共查询到18条相似文献,搜索用时 87 毫秒
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通过在超高碱值烷基水杨酸钙的合成过程中引入助表面活性剂和助促进剂,研究了反应助剂对产品收率和产品性能的影响。结果表明:随着助表面活性剂用量的增加,产品收率逐渐升高后达到平衡,加入硬脂酸、烷基苯磺酸及十二烷基酚等助表面活性剂后均可显著提高产品收率;助促进剂中,乙酸对反应的促进作用最明显,且其用量(w)为1.5%时产品收率最高;不同助表面活性剂与乙酸共同使用时的产品收率高于两者单独使用时的产品收率,且以硬脂酸与乙酸配合使用时的反应效果最好,产品收率可提高至98%以上,所制备出的超高碱值烷基水杨酸钙黏度低、与磺酸盐的配伍性好,其综合性能优异。 相似文献
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本文针对阳离子表面活性剂压裂液在阴离子岩层中损失较大、会降低岩层的渗透率等缺陷,合成出阴离子磺酸盐型表面活性剂——棕榈酸甲酯磺酸钠,将此表面活性剂与助剂十八醇按质量比1:2复配后可作为压裂液增稠剂几。JL在3.5%氯化钠溶液中迅速交联得到一种阴离子清洁压裂液。考察了该压裂液的耐温抗剪切性能、黏弹性能、携砂性能、滤失性能、破胶性能及对地层的伤害。实验结果表明:质量分数为5%的JL在3.5%的氯化钠水溶液中,1~2min内即可快速成胶,黏弹性、耐温耐剪切性较好,80℃下的体系黏度仍能达到40mPa·s。在体积比为40%的砂比下,悬砂效率比普通瓜胶体系水基压裂液提高48.7%。体系遇煤油易破胶,破胶液澄清,无残渣。对地层的伤害率低,为7.6%。体系呈中性,能够适用于酸敏碱敏地层,可满足低压低渗透油气藏压裂的要求。 相似文献
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This paper mainly covers a method for preparing a highly alkaline magnesium linoleate solution with a totalbase number (TBN) value of 328 mg KOH/g using linoleic acid as the biodegradable raw material, which can substitute fortraditional lubricant detergents as an environmentally friendly detergent. Reaction conditions, including the molar ratio ofmagnesium oxide to linoleic acid, the molar ratio of methanol to magnesium oxide, the carbonation temperature, the molarratio of water to magnesium oxide, the flow rate of CO2 gas and the duration for injection of CO2 to magnesium oxide system,were optimized. 相似文献
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润滑油清净分散剂用纳米碳酸镁的制备 总被引:1,自引:0,他引:1
介绍一种润滑油清净分散剂用纳米碳酸镁的制备工艺,指出制备工艺因素,如水的加入方式、二氧化碳流入速率等.所得产品为石油磺酸镁改性的纳米碳酸镁油溶性分散体系,其碱值高达400mg KOH/g.用红外光谱及冷冻蚀刻电镜观测技术,确定产物中含碳酸镁,且粒径在40×10-9m左右. 相似文献
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超高碱值环烷酸镁胶体粒子微观结构的研究 总被引:3,自引:0,他引:3
刘彬彬 《石油与天然气化工》1996,(2)
通过对超高碱值环烷酸镁胶体粒子微观结构的电镜分析研究,找出了胶体粒子结构与其碳酸化程度之间的关系,为高碱值环烷酸盐生产工艺的优化及其质量的改进提供了方向和依据。 相似文献
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An innovative idea was proposed to prepare the overbased nano-sized calcium carbonate-calcium petroleum sulfonate in-situ the HIGEE reactor. The test sample prepared by this technology could meet the requirement of the industry standard SH0042-91 for the first-grade product on a par with similar overseas product. The test results obtained upon observation under microscope after freezing etching of specimen revealed that the crystal size of colloidal calcium sulfonate was in the range of 10-30 nm with an average size of 20 nm. The size of the detergent additive was uniform with good transmittance and fluidity. The HIGEE technology possesses five specific features as shown below: Firstly, the carbonation reaction is completed in one step with the reaction time reduced by more than 50% as compared to traditional batch reactor process along with enhanced reaction efficiency, good operability of the process and stabilized product quality. Secondly, ammonia emitted from the reaction is used as the co- promoter without the need for adding ammonia and water as promoters to simplify the promoter system along with effective and strong coupling of reactions. Thirdly, the utilization rate of Ca(OH)2 and CO2 is increased by 15% and 30%, respectively, with product yield increased by 15%, and calcium residue decreased by 65%. Fourthly, the HIGEE technology is environmental benign because of gasoline is used in this technology instead of toxic toluene and xylene. Fifthly, the dimension of HIGEE reactor is reduced by above two-thirds. The success in development of this new technology will offer new ideas and technology platform for the synthesis of metal detergent additive to lubricating oils in China. 相似文献
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改性石油磺酸盐的合成与表征 总被引:2,自引:0,他引:2
以甲苯为初始反应物,通过付-克反应、Knoevenagel反应和磺化反应,合成了改性甲基苯磺酸钠.探索了以工业渣油为原料合成改性石油磺酸钠的方法.对合成产物进行了表征. 相似文献
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选用液压油基础油、25号变压器油、8号航空油作为研究对象,通过测定在-10~-40℃温度范围内不同温度时单种油样以及混合油样低温运动粘度,研究了低温对润滑油性能的影响。随着温度的逐渐降低,油样的粘度逐渐增加,温度越低油样粘度增加越快:当温度相对较高时(高于-20℃),随温度的降低油样粘度增加的速率较小;当温度相对较低时(低于-20℃),随着温度的逐渐降低,油样粘度增加的速率逐渐增大。并对实验现象做了解释。通过研究混合油样的低温运动粘度,为润滑油在低温条件下的应用以及研制提供依据。 相似文献
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《Petroleum Science and Technology》2013,31(6):595-606
Abstract High purity decyl methylnaphthalene sulfonate (DMNS) surfactant was synthesized. The purity of product was determined by HPLC, and the structure was confirmed by IR, UV, and ESI-MS. The surface and oil-water interfacial activities of DMNS surfactant were studied. The effects of concentrations of the surfactant, alkali, and inorganic salt on the dynamic interfacial behavior of crude oil/Shengli Oil Field/surfactant oil flooding systems were studied, and comparitive studies of systems with strong and buffered alkali were also carried out. Results showed that DMNS surfactant possessed great capability and efficiency for lowering solution surface tension and oil-water interfacial tension. The critical micelle concentration (cmc) was 0.02% and the surface tension at this concentration was 31.61 mN.m?1. At proper concentrations of the surfactant, alkali, and inorganic salt, the dynamic interfacial tension between the crude oil of the Shengli Oil Field and the surfactant oil flooding system reached a minimum value of 10?5–10?6 mN.m?1 in a very short time (3–20 min) and maintained an ultra-low value (< 10?2 mN.m?1) for a long period of time (15–87 min). The crude oil/surfactant systems presented satisfactory interfacial behavior. DMNS has great potential to be used in enhanced oil recovery (EOR) with low cost and high efficiency. 相似文献
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在菜籽油(RO)分子中引入羟基,合成了一种新型的环境友好型润滑添加剂(HORO),并利用红外光谱对其主要官能团进行了鉴定。通过SRV摩擦磨损试验机考察了以菜籽油为基础油、以HORO为添加剂时对钢-镁摩擦副抗磨减摩性能的影响,同时通过X射线光电子能谱对镁合金磨斑表面进行分析,探讨了羟基化改性菜籽油润滑添加剂的抗磨减摩机理,并对生物降解性能进行了评定。结果表明:羟基化改性菜籽油润滑添加剂对钢—镁摩擦副具有优良的极压抗磨和减摩性能,2%的该种添加剂能使镁合金磨损体积从7.8 mm3降低到2 mm3,摩擦系数则从0.054降低到0.043;其润滑作用机理是由于长链菜籽油分子在镁合金摩擦表面进行吸附或发生摩擦化学反应形成了摩擦聚酯膜与镁的氧化膜共同组成的起抗磨作用的润滑膜;生物降解试验表明羟基化改性菜籽油具有优异的生物降解性能。由此推断,研制的羟基化改性菜籽油是一种性能优异的环境友好镁合金润滑添加剂。 相似文献