Mode III fatigue delamination growth of glass fiber reinforced polymer woven laminates at cryogenic temperatures

This paper investigates the cryogenic fatigue delamination behavior of glass fiber reinforced polymer woven laminates under Mode III loading. Fatigue delamination tests were conducted using split cantilever beam specimens at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K). A finite element analysis was also employed to calculate the energy release rate. The temperature dependence of the fatigue delamination growth rate vs. energy release rate range is discussed. Fracture surfaces were examined by scanning electron microscopy to identify the delamination mechanisms under fatigue loading. The important conclusion we reach is that the Mode III fatigue delamination growth rates of woven laminates at cryogenic temperatures are lower than that at room temperature.     

Delamination growth mechanisms in woven glass fiber reinforced polymer composites under Mode II fatigue loading at cryogenic temperatures

The purpose of this research is to characterize the cryogenic delamination growth behavior in woven glass fiber reinforced polymer (GFRP) composite laminates subjected to Mode II fatigue loading. Mode II fatigue delamination tests were performed at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K) using the four-point bend end-notched flexure (4ENF) test method, and the delamination growth rate data for the woven GFRP laminates were obtained. The energy release rate range was determined by the finite element method. Microscopic examinations of the specimen sections and fracture surfaces were also carried out. The present results are discussed to obtain an understanding of the fatigue delamination growth mechanisms in the woven GFRP laminates under Mode II loading at cryogenic temperatures.     

Cryogenic fatigue behavior of plain weave glass/epoxy composite laminates under tension-tension cycling

This paper focuses on understanding the tension-tension fatigue behavior of woven glass fiber reinforced polymer laminates at cryogenic temperatures. Tension-tension fatigue tests at frequencies of 4 and 10 Hz with a stress ratio of 0.1 were conducted at room temperature, 77 and 4 K. The fatigue stress versus cycles to failure (S-N) relationships and fatigue limits for 10⁶ cycles were obtained. Fractured specimens tested under fatigue tests were also examined with optical microscope.     

Cryogenic delamination growth in woven glass/epoxy composite laminates under mixed-mode I/II fatigue loading

This paper investigates the fatigue delamination growth behavior in woven glass fiber reinforced polymer (GFRP) composite laminates under mixed-mode I/II conditions at cryogenic temperatures. Fatigue delamination tests were performed with the mixed-mode bending (MMB) test apparatus at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K), in order to obtain the delamination growth rate as a function of the range of the energy release rate, and the dependence of the delamination growth behavior on the temperature and the mixed-mode ratio of mode I and mode II was examined. The energy release rate was evaluated using three-dimensional finite element analysis. The fractographic examinations by scanning electron microscopy (SEM) were also carried out to assess the mixed-mode fatigue delamination growth mechanisms in the woven GFRP laminates at cryogenic temperatures.     

Acoustic emission and fracture behavior of GFRP woven laminates at cryogenic temperatures

This paper describes an experimental and analytical study on fracture and damage behavior of GFRP woven laminates at cryogenic temperatures. CT (compact tension) tests were carried out at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K) to evaluate the critical values of the fracture mechanics parameters. During the CT tests, AE (acoustic emission) method was implemented. AE signals can identify the critical load at which gross failure occurs. A FEA (finite element analysis) was also applied to calculate the fracture mechanics parameters. The failure criteria (Hoffman criterion and maximum strain criterion) or the damage variable based on the continuum damage mechanics was incorporated into the model to interpret the experimental measurements and to study the damage distributions within the specimen. Several methods of calculating J-integral are discussed.     

Analysis of mixed-mode interlaminar fracture and damage behavior of GFRP woven laminates at cryogenic temperatures

The objective of this work is to investigate the interlaminar fracture and damage behavior of glass fiber reinforced polymer (GFRP) woven laminates loaded in a mixed-mode bending (MMB) apparatus at cryogenic temperatures. The finite element analysis (FEA) is used to determine the mixed-mode interlaminar fracture toughness of MMB specimen at room temperature (RT), liquid nitrogen temperature (77 K) and liquid helium temperature (4 K). A FEA coupled with damage is also employed to study the damage distributions within the MMB specimen and to examine the effect of damage on the mixed-mode energy release rate. The technique presented can be efficiently used for characterization of mixed-mode interlaminar fracture and damage behavior of woven laminate specimens at cryogenic temperatures.     

Cryogenic through-thickness tensile characterization of plain woven glass/epoxy composite laminates using cross specimens: Experimental test and finite element analysis

This paper investigates the through-thickness tensile behavior of woven glass fiber reinforced polymer (GFRP) composite laminates at cryogenic temperatures. Tensile tests were carried out with cross specimens at room temperature and liquid nitrogen temperature (77 K), and the through-thickness elastic and strength properties of the woven GFRP laminates were evaluated. The failure characteristics of the woven GFRP laminates were also studied by optical and laser scanning microscopy observations. A three-dimensional finite element analysis was performed to calculate the stress distributions in the cross specimens, and the failure conditions of the specimens were examined. It is found that the cross specimen is suitable for the cryogenic through-thickness tensile characterization of laminated composite materials. In addition, the through-thickness Young's modulus of the woven GFRP composite laminates is dominated by the properties of the matrix polymer in the given temperature, while the tensile strength is characterized by both, the fiber to matrix interface energy and the cohesion energy of the matrix polymer.     

Effect of damage on the interlaminar shear properties of hybrid composite laminates at cryogenic temperatures

This paper presents the experimental and numerical characterization of the interlaminar shear failure of hybrid composite laminates at cryogenic temperatures. Cryogenic short beam shear tests were performed on hybrid laminates consisting of woven glass fiber reinforced polymer (GFRP) composites and polyimide films to evaluate their interlaminar shear strength. Microscopic observations of damage accumulation and failure mechanisms were also made on failed specimens. In addition, a progressive damage analysis was conducted to predict the initiation and growth of damage in the specimens, and the interlaminar shear strength was determined from the maximum shear stress in the failure region. The damage effect on the interlaminar shear properties of hybrid laminates at cryogenic temperatures was examined based on the experimental and numerical results.     

Cryogenic Interlaminar Fracture Properties of Woven Glass/Epoxy Composite Laminates Under Mixed-Mode I/III Loading Conditions

We characterize the combined Mode I and Mode III delamination fracture behavior of woven glass fiber reinforced polymer (GFRP) composite laminates at cryogenic temperatures. The eight-point bending plate (8PBP) tests were conducted at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K) using a new test fixture. A three-dimensional finite element analysis was also performed to calculate the energy release rate distribution along the delamination front, and the delamination fracture toughnesses were evaluated for various mixed-mode I/III ratios. Furthermore, the microscopic examinations of the fracture surfaces were carried out with scanning electron microscopy (SEM), and the mixed-mode I/III delamination fracture mechanisms in the woven GFRP laminates at cryogenic temperatures were assessed. The fracture properties were then correlated with the observed characteristics.     

Accelerated testing for long-term durability of GFRP laminates for marine use

Our proposed accelerated testing methodology for the long term durability of polymer composites is based on the time–temperature superposition principle to be held for the viscoelasticity of polymer matrix. The long term flexural fatigue life of plain woven glass fiber/vinyl-ester (GFRP) laminates for conventional marine use was predicted based on the proposed methodology. As results, the flexural fatigue strengths of GFRP laminates decreases strongly with increasing time and temperature as well as the number of cycles to failure. The long term fatigue strength at any time, temperature and number of cycles to failure can be predicted using the master curves of fatigue strength obtained based on our proposed accelerated testing methodology.     

玻璃纤维增强树脂基复合材料弯曲强度时间温度相关性

研究了玻璃纤维增强树脂基复合材料 (GFRP) 层合板弯曲强度高温加速试验的时间温度相关性。在不同的温度和加载速率下进行了三点弯曲试验。通过弯曲强度控制曲线的时间温度移动因子曲线分析了GFRP层合板的弯曲强度时间温度相关性。探讨了低温短时和高温长时的失效机理。通过玻璃纤维拉伸延迟断裂试验,对GFRP层合板的低温短时弯曲强度的时间温度相关性进行了修正。修正后的弯曲强度控制曲线的时间温度移动因子曲线与基体树脂动态杨氏模量的时间温度移动因子曲线非常吻合,表明GFRP层合板的弯曲强度取决于基体树脂的粘弹性性能。      

Microscale experimental investigation of failure mechanisms in off-axis woven laminates at elevated temperatures

Off-axis woven laminates fabricated from carbon fiber and a high glass transition temperature thermosetting resin were subjected to tensile static and fatigue loading at temperatures ranging from room temperature up to 205 °C. The damage mechanism prevalent to these specimens was investigated by post-mortem examination using a scanning electron microscope. During most of their life fatigue specimens had accumulated minimal damage which consisted of matrix cracks, transverse bundle cracks and intra-ply delamination. Just before failure fiber bundles began to straighten out and rotate towards the loading direction. This behavior led to large elongation and necking of the specimens before fracture. Overall, the matrix-dominated material behavior and fiber reorientation due to the off-axis configuration had a far greater influence on the fracture morphology than the gradual accumulation of damage due to fatigue loading. It was also found that damage formation was strongly influenced by the type of applied loading and the test temperature.     

Mixed-mode interlaminar fracture and damage characterization in woven fabric-reinforced glass/epoxy composite laminates at cryogenic temperatures using the finite element and improved test methods

The present research examines experimentally and analytically the mixed-mode interlaminar fracture and damage behavior of glass fiber reinforced polymer (GFRP) woven laminates at cryogenic temperatures. The mixed-mode bending (MMB) tests were performed with the improved test apparatus, at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K). The energy release rates at the onset of delamination crack propagation were evaluated for the woven GFRP specimens using both beam theory and finite element analysis. The fracture surfaces were also examined to verify the fracture mechanisms. In addition, the initiation and growth of damage in the specimens were predicted by a damage analysis, and the damage effect on the mixed-mode interlaminar fracture properties at cryogenic temperatures was explored.     

Fatigue delamination growth in woven glass/epoxy composite laminates under mixed-mode II/III loading conditions at cryogenic temperatures

We investigate the cryogenic delamination growth behavior in woven glass fiber reinforced polymer (GFRP) composite laminates under mixed-mode II/III fatigue loading. Fatigue delamination tests were conducted with six-point bending plate (6PBP) specimens at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K), and the delamination growth rate data for various mixed-mode ratios of Modes II and III were obtained. The energy release rate was evaluated using the three-dimensional finite element method. In addition, the fatigue delamination growth mechanisms were characterized by scanning electron microscopic observations of the specimen fracture surfaces.     

Analytical and finite element investigations of shear/compression test fixtures

Insulation systems are critical components of the international thermonuclear experimental reactor (ITER). They must meet the super conducting magnets design requirements, including mechanical strength under combined shear and compressive stresses at cryogenic temperatures. Past cryogenic magnet systems often relied on woven glass/epoxy materials for insulation. An important point is to find a reliable shear/compression test method for these materials. The present work investigates a commonly used shear/compression setup and aims at measuring the reliability of the obtained test results. Therefore, the stress and failure analysis is performed analytically and numerically using the finite element method. The model is based on woven glass fiber reinforced materials which are subjected to combined shear and compressive stresses as well as to thermal loading, that results from cooling from 293 K to the test temperature of 77 K. A short analytical section shows the problems of common failure criteria which are used to describe the interaction of the shear and compression stresses. The numerical—finite element—section is based on three-dimensional linear elastic finite element models under thermo-mechanical loading. The locations of high stress gradients are investigated using an average stress criterion. Three different model geometries (15°, 45°, and 70°) are analyzed and finally compared with respect to their reliability.     

A progressive damage simulation algorithm for GFRP composites under cyclic loading. Part II: FE implementation and model validation

The FE implementation of FADAS, a material constitutive model capable of simulating the mechanical behaviour of GFRP composites under variable amplitude multiaxial cyclic loading, was presented. The discretization of the problem domain by means of FE is necessary for predicting the damage progression in real structures, as failure initiates at the vicinity of a stress concentrator, causing stress redistribution and the gradual spread of damage until the global failure of the structure. The implementation of the stiffness and strength degradation models in the principal material directions of the unidirectional ply was thoroughly discussed. Details were also presented on the FE models developed, the computational effort needed and the definition of final failure considered. Numerical predictions were corroborated satisfactorily by experimental data from constant amplitude uniaxial fatigue of multidirectional glass/epoxy laminates under various stress ratios. The validation of predictions included fatigue strength, stiffness degradation and residual static strength after cyclic loading.     

Mode I fatigue delamination growth in GFRP woven laminates at low temperatures

The cryogenic fatigue delamination behavior of glass fiber reinforced polymer woven laminates under Mode I loading has been investigated experimentally and numerically. Fatigue delamination tests were conducted using double cantilever beam specimens at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K). Fracture surface examination using scanning electron microscopy revealed delamination mechanisms under fatigue loading. A finite element analysis was also employed to calculate the J-integral range and damage distributions. The effects of temperature and loading condition on the fatigue delamination growth rates were discussed.     

Elevated temperature off-axis fatigue behavior of an eight-harness satin woven carbon-fiber/bismaleimide laminate

The off-axis tensile fatigue behavior of a woven fiber/bismaleimide laminate is investigated at various temperatures. Emphasis was placed on characterization of the laminates and the development of an analytical fatigue damage model. Fatigue tests revealed that the material exhibits an atypical three-stage response in terms of stiffness degradation and permanent strain. Fiber yarn rotation was found to be a dominant mechanism in the initial stage of cycling causing high permanent strain and slight stiffness increase, while damage accumulation due to cyclic loading was dominant in the final stage causing rapid stiffness degradation. The mean strain variation during cycling was found to be proportional to the test temperature in each stage, and thus a more meaningful indicator for fatigue damage development. The corresponding analytical damage model was able to accurately capture the three-stage damage development. The current model can be used to determine damage development for cyclic loading at intermediate temperatures.     

Impact and subsequent fatigue damage growth in carbon fibre laminates

The influence of the ply stacking sequence on the impact resistance and subsequent O-tension fatigue performance of carbon fibre laminates has been investigated. Drop-weight impact tests were conducted on a range of 16 ply carbon fibre laminates with either all non-woven plies or mixtures of woven and non-woven plies. Damaged coupons were tested in O-tension fatigue for up to 10⁶ cycles, scanned using an ultrasonic probe and then loaded in tension until failure.The impact resistance and subsequent fatigue performance have been found to be sensitive to the ply stacking sequence. The non-woven composites showed a marked sensitivity to impact loading, but increases in residual static strength were noted after cycling. The inclusion of a woven fabric served to improve the impact resistance of the laminates. Fatigue cycling resulted in considerably improved residual static strengths; by 10⁶ cycles any effect of the impact damage had been removed.     

Interlaminar shear properties of composite insulation systems for fusion magnets at cryogenic temperatures

This paper reports the cryogenic interlaminar shear properties of composite insulation systems for the superconducting magnet coils in the International Thermonuclear Experimental Reactor (ITER). Short beam shear tests were performed at room temperature, liquid nitrogen temperature (77 K) and liquid helium temperature (4 K) on three insulation systems consisting of woven glass fiber reinforced plastic (GFRP) composites with different polymer resins and polyimide films, and the dependence of their apparent interlaminar shear strength on the temperature and the polymer resins was discussed. A detailed observation of failed specimens was made to verify the failure mechanisms. Insulation systems subjected to gamma irradiation at room temperature were also considered, and the effect of irradiation on the cryogenic interlaminar shear properties was examined.