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TiN薄膜的合成及其性能研究 总被引:1,自引:0,他引:1
用电子束蒸发沉积钛和40keV氮离子束轰击交替进行的办法合成了TiN薄膜。用RBS,AES,TEM,XPS,和X射线衍射研究TiN薄膜的组分和结构表明:用离子束增强沉积制备的TiN薄膜主要由TiN相构成;晶粒大小为30—40um,无择优取向;而非离子束轰击沉积的薄膜则是无定形的;用离子束增强沉积制备的TiN薄膜,其氧含量明显小于无离子束轰击薄膜的值;在TiN薄膜和衬底之间存在一个界面混合区,厚度为40um左右。机械性能测试表明,TiN薄膜具有高的显微硬度,低的摩擦系数。 相似文献
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本文建立了一个适用于描述离子束增强沉积(Ion Beam Enhanced Deposition,即IBED)过程的Monte-Carlo计算机模拟程序。程序由离子注入计算和蒸发沉积计算两大部分组成。离子注入计算以二体碰撞近似为基础,以随机固体为靶模型,对入射离子和所有反冲原子的力学运动进行跟踪。程序中考虑了沉积原子对靶室中某些残余气体分子的吸附;还表达了靶的组份及密度在IBED过程中的不断变化,从而实现了靶的动态化。该程序可以提供IBED薄膜组份的深度分布、界面混合以及能量沉积等信息。计算结果表明,在IBED氮化钛薄膜中,Ti沉积速率对薄膜组份有很大影响。当沉积速率较低时,薄膜组份基本与注入离子和沉积原子的到达率比(N/Ti)无关。膜与基体间的混合层厚度随离子原子到达率比(N/Ti)增加而增加。计算结果与实验测试结果符合很好。 相似文献
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WANG Xi YANG Genqing LIU Xianghuai ZHENG Zhihong HUANG Wei ZHOU Zuyao ZOU Shichang Ion Beam Laboratory Shanghai Institute of Metallurgy Academia Sinica shanghai China 《金属学报(英文版)》1992,5(11):370-374
A new method for preparation of hard TiN films has been developed by using electronbeam evaporation-deposition of Ti and bombardment with 40 keV Xe~+ ion beam ina N_2 gas environment.The synthesized TiN films were superior to PVD and CVDones in respects of improved adhesion to substrate and low preparing temperature.Theyexhibited good wear resistance and high hardness up to 2200 kg/mm~2.Some industrialapplications have been reported. 相似文献
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用离子束增强沉积方法制备了SiN薄膜,其中Si由一束Ar离子从Si靶上溅射下来,在溅射沉积的同时,以一束N离子轰击正在沉积的膜层,于是获得了SiN膜。采用卢瑟福背散射、红外光谱和透射电镜对膜层的成分和结构进行了分析,结果表明:膜面平整,膜层为非晶或微晶结构,由Si和βSi3N4组成 相似文献
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JIANG Hai TAO Kun LI Hengde Tsinghua University Beijing China lecturer Department of Materials Science Engineering Tsinghua University Beijing China 《金属学报(英文版)》1993,6(11):379-382
BN films,synthesized by ion beam assisted deposition,were analysed by RBS,AES,IR spectra and TEM.Formatiom of c-BN phase was shown not only by IR spectra atabsorption peak of 1100 cm~(-1),but also by electron diffraction pattern.The results ofAES demonstrate an effect of N~+ implantation near the film surface.The deposited filmsconsist of three layers,i.e.,ion implantation layer,film layer and mixed intermediatelayer,according to the difference of concentration.The micro-Knoop hardness of the film is25—35 GPa. 相似文献
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用单源低能氩离子束辅助沉积(IBAD)法制备了非晶碳薄膜.氩离子能量为400-1500eV.膜面光滑致密,与衬底的结合力较高。用Raman,FTIR,HRTEM,TED,SEM,ERD及RBS研究了薄膜的形貌、结构和组分,测量了膜的电阻率、显微硬度及摩擦系数.薄膜为无定形的类金刚石(DLC).其中含氢约为205at.-%,碳原子与氢原子几乎没有形成C-H键.随着离子束能量及束流的增加,显微硬度、摩擦系数增加,电阻率减小.硬度增加是由于薄膜致密度的增加,而电阻率降低是由于膜中金刚石键(sp~3键)含量减少的缘故. 相似文献
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B. Zhao F. Zeng DM. Li F. PanLaboratory of Advanced Materials Department of Materials Science Engineering Tsinghua University Beijing China 《金属学报(英文版)》2003,16(4):266-270
The Cu25 Nb75 and Ni45Nb55 amorphous films with about 500nm thickness were prepared by ion beam assisted deposition (IBAD). Potentiodynamic polarization measurement was adopted to investigate the corrosion resistance of samples and the tests were carried out respectively in 1mol/L H2SO4 and NaOH aquatic solution. The corrosion performance of the amorphous films was compared with that of multilayered and pure Nb films. Experimental results indicated that the corrosion resistance of amorphous films was better than that of the corresponding multilayers and pure Nb films for both Ni-Nb system with negative heat of formation and Cu-Nb system with positive heat of formation. 相似文献
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离子束增强沉积得到的TiN表面改性薄层的电子衍射强度与氮离子的注入能量有关,利用自编程序对其电子衍射强度和键强度作了计算,结果表明注入能量较高时出现的电子衍射强度异常现象是由于晶格中部分N原子的间隙位置发生了变化,这导致键强度也产生相应的变化. 相似文献
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采用等离子体浸没离子注入与沉积(PIII&D)技术在AISI 52100轴承钢表面合成了高硬耐磨的TiN薄膜.膜层元素分布、化学组成和表面形貌分别用XRD,XPS表征.合成薄膜前后试样的滚动接触疲劳寿命和摩擦磨损性能分别由球棒疲劳磨损试验机和球-盘磨损试验机测定;疲劳破坏后的微观形貌通过SEM观察;薄膜力学性能经纳米压痕和纳米划痕实验评价.结果表明,TiN膜中还含有少量的TiO2和Ti,N,O的化合物.在优化条件下,TiN膜层致密均匀,与基体结合良好,纳米硬度和弹性模量分别达到25和350 GPa;最低摩擦系数由基体的0.92下降到0.2.被处理薄膜试件在90%置信区间下的最大L10,L50,La和-↑L寿命较基体分别提高了约4.5,1.8,1.3和1.2倍,疲劳寿命的分散性得到了显著改善. 相似文献
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T.H.Zhang Z.Z.Yi X.Y.Wu S.J.Zhang Y.G.Wu X.Zhang H.X.Zhang A.D.Liu X.J.Zhang 《金属学报(英文版)》2002,15(2):187-190
Mo silicides MosSi3 with high quality were prepared using ion beam deposition equip-ment with two Filter Metal Vacuum Arc Deposition (FMEVAD). When the numberof alternant deposition times was 198, total thickness of the coating is 40nm. Thecoatings with droplet free can be readily obtained, so the surface is smooth. TEMobservation shows that Mo and Si alternant deposition coating is conpact structure.The fine Mo silicide grains densely distributed in the coating. The coating adherenceon silicon is excellent. 相似文献