挤压速度和电磁铸造锭坯对AZ31镁合金板材组织和性能影响

文章研究挤压条件下挤压速度和电磁铸造锭坯对挤压态AZ31镁合金板材组织和性能的影响。研究结果发现,挤压速度比较低时,板材晶粒尺寸小,板材的表面质量比较好;随着挤压速度的降低,抗拉强度、屈服强度和延伸率都有一定的提高。由于镁合金是HCP的晶体结构,同时对挤压速度非常敏感,对变形均匀性影响比较大,因此造成挤压板材的内外晶粒大小不均。在电磁场的作用下,溶质在晶内的固溶度增大,同时晶粒大小也比常规铸造的细小,因此电磁铸造的锭坯经挤压机挤压后,挤压板材的晶粒尺寸比较细小,且强度和塑性都有所提高。     

连续挤压工艺生产AZ31镁合金板材的实验研究

本文利用连续挤压技术的单、双杆进料方法试验生产了尺寸为160mm×8mm, 170mm×4mm和160mm×3mm的AZ31镁合金板材。分析了单、双杆进料方式,不同宽厚比和不同挤压速度等条件对镁合金板材横截面微观组织及力学性能的影响。讨论了应用双杆进料连续挤压工艺生产AZ31镁合金宽薄板的工艺可行性。结果表明：与单杆进料相比,双杆进料方式的连续挤压AZ31镁合金板材横截面微观组织均匀性较好,板材平均抗拉强度可达到239MPa,平均延伸率为15%。宽厚比由20增加到53,可获得5μm细化晶粒的镁合金板材。随挤压轮转速提高,板材抗拉强度降低,是由于温度升高会导致晶粒尺寸变大。     

Mg2Si强化相对AZ31镁合金挤压组织与力学性能的影响

通过Al-Si中间合金取代Al添加,并经热挤压成形,在AZ31镁合金中引入Mg₂Si强化相。采用光学显微镜(OM)、扫描电镜(SEM)、X射线衍射分析(XRD)、电子万能试验机等研究了Mg₂Si强化相对AZ31镁合金挤压组织与力学性能的影响。结果表明,添加Al-Si中间合金后的Mg-3(Al-Si)-Zn挤压组织呈现明显的双峰分布特征,Mg₂Si颗粒相可通过粒子激发形核(PSN)作用促进动态再结晶,在碎化的Mg₂Si颗粒相周围,合金组织显著细化,形成明显异于其他正常尺寸晶粒的细晶区。引入Mg₂Si强化相后,Mg-3(Al-Si)-Zn挤压态合金的屈服强度和抗拉强度都得到提高,分别达到175和269 MPa,同时伸长率略有降低。     

轧制工艺对AZ31B镁合金薄板组织与性能的影响

研究了轧制温度和轧制速度对AZ31B镁合金薄板微观组织演变和力学性能的影响。结果表明,轧辊加热有利于镁合金薄板成型;AZ31B镁合金在低温或低速轧制时薄板纵向组织为大量的切变带,切变带区域包含大量孪晶组织,横向组织为含极少量孪晶的等轴晶组织;在轧制温度为400℃和轧制速度为16m/min轧制时,由于动态再结晶,横纵截面组织均为等轴晶。AZ31镁合金薄板的最佳轧制制度为轧辊温度为70℃、轧制温度为400℃、轧制速度为6m/min,此工艺轧制的薄板横向抗拉强度、屈服强度和伸长率分别为350MPa、300MPa和12%,纵向为345MPa、290MPa和11.2%,纵向与横向性能差别明显减小。     

Effect of rolling process on microstructures and mechanical properties of AZ31B alloy sheets

AZ31B magnesium extruded slabs prepared from LFEC were rolled at fairly lower temperature at 3, 6 and 16 m/min rolling speeds into 1 mm thickness. The results indicate that the microstructures achieved by rolling at low temperature or at low rolling speed are composed of many prismatic regions divided by shear strips due to pile-up of twin crystals; the prismatic regions increase at elevated rolling temperature or at high rolling speed, and finally all are composed of equiaxed crystals without twin crystals due to dynamic recrystallization. After optimizing control of rolling process, excellent mechanical properties would be acquired. The mechanical properties ofAZ31B sheet are ab=350 MPa, cr0.2=300 MPa, and 3=12.0% when rolled at 6 m/min. At the same time, the difference of mechanical properties between transverse and longitudinal direction reduced markedly.     

离心压力对AZ31镁合金的组织和力学性能的影响

通过XRD、压缩试验等方法研究了不同离心压力对AZ31镁合金组织演变和力学性能的影响。结果表明,随着离心压力的增大,离心铸造AZ31镁合金的晶粒明显细化,平衡凝固的共晶转变被抑制,第二相β-Mg17Al12析出量减少,由粗大的“骨骼”状分布转变成弥散分布在晶界,形成以过饱和初生相ɑ-Mg为主相的凝固组织。XRD分析表明,离心压力的增大引起X射线衍射峰向高角度方向偏移,α-Mg的晶格常数减小。随着离心压力的增大,合金力学性能得到明显改善,抗压强度从199 MPa提高到256 MPa,而伸长率变化不明显。     

连铸AZ31镁合金的热挤压变形组织与性能(英文)

文章研究了电磁连铸AZ31镁合金经热挤压变形后的微观组织和力学性能。结果表明,挤压过程中的动态再结晶能够显著细化晶粒,局部细晶区的平均晶粒为2μm。与铸态合金相比,挤压后的AZ31镁合金具有更细小的晶粒和更均匀的微观组织。挤压变形后产生强烈的基面织构;挤压后材料的力学性能显著提高。屈服强度、抗拉强度和断面收缩率随着挤压比的增大而增大。挤压比为25时,屈服强度、抗拉强度和断面收缩率分别为259MPa,357MPa和30.5%,比铸态合金分别提高了86.33%,64.52%和67.40%。随着挤压比的增大,晶粒细化效果更为明显,微观组织更均匀。断口形貌分析表明,挤压变形后材料由韧脆混合型断裂,转变为韧性断裂。     

挤压比对AZ31镁合金组织结构的影响

试验研究了挤压比对AZ31镁合金组织结构的影响.结果表明,258℃挤压变形镁合金在形变初期容易出现孪晶,再结晶晶粒一般出现在晶界和孪晶附近.挤压比小时动态再结晶晶粒平均尺寸为2 μm,动态结晶细化了晶粒.随着挤压比增大,晶粒尺寸减小,组织趋于均匀.挤压比达到16时,动态再结晶基本完成.挤压比为25时,能得到晶粒细小且均匀的组织,平均晶粒尺寸为7.3 μm.     

Influence of hot extrusion on microstructure and mechanical properties ofAZ31 magnesium alloy

Extrusion treatment is a common method to refine the grain size and improve the mechanical properties of metal material. The influence of hot extrusion on microstructure and mechanical properties of AZ31 magnesium alloy was investigated. The results ,show that the mechanical properties of AZ31 alloy are obviously improved by extrusion treatment. The ultimate tensile strength （UTS） of AZ31 alloy at room temperature is measured to be 222 MPa, and is enhanced to 265.8 MPa after extrusion at 420℃. The yield tensile strength （YTS） of AZ31 alloy at room temperature is measured to be 84 MPa, and is enhanced to 201 MPa after extrusion at 420℃. The effective improvements on mechanical properties result from the formation of the finer grains during extrusion and the finer particles precipitated by age treatment. The features of the microstructure evolution during hot extruded of AZ31 alloy are dislocation slipping on the matrix and occurrence of the dynamic recrystallization.     

AZ31镁合金挤压薄板织构及力学各向异性

研究AZ31镁合金挤压薄板的显微组织、织构及室温下板面内各不同方向的力学性能。织构分析表明,挤压薄板主要有{0002}<1-010>和{10-10}<11-20>2种织构组分。拉伸测试结果显示,沿挤压方向屈服强度最高,达到200.4MPa,这是由于这种取向基面滑移和{1-012}锥面孪生均不能开动,发生织构强化的结果;与挤压方向呈45°方向伸长率最高达19.0%,这是由于具有{10-10}<11-20>织构组分晶粒的基面滑移开动;与挤压方向呈90°方向屈服强度最低仅为挤压方向相应值的一半左右,这是由于具有{10-10}<11-20>织构组分晶粒发生了{10-12}锥面孪生。     

Effects of cerium on the microstructure and mechanical properties of AZ31 alloy

AZ31 alloy with Ce addition was studied. The influence of Ce contents on the microstructure and tensile properties of the alloy was analyzed. Ce addition results in the formation of AlzCe and the annealed microstructure is improved by the addition. There was no recrystallization of the alloy after rolling, however, it did occur after annealing. The alloy can be strengthened by adding Ce and the alloy with 1.05 wt.% Ce possessed the best synthetical properties of all the tested alloys. As rolled, σb and δof this alloy are 321 MPa and 6.9%, and as annealed, they are 259 MPa and 21.8%.     

退火工艺对AZ31B温轧薄板组织和性能的影响

分析不同的退火时间对AZ31B镁合金温轧薄板的组织和性能的影响。通过试验和分析发现:镁合金温轧薄板在退火温度为573 K、退火时间为60 min时,能够获得较好的综合力学性能;进一步延长退火时间到120 min,塑性进一步改善,r值基本保持不变,n值增加。     

Effects of yttrium addition on microstructure and mechanical properties of as-extruded AZ31 magnesium alloys

The effects of yttrium addition on microstructure and mechanical properties of as-extruded AZ31 magnesium alloys were investigated by OM,XRD and SEM.The results show that the addition of yttrium results in the formation of a new phase,Al_2Y. When the addition of yttrium is higher than 1.48%-2.91%(mass fraction),another new phase,Al_3Y_5Mn_7,forms,and the amount ofβ-Mg_(17)Al_(12) phase in the AZ31 alloy decreases sharply.The tensile test at room temperature indicates that the yield strength of as-extrude...     

退火对AZ31镁合金板组织与性能的影响

镁合金板轧制后会出现大量形变孪晶,对使用性能带来非常不利影响。通过对镁合金板退火处理,用光学显微镜、扫描电子显微镜、拉伸试验机及X射线衍射仪,对AZ31镁合金板材轧制后不同退火制度下的显微组织、力学性能和衍射峰宽化现象进行了研究。结果表明,AZ31镁合金轧制后出现的大量形变孪晶,在200～350 ℃退火后,发生回复再结晶,孪晶基本消失;240 ℃退火1 h,组织为细小等轴晶粒,伸长率达到20.6%;轧制后的拉伸断裂面沿一定的晶面分离,退火后拉伸断口呈明显韧窝状,为典型的韧性断裂。轧制使层错率升高,在X射线衍射谱中表现为峰形宽化;退火使层错率降低,伸长率提升。     

深冷处理对AZ31镁合金焊接接头组织与性能的影响

针对镁合金焊接接头的软化问题,采用不同深冷时间对AZ31镁合金MIG焊接接头进行了深冷处理,并测试与分析了不同深冷时间下焊接接头的力学性能和显微组织。结果表明,深冷处理可显著强化AZ31镁合金焊接接头,其中经过(-196℃,12 h)深冷处理后的焊接接头,硬度提高了8.3%,抗拉强度与伸长率分别提高了15.43%和10.16%;随着深冷时间的延长,焊接接头的组织进一步细化,并有第二相在基体上不断析出,且呈弥散分布。     

AZ31镁合金的等温挤压及其力学性能分析

等温挤压是镁合金材料的重要加工方法,它能改善制品的质量,提高制品的力学性能。研究了等温挤压AZ31镁合金材料的力学性能。结果表明：等温挤压显著地提高AZ31镁合金的强度、硬度,但当变形程度达到82％以上时,其强度不再增加,反而下降。材料的硬度有方向性。     

Effect of extrusion ratio on microstructure and mechanical properties of AZ91D magnesium alloy recycled from scraps by hot extrusion

A method for recycling AZ91D magnesium alloy scraps directly by hot extrusion was studied. Various microstructural analyses were performed using the techniques of optical microscopy, scanning electron microscopy (SEM) and energy dispersive spectroscopy(EDS). Microstructural observations revealed that all the recycled specimens consisted of fine grains due to the dynamic recrystallization. The main strengthening mechanism of the recycled specimen was grain refinement strengthening and homogeneous distribution of oxide precipitates. The interfaces of individual scraps of extruded materials were not identified when the scraps were extruded with the extrusion ratio of 40:1. Oxidation layers of the scraps were broken into pieces by high compressive and shear forces under the extrusion ratio of 40:1. The ultimate tensile strength and elongation to failure increased with increasing the extrusion ratio. Recycled specimens with the extrusion ratio of 40:1 showed higher ultimate tensile strength of 342.61 MPa and higher elongation to failure of 11.32%, compared with those of the cast specimen.