共查询到20条相似文献,搜索用时 78 毫秒
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本文研究了用无定形氮化硅超细粉原位生长α-Si3N4晶须,晶须生长温度为1400~1450℃,恒温1~4h.讨论了在晶须生长过程中,不同的保护气氛对晶须质量的影响.当晶须在高纯N2气氛中生长时,得到的晶须中氮含量为32%~34%,氧含量为8%~6%,氯含量为0.1%左右.这类晶须中存在着大量的缺陷.当晶须在NH3气氛中生长时,得到的晶须中氮含量为39%左右,氧含量为1%,氯含量为0.01%,在这类晶须的透射电镜照片中几乎看不到缺陷. 相似文献
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Cl对Si3N4粉中α/β相含量的影响 总被引:3,自引:0,他引:3
本文研究了用SiCl4氨解法制备Si3N4粉时,要得到高α相的Si3N4粉的关键,在于必须使系统中杂质氯含量足够低,研究结果表明,在高纯N2气气氛中制粉,由于系统中氯含量较高,促使粉料中β相含量增高,α相含量降低。而在NH3气气氛中制粉,由于不断流动的NH3气,在高温下能携带出残留在粉料中的杂质NH4Cl,从而使粉料中的氯含量〈0.01%,这时制得的粉料,其α相的含量均在97%以上。 相似文献
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莫来石晶须制备新工艺与生长机理 总被引:8,自引:0,他引:8
本文首次提出了用Al2O3-SiO2玻璃粉高温热处理制取莫来石晶须的新工艺.采用XRD、SEM和TEM等手段研究了热处理温度制度及气氛对莫来石晶须生长的影响,确定了制备莫来石晶须的最佳工艺参数,所得莫来石晶须的直径为0.4~1.2Pm、长径比为10~40,其生长方向为c轴方向,生成物中莫来石晶须的含量接近98vol%.探讨了用Al2O3-SiO2玻璃粉制取莫来石晶须的生长机理. 相似文献
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碳化硅陶瓷及其复合材料的热等静压烧结研究 总被引:2,自引:0,他引:2
本文通过采用热等静压(HIP)这一先进的烧结工艺,研究了Al2O3添加量对SiC陶瓷之显微结构与力学性能的影响。并成功地制备出Si3N4粒子以及SiC晶须补强的SiC基复合材料,结果表明:Al2O3是HIP烧结SiC陶瓷及其复合材料的有效添加剂,当添加3wt%Al2O3时,采用HIP烧结工艺在1850℃温度和200MPa压力下烧结1h就可获得密度分别高达97.3%、99.4%和97.0%的SiC的 相似文献
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应用差热分析、X射线粉末衍射及电测量技术对Na2Mo(0.1)S(0.9)O4(α)-Pr2(SO4)3体系进行了研究,结果表明,在Na2Mo(0.1)S(0.9)O4相中加入少量的Pr2(SO4)3就可以形成完全固熔体,且无任何相变存在,当Pr2(SO4)3含量达到4mol%时,电导率较纯Na2Mo(0.1)S(0.9)O4提高两个数量级(553K时,σ=1.09×10(-3)Scm(-1)),同时还证明了该类导体的导电机理,揭示了电导率与有效空位浓度、掺杂剂浓度及温度之间的依赖关系。 相似文献
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《International journal for numerical methods in engineering》2018,113(9):1488-1506
In this paper, we present a new method for inserting several triangulated surfaces into an existing tetrahedral mesh generated by the meccano method. The result is a conformal mesh where each inserted surface is approximated by a set of faces of the final tetrahedral mesh. First, the tetrahedral mesh is refined around the inserted surfaces to capture their geometric features. Second, each immersed surface is approximated by a set of faces from the tetrahedral mesh. Third, following a novel approach, the nodes of the approximated surfaces are mapped to the corresponding immersed surface. Fourth, we untangle and smooth the mesh by optimizing a regularized shape distortion measure for tetrahedral elements in which we move all the nodes of the mesh, restricting the movement of the edge and surface nodes along the corresponding entity they belong to. The refining process allows approximating the immersed surface for any initial meccano tetrahedral mesh. Moreover, the proposed projection method avoids computational expensive geometric projections. Finally, the applied simultaneous untangling and smoothing process delivers a high‐quality mesh and ensures that the immersed surfaces are interpolated. Several examples are presented to assess the properties of the proposed method. 相似文献
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Standards are the basis for production enterprises to organize production ex-factory inspection trade 《中国标准化(英文版)》2008,25(1):24-25
Standards are the basis for production enterprises to organize production, ex-factory inspection, trade (delivery) and technical exchanges, product certification, quality arbitration and supervision.…… 相似文献
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A flow calorimeter for enthalpy increment measurements on condensed gases is presented. A better knowledge of the properties of the liquefied natural gas is needed, and therefore a liquid loop has been designed for our flow calorimeter. The fluid loop in the calorimeter is designed in order to avoid the two-phase region, since two phases would give compositional disturbances in the measurements. The avoidance of the two-phase region is made possible by increasing the pressure of the test fluid after the measurement section, then heating the fluid at super-critical pressure past the critical point. Finally, the fluid is throttled to the low-pressure gas state at the inlet condition of the compressor that circulates the fluid. To perform the pressure increase, a new cryogenic pump has been designed. To evaluate the new equipment, measurements were taken on liquid ethane over the temperature range 146–256 K at pressure between 0.9 and 5.1 MPa. 相似文献
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On November 30, 2007, the China Association for Standardization (CAS) held a press conference at Beijing Diaoyutai State Guest House. Leaders from the China Household Electric Appliance Research Institute, the China Household Electric Appliance Association, and the China Consumers' Association attended and made speeches.…… 相似文献
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Zusammenfassung Bei der Gestaltung von Ernteprozessen — beispielsweise des Prozesses Mähdrusch, Körnertransport und -abnahme — als transportverbundene Fließarbeitsverfahren mit mindestens zwei verschiedenen Arbeitsmitteln gibt es einen großen Optimierungsspielraum. Solche Prozesse sind mehrstufige Bedienungsprozesse mit gemischter Anordnung der Bedienungseinrichtungen. Außerdem besitzen sie stark ausgeprägte räumliche Aspekte. Es wird vor allem gezeigt, welche Merkmale solcher Prozesse in Simulationsmodellen abgebildet sein müssen, welche Zielgrößen in Abhängigkeit von welchen Einflußgrößen unter Berücksichtigung welcher Prozeßbedingungen ermittelt werden sollten und wie der Bewertungsprozeß zur Ermittlung der gewünschten Informationen gestaltet werden muß. 相似文献
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C. Qihong W. Zhan‐Wen J. Yi J. Yehua L. Fei F. Hanguang 《Materialwissenschaft und Werkstofftechnik》2014,45(7):582-590
In the present study a high‐boron high speed steel (HSS) roll material was designed. Many expensive alloy elements have been substituted by cheap boron alloy, and high‐boron high speed steel roll has been manufactured by centrifugal casting method. The microstructures, mechanical properties and wear resistance of centrifugal casting high‐boron high speed steel roll have been investigated by optical microscopy (OM), scanning electron microscopy (SEM), and X‐ray diffraction (XRD) analysis, hardness test, impact test and wear test. The results indicated that the solidification microstructures of high‐boron high speed steel roll consisted of M2(B,C), (W,Mo)2(B,C), M3(B,C), M23(B,C)6 type borocarbides and martensite, a small amount of retained austenite. Borocarbides were continuously distributed over the grain boundary. After quenching from 1050 °C, local broken network appeared in partial borocarbides, and fine secondary borocarbide precipitated from the matrix. After tempering from 525 °C, the amount of precipitated borocarbide increased significantly. After heat treatment, the hardness of high‐boron high speed steel roll excelled 60 HRC, and its impact toughness excelled 8.0 J/cm2. The single groove steel rolling amount of high‐boron high speed steel rolls increases by 500% than that of bainite cast iron roll, when the rolls are used in K1 mill housing of bar mill. 相似文献
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Dimiter Hadjistamov 《材料科学与工程:中英文B版...》2019,(2):56-65
The definition of the thixotropy is a decrease in viscosity with time in shear and a subsequent recovery of viscosity after the shear deformation is removed.We ... 相似文献
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《中国标准化(英文版)》2014,(4)
正Responding to ISO’s appeal for survey for the to-be-developed ISO Strategy Plan for 2016-2020,SAC hosted a special workshop over the needs and comments of various fi elds on June 8 in Beijing.The workshop was attended by ISO President-elect and Ansteel General Manager Zhang Xiaogang,SAC Vice-Administrator Yu Xinli,and 30 experts from 相似文献
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《中国标准化(英文版)》2014,(5)
正The review group of Asia Pacific Laboratory Accreditation Cooperation(APLAC)carried out a 4-day peer review of the proficiency testing provider(PTP)for China National Accreditation Service for Conformity Assessment(CNAS)from July 28 to 31,2014.CNAS passed the PTP review with excellent performance.Two senior peer reviewers of APLAC made a comprehensive,rigorous and detailed review of CNAS’s PTP accreditation activities,and made the on-spot inspection of the review groups in Shanghai and Shenzhen respectively. 相似文献