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采用干法工艺,即利用高速粉碎混合机对原土进行高混,常温自然放置进行充分钠化的方法,对甘肃平凉膨润土进行了钠化改性,就不同钠化剂(碳酸钠、氯化钠、氢氧化钠)的选择和配比、钠化高混时间、自然放置时间时钠化土性能的影响进行了研究.将干法制备的钠化土与涅法工艺进行了对比,在制备出性能较好的钠化土的同时,干法工艺具有流程简单、生产效率高等优点,能有效减少能耗、降低成本.用傅立叶红外变换光谱(FTIR)和X-射线衍射(XRD)对钠化土进行分析,发现钠化土在不改变原土结构的同时发生了阳离子交换,有效增大了原土的层问距. 相似文献
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采用化学脱水剂对明胶改性聚酰胺酸薄膜进行不同时间的化学亚胺化.通过红外光谱、示差扫描量热、热重分析等手段对化学亚胺化过程中薄膜的业胺化程度、热性能和力学性能进行了测定.结果表明,在化学亚胺化初期,薄膜的亚胺化程度、玻璃化温度和拉伸强度随着化学亚胺化时间的延长而增加.当化学亚胺化时间超过12 h后,继续延长化学亚胺化时间,薄膜的亚胺化程度、玻璃化温度和拉伸强度基本不变,薄膜的化学亚胺化基本完成.这时可得到玻璃化温度为205 ℃左右、耐520 ℃高温、拉伸强度较高的薄膜. 相似文献
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对企业自主研发的石墨化阴极技术指标和石墨化阴极在国内外铝电解槽上应用情况进行统计分析,得出结论:石墨化阴极具有良好的导电性、导热性、抗热震性和抗钠侵蚀性,可降低电解铝吨铝电耗,提高电解槽电流强度和电流效率,延长电解槽使用寿命,减少废阴极对环境的污染.同时对石墨化阴极在国内应用存在的问题进行了分析,对石墨化阴极的经济效益和发展前景进行了科学预测. 相似文献
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从香兰素合成3,4,5-三甲氧基苯甲醛 总被引:7,自引:0,他引:7
以香兰素为原料,经溴化、甲氧基化、甲基化3步反应合成药物中间体3,4,5-三甲氧基苯甲醛(TMB),总收率达75.7%。溴化采用氢溴酸与过氧化氢作为溴化试剂,甲氧基化以氯化亚铜、二氧化碳协同催化,丁香醛酚钠盐不需酸化直接进行甲基化反应 相似文献
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采用不同改性的短油度醇酸树脂作甲组分,异氰酸酯预聚物作乙组分,配制双组分聚氨酯涂料,探讨甲组分对双组分聚氨酯涂料性能的影响。结果表明,椰子油改性短油度醇酸树脂,颜色水白、耐黄变性能和丰满度好,可以作为高档的亮光清面漆、耐黄变的面漆用树脂;蓖麻油改性短油度醇酸树脂,颜色较深、丰满度较好、干燥速度慢及柔韧性好,可以作为普通的亮光面漆用树脂;豆油改性短油度醇酸树脂,干燥速度较快,应用于底漆和哑光面漆;合成脂肪酸改性短油度醇酸树脂,颜色水白、流平好、干燥速度慢、丰满度高及硬度高,可以作为高档的亮光面漆用树脂。 相似文献
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通过调节刮膜式分子蒸馏操作参数,考察了不同类型废油再生产品的透光率。结果表明,温度升高,一级再生油的透光率下降,二级再生基础油的透光率上升,废内燃机油的操作温度应控制在225℃左右,废液压油应控制在210℃左右,废混合油应控制在215℃左右为最佳;真空度升高,一级再生油的透光率上升,二级再生油的透光率下降,废内燃机油的真空度应控制在12 Pa左右,废液压油应控制在18 Pa左右,废混合油应控制在16 Pa左右为最佳;进料流量增加,一级、二级再生油的透光率均缓慢下降,因此应尽量维持较低流量。 相似文献
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大庆油页岩及干馏产物的利用途径分析 总被引:1,自引:0,他引:1
大庆油页岩的舍油率大部分都在10%以上,具有很好的经济开发价值.对大庆油页岩及其干馏产物性质的实验研究表明,油页岩的机械强度较低,应选择粉末、颗粒干馏炉进行加工处理;页岩油主要由柴油馏分和重油馏分组成,分别可加工成成品油和直接用作燃料油;热解干馏气热值约为17MJ/m3,可以在除作自身干馏所需的热量燃料外,用作城市煤气或工业锅炉的燃料;半焦着火点低,热值约为23 MJ/kg,可作为清洁燃料用于发电或民用;页岩灰的主要组分是氧化钙争氧化硅,可用于生产建筑材料. 相似文献
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聚硅氧烷消泡剂的失活和再生机理 总被引:2,自引:0,他引:2
介绍了聚硅氧烷消泡剂失活和再生的现象,分析了失活过程中消泡剂分散体粒径大小和分布,泡沫体系的表面张力、接触角、硅油铺展层的厚度以及泡沫膜的结构和状态,结果表明:硅油组成的改变、硅油和疏水二氧化硅微粒的分离、消泡剂分散体粒径的变小、铺展油层的消失和白色絮凝物的出现导致消泡剂失活,其中二氧化硅硅粒-硅油的分离和泡沫膜上硅油铺展油层的消失是主要因素。失活的消泡剂中加入硅油,消泡活性可再次恢复,这主要是由于消泡剂分散体粒子中的硅油-二氧化硅硅粒比例达到最佳的状态并在泡沫膜上又形成了新的具有消泡活性的硅油铺展油层。 相似文献
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An electronic nose was used for the detection of maize oil adulteration in camellia seed oil and sesame oil. The results of multivariate analysis of variance showed that the sensor signals of different kinds of oil are significantly different from each other. Principal component analysis (PCA) cannot be used to discriminate the adulteration of camellia seed oil, but can be used in the discrimination of adulteration in sesame oil. Linear discriminant analysis (LDA) is more effective than PCA and can be used in adulteration discrimination for both camellia seed oil and sesame oil. In order to check the discriminative power of LDA, canonical discriminant analysis was performed as well. Acceptable results were also obtained: The accuracy of prediction was 83.6% for camellia seed oil and 94.5% for sesame oil. The artificial neural network (ANN) model was used to detect the percentage of adulteration in camellia seed oil and sesame oil. The results showed that, based on ANN as its pattern recognition technique, the electronic nose cannot predict the percentage of adulteration in camellia seed oil, but can be used in the quantitative determination of adulteration in sesame oil. 相似文献
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Liquefaction of cellulosic wastes: III. Production,characterization and evaluation of pyrolytic oils
Hussein Kh. Gharieb Sami Faramawy Fawzi A. El-Amrousi 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》1993,58(4):395-402
Liquefaction of municipal solid wastes has been achieved in an atmosphere of hydrogen gas and in the presence of boric acid which catalyzes the pyrolysis reaction. Two petroleum distillates, namely gas oil and residual fuel oil, were used as carrier media of solid refuse. The yield of pyrolytic oil was studied as a function of different operational conditions (temperature, pressure of hydrogen, carrier oil medium and concentration of boric acid). Hydrocarbon constituents of the oil mixtures, produced by liquefaction of cellulosic wastes slurried in fuel oil, were investigated by means of gas chromatography. It was found that the oil mixture, obtained at optimum reaction conditions, showed pronounced occurrence of low hydrocarbons in the range C3-C15 as compared with the original fuel oil and the oil resulting from the pyrolysis of carrier oil without solid refuse. The residual pyrolytic char exhibited catalytic activity towards hydrocracking. It was suggested that the activity of char is due to the presence of transition metals as evidenced by an electron dispersion system (EDS). The hydrocracking activity of char seemed to be dependent on the operational conditions of the liquefaction. Multiple analytical parameters including API gravity, calorific value, total acid number and wt% of residue over 450°C were used to evaluate the oil mixtures produced as a petroleum crude oil. Carrier oils, particularly fuel oil, seemed to be highly modified in the course of the pyrolysis process. Also, the oil mixtures produced were distinguished from the original carrier oils by a considerably higher acidity due to association with oxygenated compounds which could be derived from cellulose macromolecules. 相似文献
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对一种炼油副产品作为乳化炸药油相材料的可行性进行了研究。该炼油副产品价格低廉,可降低乳化炸药的生产成本。通过对乳化效果、乳化基质稳定性以及敏化效果进行实验发现,此种炼油副产品能取代目前的油相材料制备乳化炸药。将炼油副产品和机械油、微晶蜡复配具有较强的乳化效果,所制备的乳化基质稳定性较好。此外,采用炼油副产品制备的乳化基质可按目前的敏化配方和工艺进行敏化。 相似文献
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John E. Blum 《Journal of the American Oil Chemists' Society》1966,43(6):416-417
Safflower oil has been used as an edible oil in numerous countries for many years. In the US, commercial use of safflower
oil as an edible product was noted in the 1950's and the use continues at progressively higher levels each year.
One use of safflower oil in “dressing” type products is related to the natural cold resistance of the oil. Other applications
include oil, margarine and some imitation dairy products. Additional development work has been done on other food products
so that the scope of usage could be broadened if there should be increased demands for safflower oil.
The susceptibility of safflower oil to oxidation has been minimized by improved processing and packaging.
Further use of safflower oil appears to be dependent upon availability, pricing, good cold resistance and the role of polyunsaturates
in the diet. 相似文献