ZTA陶瓷刀具连续切削淬硬T10A时的切削性能研究

研究两种自主研制的新型ZTA(Al2O3/Zr O2)陶瓷刀具切削淬硬T10A时的切削性能。刀具后刀面磨损量随切削深度和切削速度的增加而增大;刀具的主要磨损形态为后刀面磨损;主要磨损机理为后刀面磨粒磨损和部分粘结磨损。     

Effects of Loading and Sliding Speed on the Dry Sliding Wear Behavior of Mg-3Al-0.4Si Magnesium Alloy

The friction and wear properties of Mg-3Al-0.4Si alloy were investigated using a pin-on-disc tester. Morphologies and compositions of worn surfaces were characterized by scanning electron microscopy (SEM) and energy dispersive X-ray spectrometry (EDS) for identification of the wear mechanisms. Microstructural evolution and hardness change in subsurfaces were analyzed by confocal scanning laser microscopy and hardness testing. The results revealed that the wear behavior of Mg-3Al-0.4Si alloy was classified into two types of wear regimes; that is, mild and severe. In the mild wear regime, wear rates increased at a low slope with increasing load; the corresponding wear mechanisms were oxidation, abrasion, and delamination. In the severe wear regime, wear rates increased rapidly at a high slope with load; the wear mechanisms were severe plastic deformation and surface melting. Analysis of microstructural evolution on the subsurface identified the reason for the transition from mild to severe wear; that is, the realization of dynamic recrystallization (DRX) in the surface layer material. A contact surface DRX temperature criterion for the mild to severe wear transition was proposed, and the critical DRX temperatures for the mild to severe wear transition were calculated using DRX kinetics.     

The Effect of Heat Treatment on Sliding Wear Behaviour of a Zinc-Based Alloy Containing Nickel and Silicon

This investigation deals with the observations made pertaining to the sliding wear behaviour of a zinc-based alloy containing nickel and silicon in partially lubricated condition. Wear tests were conducted over a range of applied pressures and sliding speeds. The effect of microstructural changes brought about through T6 heat treatment involving solutionizing followed by artificial ageing on wear behaviour was also investigated. The wear rate increased with pressure. The slope of the wear rate versus pressure plots was low initially up to a specific pressure. This was followed by a higher slope beyond the (specific) pressure. In some cases, the rate of change in wear rate, i.e. the slope, decreased at still higher pressures. Moreover, the (specific) pressure decreased with sliding speed in general. Increasing sliding speed caused the wear rate of the as-cast zinc-based alloy to increase up to a sliding speed of 2.68m/s. The trend reversed at a still higher speed of 4.60m/s. However, increasing wear rate with speed was noted for the heat-treated alloy over the entire speed range. Heat treatment led to reduced wear rate up to a sliding speed of 2.68m/s. An opposite trend was observed at a higher speed of 4.60m/s in this case. Specimen seizure was noted at speeds above 2.68m/s in the case of the as-cast alloy whereas seizure took place only at 4.60m/s for the heat-treated alloy samples. Frictional heating increased with pressure and speed. The specific response and changing mode of distribution of various phases were thought to be responsible for the typical wear behaviour of the alloy in specific material and test conditions. The predominance of parameters like thermal stability and cracking tendency over each other is suggested to lead to the varying wear behaviour of the alloy in different (material and sliding) conditions. The wear response of the samples has been substantiated through characteristics of their wear surfaces, subsurface regions and debris.     

On the fretting wear mechanism of Zr-alloys

Zirconium alloys are highly desirable in nuclear applications due to their transparency to thermal energy neutrons and for their high corrosion resistance. The main objective of this study is to investigate the fretting wear mechanism of Zr–2.5%Nb alloy. The experimental work was carried out in air at 265 °C, using a specially designed fretting wear tribometer. The transfer of material, the change in the wear volume and the maximum wear depth with the number of cycles were measured through 3D mapping of the topography of the fretted surface. SEM and Fourier Transform Infrared Interferometry methods were used to examine the microspall pits and to measure the distribution of the thickness of oxide layer in the fretting region. For relatively small slip amplitude, the results showed that the fretting wear mechanism is initially dominated by adhesion and abrasion actions and then by delamination and surface fatigue. The time variation of the wear losses was shown to be cyclic until a steady state value is reached. At high slip amplitudes, however, abrasion and delamination are the only dominant wear mechanisms. The volumetric wear losses were found to decrease monotonically with the number of cycles. A novel approach was introduced, whereby the thermal and electrical contact resistances of the fretting interface are simultaneously measured. The results demonstrated the potential use of this non-intrusive approach for real-time monitoring of the fretting wear mechanism.     

Al2O3陶瓷阀芯耐磨性的研究

从陶瓷零件副的实际应用出发,采用失重法研究了Al2O3陶瓷的磨损情况,根据磨损结果,分析了陶瓷材料的磨损表面,磨损机理,表明陶瓷的磨损率较低,具有广阔的应用前景。     

Tribological characterization of alumina and silicon carbide under lubricated sliding

The aim of this study was to investigate the tribological properties of four different advanced ceramics - monolithic alumina, SiC whisker-reinforced alumina, monolithic silicon carbide and SiSiC-during lubricated sliding. Advanced techniques of electron microscopy and spectroscopy have been used to characterize the materials before and after testing. Tests have been performed where two flat discs were rotated against each other under closed contact in an environment of oil and water. The main wear mechanisms of the four ceramics are identified and discussed. What clearly emerges from these studies is the much more reliable performance of the silicon carbides than the aluminas. The silicon carbides have a low wear rate where microfracture and oxidation are the main deteriorating mechanisms. The capability to maintain smooth surfaces and thus also a high degree of hydrodynamic lubrication is largely due to the potential of the water to dissolve formed wear debris. The main wear mechanism of the aluminas is surface fracture. The rough fracture surfaces and the fact that the wear fragments form a discontinuous surface film will reduce the effect of the lubrication, thus accelerating the wear. Furthermore, a deformation layer with microcracks develops in the contact which decreases wear resistance.     

平底直动从动件凸轮机构磨损失效分析及磨损量计算

凸轮轴和挺杆体是发动机的重要零件,它们的状况直接影响着发动机能否正常工作.文中研究了平底直动从动件凸轮机构运动模型和受力情况,并对其磨损失效成因、磨损形式、磨损规律进行了分析;剖析了相对滑动、润滑条件和接触应力对其工作环境的影响机理,建立了磨损计算模型;并提出从凸轮挺杆材料选配、润滑油、运动参数方面降低凸轮机构磨损的相应措施;提高了凸轮机构的工作可靠性,延长了工作寿命.     

结构陶瓷材料显微结构对摩擦磨损特性影响的研究

结构陶瓷具有高强度、耐高温和耐磨蚀等优点,作为摩擦学部件已得到广泛的应用。从陶瓷材料的显微结构讨论了陶瓷材料的摩擦磨损行为及机制,以促进正确设计和使用陶瓷材料作为摩擦学部件。     

玻璃陶瓷材料与轴承钢表面摩擦磨损的试验研究

在盘销式摩擦磨损试验机上考察了氟金云母玻璃陶瓷与轴承钢的摩擦磨损性能,在不同载荷条件下,测试了摩擦因数和玻璃陶瓷的磨损率,用金相显微镜观察和分析磨损表面形貌,并探讨了玻璃陶瓷材料的磨损机制。结果表明：在低载荷条件下,摩擦因数较低;随着载荷的增加,摩擦副的摩擦因数比较稳定,氟金云母玻璃陶瓷与轴承钢的平均摩擦因数为0.095。玻璃陶瓷和轴承钢的磨损率存在波动,其对磨过程以磨料磨损为主。     

Effect of Sand Concentration in the Medium and Travel Distance and Speed on the Slurry Wear Response of a Zinc-Based Alloy Alumina Particle Composite

Slurry wear characteristics of a zinc-based alloy composite containing 10 wt.% alumina particles have been analyzed by sample rotation technique in this study. The slurry comprised 0.4 g sodium chloride and 0.5 cm³ concentrated sulphuric acid dissolved in one litre of water plus varying concentration (up to 60 wt.%) of sand particles. The traversal distance was varied in the range of 15–500 km while test speeds were maintained at 4.71 and 7.02 m/s. It was observed that the wear response of the composite was influenced by parameters such as traversal speed and distance and the content of the sand particles in the environment. Wear rate reduced with increasing speed when tests were conducted in the liquid-only medium while the trend tended to reverse in the presence of the suspended sand particles in the medium. Further, the wear rate increased initially with distance, attained a peak and decreased thereafter at longer traversal distances. Testing the samples in the environment without sand led to higher wear rate when compared with the ones in the media containing sand. Further, within the liquid plus sand media, intermediate sand content (in the test environment) caused maximum wear rate. In this case, the maximum sand content exhibited minimum wear rate. The wear behaviour of the composite under varying conditions has further been substantiated through the characteristic features of the affected surfaces and subsurface regions. Operating wear mechanisms have been observed to be corrosion assisted erosion and abrasion. The predominance of one mechanism over the other(s) actually controlled the wear response of the composite in specific conditions of wear.     

Study on the thermal wear of diamond segmented tools in circular sawing of granites

An investigation is reported of an analysis on the thermally induced sawblade wear in circular sawing of granites with diamond segmented tools. The temperatures at the diamond–workpiece interface were measured in dry sawing using a foil thermocouple in order to examine the contribution of temperatures to the wear of the segments. Scanning electron microscope and energy dispersive spectrometers were employed to analyze the mechanisms for the bonding of Ti/Cr-coated diamonds to an iron-based matrix. Over 90% of the consumed energy was found to conduct into the diamond segments as heat in the sawing. Strong metallurgical bonding was observed at the diamond–matrix interface and subsequently the retention ability of the matrix to diamonds was increased. However, the retention effect of the coating was greatly offset by the disparity of diamond crystal strength, which could be improved by multistage shape selecting and magnetic separating. Coupled with the mechanisms for thermal wear, attempts were made to reduce thermally induced wear by using Ti/Cr-coated diamonds, reducing the disparity of diamond crystal strength, designing unique structured segments and selecting optimal machining parameters.     

氟金云母陶瓷钻削刀具磨损特性的研究

分别采用硬质合金和高速钢钻头对氟金云母可加工陶瓷进行钻削加工,测试主后刀面的磨损宽度,考察刀具磨损特性,通过单因素试验法考察刀具材料、冷却条件、刀具角度等参数对刀具磨损的影响。试验结果表明:刀具材料和冷却方式是影响刀具磨损的主要因素,高速钢刀具不适于氟金云母陶瓷的钻削加工,冷却条件对硬质合金刀具磨损的影响较为显著,刀具磨损率随钻头顶角增大时对刀具磨损率的影响较小。因此优化刀具材料和工艺参数对氟金云母陶瓷的钻削加工工程应用具有现实价值。     

基于不同冲击频率条件下的套管磨损表面分形特征及磨损机制研究

选取TP140套管在自行研制的套管磨损试验机上进行磨损试验,利用表面形貌仪测量在不同冲击频率条件下的套管表面磨损形貌,选用结构函数法考察磨损形貌的分形特征,使用拟合误差法确定分形曲线的无标度区间并计算分形维数,利用扫描电子显微镜分析其磨损机制。结果表明:在不同冲击频率条件下的套管表面形貌存在明显的分形特征,但分形维数会随频率的不同而有所变化。从光学图像和扫描电镜图像可以看出磨损机制主要有粘着磨损和犁沟。     

Intelligent identification of wear mechanism via on-line ferrograph images

Condition based maintenance（CBM） issues a new challenge of real-time monitoring for machine health maintenance. Wear state monitoring becomes the bottle-neck of CBM due to the lack of on-line information acquiring means. The wear mechanism judgment with characteristic wear debris has been widely adopted in off-line wear analysis; however, on-line wear mechanism characterization remains a big problem. In this paper, the wear mechanism identification via on-line ferrograph images is studied. To obtain isolated wear debris in an on-line ferrograph image, the deposition mechanism of wear debris in on-line ferrograph sensor is studied. The study result shows wear debris chain is the main morphology due to local magnetic field around the deposited wear debris. Accordingly, an improved sampling route for on-line wear debris deposition is designed with focus on the self-adjustment deposition time. As a result, isolated wear debris can be obtained in an on-line image, which facilitates the feature extraction of characteristic wear debris. By referring to the knowledge of analytical ferrograph, four dimensionless morphological features, including equivalent dimension, length-width ratio, shape factor, and contour fractal dimension of characteristic wear debris are extracted for distinguishing four typical wear mechanisms including normal, cutting, fatigue, and severe sliding wear. Furthermore, a feed-forward neural network is adopted to construct an automatic wear mechanism identification model. By training with the samples from analytical ferrograph, the model might identify some typical characteristic wear debris in an on-line ferrograph image. This paper performs a meaningful exploratory for on-line wear mechanism analysis, and the obtained results will provide a feasible way for on-line wear state monitoring.     

ZrO2陶瓷与304钢配副高水基液压元件摩擦学性能

采用Rtec摩擦磨损试验机MFT-5000、白光三维干涉仪和扫描电镜,考察不同载荷和高水基乳化液浓度条件下ZrO2陶瓷与304钢配副的摩擦系数、磨损体积和表面形貌1并探讨其磨损机制.通过控制变量法分析表明:载荷比高水基乳化液浓度对摩擦系数的影响较大,且随着载荷的增大,摩擦系数趋于稳定,而磨损体积增大;随着浓度的增大,摩...     

Tribological Characteristics and Tribochemical Reactions of Various Ceramics Lubricated with HFC-134a Gas

The role of tribochemical products in the friction and wear reduction of ceramics with different fractional ionic character in CF₃CH₂F (HFC-134a) gas was investigated using a ball-on-disk type tribometer. Without exposure to air, the wear tracks on the disks were characterized with the aid of a micro-spot X-ray Photoelectron Spectroscope (XPS) whose analytical chamber was connected to the friction chamber of the tribometer. Further, the adsorption and desorption behaviors of HFC-134a molecules on the nascent surfaces of the ceramics were studied using an adsorption test apparatus in high vacuum. It was found that the lubricating effect of HFC-134a gas was closely related to the fractional ionic or covalent characters of the ceramics. HFC-134a gas was more effective in lubricating ionic ceramics than the covalent ceramics. XPS analysis revealed that metal fluorides were mainly formed on the frictional surfaces of the ionic ceramics, whereas the composition of the tribochemical products on the frictional surfaces of the other ceramics was complicated. The adsorption tests proved that HFC-134a was decomposed to an olefin CF₂=CHF on the nascent surfaces of the ionic ceramic Al₂O₃ and the covalent ceramics. However, the formation of organic fluorine-containing compounds was not detected on the frictional surfaces of the ionic ceramics by XPS. This result implies that the mechanism of tribochemical reactions is strongly dependent on the bond type of ceramics. It is concluded that the low friction and wear of the ionic ceramics in HFC-134a gas result from the metal fluorides formed with high surface concentration on the sliding surfaces.     

Characterization of wear scar surfaces using combined three-dimensional topographic analysis and contact resistance measurements

In this paper, a technique for the quantitative characterization of wear scar surfaces, using combined three-dimensional topographical analysis and contact resistance measurements, is introduced. Parameters for the characterization of wear surfaces, developed during sliding of pin-on-disk specimens in oxygen at high temperature, such as wear volume, roughness, average wear depth on the disk specimen, surface coverage by wear-protective oxide layers and their distributions over the wear surface, are presented and calculated. Such analyses provide more effective data for the analysis of wear processes and wear mechanisms.This method has been applied to the analysis of dry reciprocating sliding wear of a nickel-base alloy, N80A, at temperatures to 600°C. It was found that there was usually a difference between the wear rates of the pin and the disk. This difference increased with increase in temperature, the wear of the pin being much less than that of the disk at the higher temperatures. Although the total wear of both the pin and the disk decreased considerably with increase in temperature, the damage to the disk, judged by the wear depth of the scar, was much higher at elevated temperatures than at low temperatures. The roughnesses of the wear surfaces generally increased with increase in temperature. Less than 50% coverage of the scar surfaces by wear-protective oxide layers was sufficient for the severe-to-mild wear transition. However, the distribution of the wear-protective layers over the wear surfaces was non-uniform. Most of them were concentrated near the centre of the scar, along the sliding direction, under the present conditions. These features of the wear scar surfaces were mainly related to the adhesion and compaction of wear debris particles onto the wear surfaces, leading to development of the wear-protective layers at the various temperatures.     

硬质合金刀具车削氧化铝陶瓷生坯的磨损机理研究

陶瓷生坯是未经烧结的陶瓷压坯,粉体颗粒间未形成冶金结合力,没有陶瓷的硬、脆等特性,因此可以利用这一优点用车削方式加工陶瓷生坯。用冷等静压技术制备Al2O3陶瓷生坯柱体进行车削试验,探究陶瓷生坯切削加工质量和刀具磨损机理。试验表明刀具主要受到磨粒磨损且适当改变切削参数能明显改善加工表面质量和刀具寿命;并且在试验参数范围内,随着背吃刀量的增加,刀具寿命随之增加;进给量对刀具寿命影响不明显。     

Ceramic wear maps

Ceramic wear maps have been developed to elucidate the complex interactions of the operating parameters, environments, and wear mechanisms. This paper summarizes these interactions for four ceramics, alumina, yttria-doped zirconia, silicon carbide and silicon nitride. Wear maps of these ceramics are systematically constructed using measured data under dry sliding, water, and paraffin lubricated conditions. For each material, different wear level regions acid wear transition zones are identified as a function of operating conditions and lubrication conditions. Wear mechanism studies performed within each wear region give rise to the wear mechanism maps. These maps facilitate material comparison and selection. The knowledge of wear, wear transitions, and wear mechanisms for a material pair enables realistic wear model development. One outcome of this approach is the recognition that a single wear model for a material pair cannot cover all operating conditions and environments.

As wear maps are constructed today, they are material pair specific. Within a material pair, there are microstructural dependence and surface properties influence. These parameters can change substantially for a given chemical composition of the material. How to incorporate these factors into the wear map research remains an issue. The search for a universal parameter such as the “asperity temperature” in Ashby's wear map continues in spite of mounting evidence that this may not be practical or feasible. But the hope remains that some parameters can be identified to normalize a large number of materials, operating conditions, and environments for tribological applications. Systematic wear maps are the first steps in this direction.     

不同润滑条件下氧化铝陶瓷衬板的磨损机制

在干摩擦、水润滑、油润滑3种不同润滑条件下对氧化铝陶瓷进行摩擦磨损试验。利用SEM对磨损后的磨痕进行观察并进行显微组织结构分析,探讨不同介质下氧化铝陶瓷的磨损机制。结果表明:氧化铝陶瓷材料干摩擦条件下的磨损机制为大量的脆性剥落和大量的磨粒磨损,在水润滑条件下为较少的脆性剥落和轻微的磨粒磨损,在油润滑条件下为很少的脆性剥落和极微的磨粒磨损;液体润滑剂可使氧化铝陶瓷材料的磨损量大幅度降低,其中油润滑条件的减磨效果最为突出。