒总得分高2 分,黑果腺肋花楸作为黑色浆果具有开发酿酒的价值。     

Sensory profiling of aroma in Greek dry red wines using rank-rating and monadic scoring related to headspace composition

Rank-rating and monadic scoring were compared in profiling sensory aroma character of 27 Greek dry red wines with 16 attributes. In parallel wine headspace volatiles were quantified using solid-phase micro-extraction gas chromatography but not identified. In rank-rating, 14 aroma attributes showed discriminations with P<0.05 and 11 P<0.001. In scoring, 6 of 16 attributes showed P<0.05. Principal component analysis (PCA) explained 88% variance in rank-rating data, with six significant components (PCs), in scoring 40% in two PCs. PCA analysis of 83 common flavour volatiles explained 48% variance in six PCs. Partial least-squares regression (PLS1) modelling achieved more and better models for attributes using rank-rating, 8 of 14, than for scoring, 3 of 16; PLS2 explained greater variance in rank-rating. For wine sensory/instrumental correlation studies, rank-rating has distinct advantages over monadic scoring in deciding volatiles contributing to sensory character prior to identification strategies such as HRGC–mass spectrometry.     

Sensory changes during bottle storage of Spanish red wines under different initial oxygen doses

Sixteen commercial Spanish red wines selected to cover a wide range of sensory properties were stored at 25 °C for 6 months in air-tight containers under different oxygen doses (0–30 mg L^− 1) mimicking real and extreme bottling situations. The 16 initial samples (before storage) and the 80 stored samples (16 wines × 5 oxygen doses) were submitted to sensory analysis. Sensory changes related to post-bottling storage and initial oxygen dose were evaluated by means of discriminant and characterisation sensory strategies.Significant increases in black fruits, dried fruits, woody, lactic and stronger increases in cooked vegetables and spicy notes reveal a general pattern of aroma evolution. Remarkable departures to this general pattern have been observed, which can be related to the initial sensory properties of the wines and to their basic polyphenolic composition. The effect of post-bottling storage in bitterness is wine dependent, while global decreases in both global intensity and persistence evaluated in mouth are observed. Discrete increases in astringency are observed for wines with the lowest initial astringent scores. Important sensory interactions between aroma attributes (herbal and spicy) and bitterness and between roasted and astringency perception are shown. Little impact of the initial oxygen dose in the in-mouth sensory properties is reported. These results are relevant for wine experts in that they help understanding the evolution of wine sensory properties in the bottling stage. This study may help them to develop strategies for managing this winemaking stage with objective criteria.     

RICE WINE BREWING WITH SPROUTING RICE,SPROUTING RICE INFECTED WITH ASPERGILLUS ORYZAE AND RICE KOJI

Fermentation tests were performed with sprouting rice, sprouting rice infected with koji mold, i.e. Aspergillus oryzae and rice koji, as saccharifying agent. Characteristics of the various rice wines were compared by gas chromatography and organoleptic testing. The rice wine made with sprouting rice was colorless and had light and refined characteristics in terms of both aroma and taste. The rice wine made with sprouting rice infected by Aspergillus oryzae was rich in isoamyl alcohol, isoamyl acetate and acetaldehyde; it was faintly yellow in color and had rich and mild characteristics. This rice wine had something in common with conventional Japanese sake as compared with the sprouting rice wine, and it might be a transitional intermediate between ancient sprouting rice wine and conventional Japanese sake. In accordance with the traditional method for sake brewing, starchy materials, tap water and sprouting rice as the saccharifying agent were added to the initital mash as first and second additions. The rice wine was somewhat improved by these additions, as assessed by organoleptic testing. The body of the resultant rice wine was fortified with dextrin and its acidic taste was masked by sugar and dextrin.     

Volatile secondary metabolites of Greco (Vitis vinifera L.) must

Greco grape (Vitis vinifera L.), a typical white variety of Campania region in the South of Italy, was investigated for the first time determining volatile‐free and glycosidically bound secondary metabolites that could be at the base of the aroma profile of DOCG ‘Greco di Tufo’ wines. C₁₈ reversed‐phase isolates of ‘Greco’ musts have been investigated by gas chromatography/mass spectrometry. ‘Greco’ must resulted characterised by a content of glycoconjugated terpenoids ranging from 180 to 370 μg L^?1. Linalool and geraniol detected in the ‘Greco’ must above their odour thresholds could explain a floral character attributed to the wine. Guaiacol in free fraction, 4‐vinylguaiacol and eugenol in the bound fraction could be at the origin of nutty and spicy notes of the wine. Some observations of this study also show that precursors of floral, spicy and nutty odorants seem to be enhanced by clay soil and good sun exposure.     

不同工艺对‘关口’葡萄干白葡萄酒品质的影响

目的:采用不同酿造工艺技术对‘关口’葡萄进行干白葡萄酒的酿造,揭示不同果皮浸渍工艺对‘关口’葡萄干白葡萄酒的影响,以期最大程度地发挥‘关口’葡萄的深加工可能性。方法:分别对‘关口’葡萄进行发酵前的果皮浸渍(fermentation before skin contact,FbSC)、带皮发酵(fermentation on skins,FoS),以澄清汁发酵作对照处理,测定各处理所得葡萄酒的基本理化指标、酚类物质、香气成分,并进行感官评价。结果:与对照组相比,采用FbSC和FoS工艺所得葡萄酒的pH值均增加,可滴定酸质量浓度均降低;对于采用FoS工艺所得的葡萄酒,其总酚、总黄酮、总黄烷醇、单体酚的质量浓度显著高于采用FbSC工艺所得的葡萄酒和对照组的葡萄酒(P0.05),香气成分总质量浓度则显著低于FbSC组和对照组(P0.05);与对照组相比,采用FbSC和FoS工艺所得葡萄酒的香气成分中的酸类和酯类物质质量浓度显著降低(P0.05),醇类和萜烯类物质质量浓度显著增大(P0.05)。另外,经过FbSC与FoS处理后,‘关口’葡萄干白葡萄酒的香气由以果香等香气为主转化为以果干、蜂蜜及成熟水果类香气为主;并且在澄清度、颜色、香气质量、口感纯正度、口感浓度、口感持久性、口感质量、整体平衡性等方面也均优于对照组。结论:果皮浸渍处理一定程度上提高了‘关口’葡萄干白葡萄酒的品质。     

FLAVOR AND AROMA ATTRIBUTES OF RIESLING WINES PRODUCED BY FREEZE CONCENTRATION AND MICROWAVE VACUUM DEHYDRATION

This article describes the production of sweet dessert wines produced using late‐harvest freeze concentration, wine produced from fresh grapes frozen using refrigeration and wine produced from grapes partially dried using microwave vacuum dehydration. The objective was to compare the aroma and flavor attributes of the wines to determine the effect of each method of juice concentration. The replicated wine samples were evaluated by 12 experienced judges, and the wines were analyzed using solid‐phase microextraction. The microextraction detected 28 compounds; however, levels of concentration of these compounds were below published aroma thresholds. Although all the wines were judged as acceptable sweet dessert wines, the judges detected significant differences. The wine made from the dehydrated grapes exhibited lower fresh fruit aroma, higher fusel oils and oxidation, and flavor notes including citrus/grapefruit and acidity were lower.