An instrumentation system for multi-parameter measurements of gas-solid two-phase flow based on Capacitance-Electrostatic sensor

In this paper, an instrumentation system for the measurements of local solid volumetric concentration, local solid velocity, local solid mass flowrate and solid mass flowrate in gas-solid two-phase flow system is developed. It is based on a new type of a Capacitance-Electrostatic sensor (CES). The CES sensor is mainly composed of a capacitance electrode array and two electrostatic electrode arrays. The optimum design of the sensor is achieved by finite element method. The capacitance electrode array is employed to detect the solid distribution over the cross-section of the pipe, and the local solid volumetric concentration measurement is further derived. The electrostatic electrode arrays are used to measure the local solid velocities in conjunction with cross-correlation method. From the local solid velocity and local volumetric concentration, the solid mass flowrate and the local solid mass flowrate can be achieved. The developed system for the local solid volumetric concentration measurement is verified through analogue simulation experiments and static experiments. Finally, the system is employed to measure the local solid volumetric concentration, local solid velocity, local solid mass flowrate and solid mass flowrate on a belt conveyor. The experimental results show that the measurement error of the local solid volumetric concentration measurement results are less than 10.43% for solid local volumetric concentration ranging from 0.02 to 0.56, the standard deviations of the local solid velocity measurement results are less than 0.42 for solid velocity ranging from 3.5 m/s to 15.0 m/s, and the relative error of the solid mass flowrate is within −19.6% to +14.9% for solid mass flowrate ranging from 0.006 kg/s to 0.103 kg/s, indicating that the system is capable of achieving multi-parameters measurement in gas-solid two-phase flow system.     

Non-contact temperature measurement of silicon wafers based on the combined use of transmittance and radiance

We propose a non-contact temperature measurement method that combines the temperature dependence of transmittance below 600 °C and radiation thermometry above 600 °C. The combined method uses a polarization technique and the Brewster angle between air and a dielectric film such as SiO₂ or Si₃N₄ grown on silicon wafers. A prominent feature of this method is that both measurements of transmittance and radiance are performed with the same geometrical arrangement.For a semitransparent wafer, the measurement of p-polarized transmittance at the wavelengths of 1.1, 1.2 and 1.3 μm enables temperature measurement in the range from room temperature to 600 °C. For an opaque wafer above 600 °C, the p-polarized radiation thermometry at the wavelength of 4.5 μm allows the temperature measurement without the emissivity problem. The combined method with the use of transmittance and radiance is valid in the entire temperature range irrespective of variations of film thickness and resistivity.     

Miniaturized liquid film sensor (MLFS) for two phase flow measurements in square microchannels with high spatial resolution

Two miniaturized liquid film sensors (MLFS) based on electrical conductance measurement have been developed and tested. The sensors are non-intrusive and produced with materials and technologies fully compatible and integrable with standard microfluidics. They consist of a line of 20 electrodes with a purpose-designed shape, flush against the wall, covering a total length of 5.00 and 6.68 mm. The governing electronics achieve 10 kHz of time resolution. The electrode spacing of the two sensors is 230 μm and 330 μm, which allows measurements of liquid films up to 150 μm and 400 μm for sensors MLFS_A and MLFS_B, respectively. The sensor characteristics were obtained by imposing static liquid films of known thickness on top of the actual sensor. Further dynamic measurements of concurrent air-water flow in a horizontal microchannel were performed. The line of electrodes is placed across the flow direction with an angle of 3.53° from the direction of flow, allowing for a spatial resolution perpendicular to the flow of 14.2 μm for sensor MLFS_A and 20.5 μm for sensor MLFS_B. The high time and spatial resolution allows for fast and accurate detection of the presence of bubbles, and even measurement of film thickness and bubble velocity. Further information, such as the bubble shape, can be gathered based on the shape of the liquid layer underneath the bubble, which is particularly important for heat transfer studies in microchannels.     

Assembly and constraint technology for large arrays of capillaries

Discovering the genetic causes of common diseases may require pan-genomic mutation scanning of all genes in a million people. An increase in throughput of genetic analysis instrumentation by several orders of magnitude is essential to undertake such an ambitious task. To this end, we report on the design, manufacture, and testing of assembly and constraint technologies for arrays containing as many as 10,000 capillaries packed into 1-D rows or 2-D arrays with 1 mm spacing. Capillaries are sealed around their perimeters against pneumatic and hydrodynamic pressures useful for automated capillary array electrophoresis. We show that both ends of the arrayed capillaries are aligned axially to 11 ± 5 μm accuracy and repeatability. Radially, the capillary tips are aligned well enough for insertion into arrays of sample wells and subsequent end-of-capillary fluorescence detection. We have loaded, electrophoresed, and detected 10⁸ to 10¹⁰ fluorescently labeled DNA molecules in a 25 capillary sub-array to validate functionality. Using our semi-automated assembly machine, we demonstrate 100 capillary array assembly in 12 min. This array assembly and constraint technology could be incorporated into commercial capillary instruments, and may enable a new generation of ultrahigh throughput instruments with 2-D arrays of 10,000 or more capillaries.     

Pulverized coal flow metering on a full-scale power plant using electrostatic sensor arrays

On-line continuous monitoring of pulverized coal in fuel injection pipes will allow power plant operators to optimize fuel conveying conditions and ultimately to achieve higher combustion efficiency and lower atmospheric emissions. This paper presents the design, implementation and trials of a prototype instrumentation system for the on-line measurement of pulverized coal on a full-scale power plant. An array of three identical arc-shaped electrostatic electrodes is housed in a sensing head to derive particle flow signals. Pulverized coal flow parameters such as velocity, mass flow rate and fuel distribution among the injection pipes from the same pulverizing mill are obtained by processing the signals and fusing the resulting measurements. On-plant demonstration trials on 560 mm bore pneumatic conveying pipes feeding a 600 MW boiler were undertaken following system evaluation tests on a 50 mm bore laboratory test rig. Experimental results demonstrate that reliable monitoring of pulverized coal flow parameters is achieved and that the system is able to track both transient and long-term fluctuations of pulverized coal flow in fuel injection pipes under real power plant conditions.     

Investigations on pressure dependence of Coriolis Mass Flow Meters used at Hydrogen Refueling Stations

In the framework of the ongoing EMPIR JRP 16ENG01 “Metrology for Hydrogen Vehicles” a main task is to investigate the influence of pressure on the measurement accuracy of Coriolis Mass Flow Meters (CFM) used at Hydrogen Refueling Stations (HRS). At a HRS hydrogen is transferred at very high and changing pressures with simultaneously varying flow rates and temperatures. It is clearly very difficult for CFMs to achieve the current legal requirements with respect to mass flow measurement accuracy at these measurement conditions. As a result of the very dynamic filling process it was observed that the accuracy of mass flow measurement at different pressure ranges is not sufficient. At higher pressures it was found that particularly short refueling times cause significant measurement deviations. On this background it may be concluded that pressure has a great impact on the accuracy of mass flow measurement. To gain a deeper understanding of this matter RISE has built a unique high-pressure test facility. With the aid of this newly developed test rig it is possible to calibrate CFMs over a wide pressure and flow range with water or base oils as test medium. The test rig allows calibration measurements under the conditions prevailing at a 70 MPa HRS regarding mass flows (up to 3.6 kg min⁻¹) and pressures (up to 87.5 MPa).     

Application of ultrasonic Doppler velocimetry to molten glass by using broadband phase difference method

An ultrasonic velocity profile (UVP) measurement in high temperature molten glass was presented using buffer rod technique. A ceramic buffer rod was used to transmit ultrasound into molten glass. The rod had a taper shape and porous cladding to suppress trailing echo, which is the spurious echo in the buffer rod measurement. The broadband signal processing method was presented to improve noise tolerance in velocity estimation. This method is based on the phase difference method, which is originally proposed as a narrowband method. Measurable distance of the UVP measurement was investigated combining the buffer rod and the broadband signal processing method. Experiment was conducted at the temperature from 1000 °C to 1200 °C. As a preliminary test, motion tracking in molten glass was successfully demonstrated.     

Fabrication of disk microelectrode arrays and their application to micro-hole drilling using electrochemical micromachining

Minimal-taper microholes are widely used in modern industries. Electrochemical micromachining (EMM) has been demonstrated to be a feasible method to fabricate these microholes. In this study, based on its unique processing properties and productivity, a disk microelectrode array was fabricated via electrolysis for producing micro-holes. The dimensions of the cathode for hydrolysis were optimized by applying the finite element method to the constructed physical model. A 3 × 3 disk microelectrode array and a 5 × 5 cylindrical microelectrode array with uniform dimensions were then fabricated using the optimized cathode. Micro-holes were drilled on stainless-steel plates using both disk and cylindrical microelectrode arrays. The taper of the resulting micro holes obtained using the new disk microelectrode array was lower than that of the holes formed using the cylindrical microelectrode array. The effects of EMM parameters, including the applied voltage, feeding speed, and pulse-on time, on the hole diameter and taper were also investigated. The results suggest that appropriate machining parameters should be selected in consideration of the effects of these parameters on hole diameter, taper, localization, and material removal rate.     

An ultra high-pressure test rig for measurements of small flow rates with different viscosities

Within the framework of a research project regarding investigations on a high-pressure Coriolis mass flow meter (CMF) a portable flow test rig for traceable calibration measurements of the flow rate (mass - and volume flow) in a range of 5 g min⁻¹ to 500 g min⁻¹ and in a pressure range of 0.1 MPa to 85 MPa was developed. The measurement principle of the flow test rig is based on the gravimetrical measuring procedure with flying-start-and-stop operating mode. Particular attention has been paid to the challenges of temperature stability during the measurements since the temperature has a direct influence on the viscosity and flow rate of the test medium. For that reason the pipes on the high-pressure side are double-walled and insulated and the device under test (DUT) has an enclosure with a separate temperature control. From the analysis of the first measurement with tap water at a temperature of 20 °C and a pressure of 82.7 MPa an extensive uncertainty analysis has been carried out. It was found that the diverter (mainly due to its asymmetric behaviour) is the largest influence factor on the total uncertainty budget. After a number of improvements, especially concerning the diverter, the flow test rig has currently an expanded measurement uncertainty of around 1.0% in the lower flow rate range (25 g min⁻¹) and 0.25% in the higher flow rate range (400 g min⁻¹) for the measurement of mass flow. Additional calibration measurements with the new, redesigned flow test rig and highly viscous base oils also indicated a good agreement with the theoretical behaviour of the flow meter according to the manufacturers׳ specifications with water as test medium. Further improvements are envisaged in the future in order to focus also on other areas of interest.     

Effects of flow patterns and salinity on water holdup measurement of oil-water two-phase flow using a conductance method

This research investigates the effects of flow pattern and salinity of oil-water two-phase flow on water holdup measurement using a conductance method. Firstly, vertical upward oil-water two-phase flow experiment is conducted in a 20 mm inner diameter (ID) pipe, in which the salinities of aqueous solutions are set as 151 ppm, 1003 ppm, 2494 ppm and 4991 ppm respectively. Experimental water-cut and mixture velocity are set as 80–100% and 0.0184–0.2576 m/s. In the experiment, three different flow patterns, i.e., dispersed oil-in-water slug flow (D OS/W), dispersed oil-in-water flow (D O/W) and very fine dispersed oil-in-water flow (VFD O/W) are observed and recorded by a high speed camera. Meanwhile, we collect the response of Vertical Multiple Electrode Array (VMEA) conductance sensor excited by a sine voltage signal. The result shows that, for VFD O/W, the water holdup from VMEA sensor shows a satisfied agreement with that of quick closing valve (QCV) method under certain salinities, i.e., 1003 ppm as well as 2494 ppm. For D OS/W flow and D O/W flow characterized by dispersed oil droplets with various sizes, considerable deviations of water holdup between VMEA sensor and QCV method under four kinds of salinity aforementioned are presented. Afterward, according to experimental analysis along with theoretical deviation, it is concluded that the deviation of the measurement system reaches its minimum when reference resistance in the measurement circuit and salinity of the aqueous solution satisfy constraint conditions, and the accuracy of water holdup using the conductance method can be improved through adjusting reference resistance to match the salinity of water phase. Finally, the recurrence plot algorithm is utilized to identify typical flow patterns mentioned above and it shows satisfied results on comprehending the discrepancies among different flow patterns, demonstrating that the recurrence plot algorithm can be effectively applied in flow pattern identification regarding oil-water flows.     

Measurement of vertical oil-in-water two-phase flow using dual-modality ERT–EMF system

Oil-in-water two-phase flows are often encountered in the upstream petroleum industry. The measurement of phase flow rates is of particular importance for managing oil production and water disposal and/or water reinjection. The complexity of oil-in-water flow structures creates a challenge to flow measurement. This paper proposes a new method of two-phase flow metering, which is based on the use of dual-modality system and multidimensional data fusion. The Electrical Resistance Tomography system (ERT) is used in combination with a commercial off-the-shelf Electromagnetic Flow meter (EMF) to measure the volumetric flow rate of each constituent phase. The water flow rate is determined from the EMF with an input of the mean oil-fraction measured by the ERT. The dispersed oil-phase flow rate is determined from the mean oil-fraction and the mean oil velocity measured by the ERT cross-correlation velocity profiling. Experiments were carried out on a vertical upward oil-in-water pipe flow, 50 mm inner-diameter test section, at different total liquid flow rates covering the range of 8–16 m³/hr. The oil and water flow rate measurements obtained from the ERT and the EMF are compared to their respective references. The accuracy of these measurements is discussed and the capability of the measurement system is assessed.     

Performance tests of a new non-invasive sensor unit and ultrasound electronics

Industrial applications involving pulsed ultrasound instrumentation require complete non-invasive setups due to high temperatures, pressures and possible abrasive fluids. Recently, new pulser-receiver electronics and a new sensor unit were developed by Flow-Viz. The complete sensor unit setup enables non-invasive Doppler measurements through high grade stainless steel. In this work a non-invasive sensor unit developed for one inch pipes (22.5 mm ID) and two inch pipes (48.4 mm ID) were evaluated. Performance tests were conducted using a Doppler string phantom setup and the Doppler velocity results were compared to the moving string target velocities. Eight different positions along the pipe internal diameter (22.5 mm) were investigated and at each position six speeds (0.1–0.6 m/s) were tested. Error differences ranged from 0.18 to 7.8% for the tested velocity range. The average accuracy of Doppler measurements for the 22.5 mm sensor unit decreased slightly from 1.3 to 2.3% across the ultrasound beam axis. Eleven positions were tested along the diameter of the 48.4 mm pipe (eight positions covered the pipe radius) and five speeds were tested (0.2–0.6 m/s). The average accuracy of Doppler measurements for the 48.4 mm sensor unit was between 2.4 and 5.9%, with the lowest accuracy at the point furthest away from the sensor unit. Error differences varied between 0.07 and 11.85% for the tested velocity range, where mostly overestimated velocities were recorded. This systematic error explains the higher average error difference percentage when comparing the 48.4 mm (2.4–5.9%) and 22.5 mm (1.3–2.3%) sensor unit performance. The overall performance of the combined Flow-Viz system (electronics, software, sensor) was excellent as similar or higher errors were typically reported in the medical field. This study has for the first time validated non-invasive Doppler measurements through high grade stainless steel pipes by using an advanced string phantom setup.     

Design and experimental validation of an ultra-precision Abbe-compliant linear encoder-based position measurement system

The design and development of an Abbe-compliant linear encoder-based measurement system for position measurement with a targeted 20 nm uncertainty (k = 2) in machine tools and CMMs is presented. It consists of a linear scale and a capacitive sensor, mounted in line on an interface which is guided in the scale's measurement direction and driven by a linear motor based on the output signal of the capacitive sensor. The capacitive sensor measures the displacement of a target surface on the workpiece table. The functional point, which is the center of a tool or touch probe, is always aligned with the scale and capacitive sensor such that this configuration is compliant with the Abbe principle. Thermal stability is achieved by the application of a thermal center between the scale and capacitive sensor at the tip of the latter, which prevents both components to drift apart. Based on this concept, a prototype of a one-DOF measurement system was developed for a measurement range of 120 mm, together with an experimental setup aimed at verifying the reproducibility of the system for changing ambient conditions of ±0.5 °C and ±5%rh and the repeatability during tracking of a target surface over a short period of time. These experiments have shown that the measurement uncertainty of the one-DOF system is below 29 nm with a 95% confidence level.     

A motorized 5 m tape comparator for traceable measurements of tapes and rules

A motorized 5 m tape comparator was constructed in TUBITAK UME for calibration of tapes and rules up to 5 m length in one set-up and further lengths in multiple set-ups. The system is a practical development and provides a cost effective solution for calibration of tapes in which the highest grade’s accuracy requirement in OIML R35-1 e.g. is 600 μm for 5 m length and 1100 μm for 10 m length. It is mainly composed of 6 m rail system, mechanical parts, optical units and an integrated 6 m incremental linear encoder as a reference measurement axis for traceable measurements. The rails are kinematically located on a heavy marble construction and a motorized carriage, which employs a camera for probing of the scales on the tapes, is moved along the rails during the measurement. The image of the scale taken by the camera is viewed on the monitor screen together with the running software. The operator can perform the probing process by simply moving the carriage over the measured scales (tapes or rules) using a joystick. The carriage movement is measured by the incremental linear encoder previously calibrated by a laser interferometer and the software automatically takes the measurement results from the incremental linear encoder, applies correction values previously defined and determines the length of the tapes and rules as well as deviations from nominal lengths. The estimated expanded uncertainty of the steel tape measurement is U = 54 μm in one set-up (for 5 m length) and U = 77 μm in two set-ups (for 10 m length) at the confidence level of approximately 95%. Uncertainty budget for calibration of the device itself and for calibration of the test tapes are explained in detail. The results of extensive experimental work and analysis are provided by demonstrating application of science and technology of measurement and instrumentation. Investigations for long term stability of the system are given with the reported test results for the years of 2003-2011 and participated intercomparison results to validate the device scientifically are illustrated.     

An improved portable biosensing system based on enzymatic chemiluminescence and magnetic immunoassay for biological compound detection

In this paper, an improved portable biosensing system has been developed for biological compounds detection. The device is based on enzymatic chemiluminescence and magnetic immunoassay with a miniaturized flow injection module. The immunoassay procedure involved a sandwich format, in which the antigen in the sample was first captured by the immobilized primary antibody on the surface of the magnetic beads, and then recognized by the second antibody labeled with enzyme. 3-(2′-spiroadamantyl)-4-methoxy- 4-(3″-phosphoryloxy)-phenyl-1,2-dioxetane (AMPPD) as the substrate amplified the enzymatic signal for the biological compound measurement. The portable biosensing system was characterized in a series of experiments with cardiac troponin I (cTnI), a golden standard protein marker for diagnosis of myocardial infarction, as a biological substance measurement model. It provided a linear response range of cTnI from 0.1 to 50 ng mL⁻¹ (R = 0.99). The coefficient of variation was 6.7% in the repeatability test (n = 6). The novel system has great potential applications in the rural and community hospitals and can be easily extended to a variety of protein compounds analysis.     

Low flow regime measurements with an automatic pulse tracer velocimeter (APTV) in heterogeneous aquatic environments

Cost-effective velocity measurements at lab and field scales are required for understanding and modeling the flow characteristics in aquatic environments such as constructed wetlands, coastal marshes, lakes and reservoirs. This paper presents a new measurement device—the automatic pulse tracer velocimeter (APTV) that is designed to measure water velocities for low flow regimes (0.2–5.0 cm s⁻¹) in heterogeneous aquatic environments using NaCl pulse tracer measurements. Hydraulic data collected in a laboratory-scale flume and field-scale constructed wetland were analyzed to determine velocity, directional flow and dispersion coefficients measured by using a cross-type and arc-type APTV. Acoustic Doppler velocimeters (ADVs) were used to collect calibration measurements in a hydraulic flume to gain fundamental understanding in support of field experiments. To test the effects of vegetation, four scenarios of laboratory-scale tests having both submerged and emergent artificial vegetation were conducted in a flume including; (1) no artificial vegetation (NAV), (2) submerged artificial vegetation (SAV) (3) emergent artificial vegetation (EAV), and (4) mix artificial vegetation (MAV). Directional flow detection and simulated storm event flow tests were conducted using an arc-type APTV data in the flume to gain perspectives of APTV performance in variable flow conditions. Cross-type APTV pulse data were eventually analyzed to determine dispersion coefficients based on the tracer curves. Finally APTVs were tested alongside an ADV for a three-day duration in a constructed wetland nearby the Everglades, Florida. Operating advantages of the APTV compared to other similar sensors were summarized in the end to enhance the application potential. Results indicate that APTVs are ideal device for affordable measurements of velocities in a 0.2–4.5 cm s⁻¹ range with the prediction of both velocity field, direction and dispersion coefficients, and capable of autonomous deployment and control in a sensor network.     

Concentration measurement with thermal probe for pulverized coal in the pneumatic pipeline of power plant

The concentration measurement of pulverized coal in a pneumatic pipeline is a challenging issue in power plant. A thermal probe manufactured with abrasion-proof steel was developed for coal concentration measurement in such a situation. The probe generates 15 W of heat. This method is based on the heat transfer between the thermal probe and the gas–solid two-phase flow. Experiments were conducted in a horizontal pneumatic pipeline to assess the accuracy of the thermal probe, where the gas was air and the solid was pulverized coal with mean diameter of 65 µm. The wall temperature of the thermal probe was found to be dependent on both coal powder concentration and air velocity. A new heat transfer correlation was proposed in terms of the modified Reynolds and Nusselt numbers for the gas–solid two-phase flow across the thermal probe. In the range of coal powder concentration from 0.1 to 0.65 kg/kg, the standard deviation is 0.01 kg/kg for the thermal probe. The thermal probe has potential application for concentration measurement of pulverized coal in the pneumatic pipelines of power plants.     

Calculation of scattering parameters in multiple-interface transmission-line transducers

Transmission-line scattering parameters becomes unpractical to calculate as one includes more interfaces. Thus, to get an analytical expression, approximations are required. In this paper, an approximation methodology for the calculation of scattering parameters of transmission-line transducers is presented. The transducer cell is partitioned at each interface and the partial scattering equations are calculated, considering two interfaces at a time. Next, standard techniques are applied to solve the signal-flow diagrams to obtain the full scattering equations. Transmission-line transducers are used for the measurement of power absorption and reflection of different materials, such as: liquids, granular medium, and ground, in the RF/microwave range. Such measurements are used to extract materials properties. The proposed methodology has been applied to a coaxial transducer cell filled with different low-loss liquids. The results have been validated with computer simulations and experimental measurements. Measurements and simulations were carried out in the 300 kHz to 3 GHz frequency range.     

Measurement and statistical analysis toward reproducibility validation of AZ4562 cylindrical microlenses obtained by reflow

This paper presents the statistical analysis applied into the shape of microlenses (MLs) for validating the high-reproducibility feature of their fabrication process. The MLs were fabricated with the AZ4562 photoresist, using photolithography and thermal reflow processes. Two types of MLs arrays were produced for statistical analysis purposes: the first with a cross-sectional diameter of 24 μm and the second with a cross-sectional diameter of 30 μm, and both with 5 μm spacing between MLs. In the case of 24 μm diameter arrays, the measurements showed a mean difference in diameter of 2.78 μm with a standard deviation (SD) of 0.22 μm (e.g., 2.78 ± 0.22 μm of SD) before the reflow, and 2.34 ± 0.35 μm of SD after the reflow. For the same arrays, the mean difference in height obtained was, comparatively to the 5.06 μm expected, 0.76 ± 0.10 μm of SD before the reflow and 1.91 ± 0.15 μm of SD after the reflow, respectively. A mean difference in diameter of 2.64 ± 0.41 μm of SD before the reflow, and 1.87 ± 0.34 μm of SD after the reflow was obtained for 30 μm diameter MLs arrays. For these MLs, a mean difference in height of 0.71 ± 0.12 μm of SD before the reflow and 2.24 ± 0.24 μm of SD after the thermal reflow was obtained, in comparison to the 5.06 μm of height expected to obtain. These results validate the requirement for reproducibility and opens good perspectives for applying this fabrication process on high-volume production of MLs arrays.