合金成分对定向凝固柱晶高温合金热裂倾向性的影响

为研究定向凝固柱晶高温合金薄壁铸件凝固过程的热裂纹形成倾向,采用定向凝固空心薄壁管状试样,考察了Ti,Zr,Hf,Al和B等元素对定向凝固柱晶高温合金热裂倾向性的影响;采用SEM、断口分析及DSC方法,分析了热裂的晶界宏观形态.结果表明:随着Ti含量的增加,γ/γ′共晶增多,尺寸增大,合金凝固温度范围变大,定向合金的热裂倾向性严重;Zr元素含量增加,促成共晶形成,合金出现热裂纹;Hf含量的变化对合金的热裂没有影响;Al,B含量增加,微观组织无明显变化,但合金凝固温度范围变大,导致定向凝固合金出现热裂.     

浇注温度对定向凝固Al－Cu合金热裂的影响

针对空心叶片类定向凝固铸件存在的热裂问题，开展了定向凝固热裂规律的研究。本文选择凝固参数较全的Ａｌ－Ｃｕ系合金，研究了定向凝固工艺参数之一的浇注温度对Ａｌ－０．６ｗｔ％Ｃｕ和Ａｌ－２．０ｗｔ％Ｃｕ合金热裂的影响。定向凝固热裂试验表明，提高浇注温度可以降低Ａｌ－０．６ｗｔ％Ｃｕ合金的热裂程度，但对Ａｌ－２．０ｗｔ％Ｃｕ则无作用。理论分析认为，合金在不可补缩区的冷却速率变化是改变合金热裂程度的重要因素。     

抽拉速率对铝合金定向凝固热裂形成的影响

在半连续真空定向凝固设备上进行了Ａｌ－０．６ｗｔ％Ｃｕ和Ａｌ－２．０ｗｔ％Ｃｕ两种铝合金的热裂试验，结果表明，两种成分铝合金试样的热裂程度随抽拉速率的提高而增大，理论分析认为，抽拉速率的提高，增加了合金凝固后期的收缩速率，因而造成热裂程度的增加。     

浇注温度对定向凝固Al－Cu合金热裂的影响EI

针对空心叶片类定向凝固铸件存在的热裂问题，开展了定向凝固热裂规律的研究。本文选择凝固参数较全的Ａｌ－Ｃｕ系合金，研究了定向凝固工艺参数之一的浇注温度对Ａｌ－０．６ｗｔ％Ｃｕ和Ａｌ－２．０ｗｔ％Ｃｕ合金热裂的影响。定向凝固热裂试验表明，提高浇注温度可以降低Ａｌ－０．６ｗｔ％Ｃｕ合金的热裂程度，但对Ａｌ－２．０ｗｔ％Ｃｕ则无作用。理论分析认为，合金在不可补缩区的冷却速率变化是改变合金热裂程度的重要因素。     

高强管线钢冷裂敏感性的斜Y坡口实验研究

采用七种高纤维素型立向下电焊条,通过斜Y坡口裂纹实验,对高强管线钢的冷裂敏感性进行实验研究.通过理论公式计算了其冷裂敏感系数,并根据实验结果确定了避免冷裂产生的最低预热温度,为高强管线钢施工及制定焊接工艺提供了实验和理论依据,也为高强管线钢的冷裂敏感性的标准实验方法提供参考.     

水玻璃石英砂和呋喃树脂石英砂对铸钢件热裂的影响

热裂是铸钢件生产中最严重的缺陷之一,防止和控制热裂是铸造工作者的共同目标。本文探讨了型砂对铸钢件热裂的作用,指出呋喃树脂石英砂和水玻璃石英砂对热裂的不同影响。     

微量锆对DZ3高温合金凝固行为的影响

DZ3合金除去0. 1％Zr显著地减低热裂倾向。这与Zr对合金凝固行为的影响有关。 0. 1％Zr明显地促进γ+γ′共晶的形成,zr偏析形成低熔点的Ni_5Zr相。在凝固过程中富Zr的液膜保持到低于1180℃的温度,结果使合金的凝固范围扩大了80℃。使失去枝晶间补缩的温度与固相线的温度范围扩大了60℃。这是含Zr含金热裂倾向大的原因之一。     

挤压工艺对Mg-0.6Zr-0.5Y合金力学和阻尼性能的影响

系统地研究了挤压温度和挤压比对Mg-0.6Zr-0.5Y合金力学和阻尼性能的影响规律.采用光学金相显微镜、电子式万能试验机及动态机械分析仪(DMA)等手段分析合金显微组织、力学和阻尼性能的变化,并讨论了晶粒细化与合金力学和阻尼机理之间的内在联系.研究发现,合金在挤压过程中发生了动态再结晶,晶粒显著细化,使综合力学性能得...     

In含量对SnBi36Ag0.5无铅焊料合金性能的影响

为了研究In的添加对合金显微组织、熔化特性、润湿性和力学性能的影响.按质量比将纯锡、铋锭、银锭和铟锭在400℃熔化,保温6h,搅拌均匀后在320℃浇铸,制备成SnBi36Ag0.5Inx(x=0％、0.1％、0.2％、0.3％、0.4％、0.5％)焊料合金.利用X射线衍射仪、光学金相显微镜(OM)、扫描电镜能谱(SEM...     

镍基单晶合金CMSX-6的再结晶行为及热裂倾向

在不同热处理温度和载荷下,研究了CMSX-6单晶的再结晶现象。结果表明:在低于1 150℃×4 h热处理后,没发现再结晶现象,但在载荷的作用下,单晶退火时γ'相形成元素自发偏析,造成大量的大颗粒γ'相在共晶周围析出;随着热处理温度升高,载荷影响区再结晶经历由压痕周围胞状再结晶、枝晶干再结晶、多个等轴再结晶三个阶段;在高于1 150℃×4 h热处理时,单晶随着载荷的增加,再结晶的范围和深度明显增大;以及随冷却速率的增加,再结晶晶粒之间的热裂倾向增大,致使大量热裂沿晶界分布。     

A modified hot tearing criterion for direct chill casting of aluminium alloys

Using the good criteria to predict hot tearing is very important during DC casting of aluminium alloys. Among all the hot tearing criteria, a fracture-mechanics based SKK criterion proposed by Suyitno et al. has made considerable improvements in the hot tearing prediction. However, its obtained hot tearing susceptibility (HTS) evolution during solidification is also not completely consistent with real industrial production circumstances, especially when approaching the solidus temperature. In this paper, some further modifications are made based on the SKK criterion to emphasise the important effect of solid bridging/grain coalescence on hot tear propagation. It is proved that the HTS evolution in freezing range predicted by the modified hot tearing criterion is in good agreement with casting practice.     

An investigation on solidification path and hot tearing tendency of Mg−2Zn−3Y−xAl alloys

Based on the improved Clyne‐Davies’ model (CSC_T), the hot tearing tendency of Mg?2Zn?3Y?xAl (x = 0, 0.5, 1, 2, wt.%) alloys were predicted. The concretion path, the solidification characteristic temperature, the dendrite coherent solid fraction were studied by the double thermocouples thermal analysis. The curve of solidification contraction stress with temperature (or time) was measured with a “T” type hot tearing permanent‐mold. The experimental results show that the modified Clyne‐Davies’ model prediction values are in good agreement with the experimental results. Al₂Y phase can be used as the heterogeneous nucleation core of α‐Mg matrix and refine the α‐Mg grain size. It is found that Al₂Y increases, grain refinement is more obvious, dendrite coherence is postponed, and the hot tearing susceptibility of the alloy decreases significantly with increasing aluminum content.     

Determination of hot crack susceptibility in various kinds of steels

The aim of this investigation was to study the hot crack susceptibility of some Turkish and German structural steel plates with a modified varestraint-transvarestraint test method. Testing was accomplished using a Tungsten Inert Gas (TIG) welding process. The results of this study revealed that total crack length increases as welding current increases or punch radius or welding speed decreases. An attempt is made to provide explanations for these phenomena.     

Effect of minor content of Gd on the mechanical and degradable properties of as-cast Mg-2Zn-xGd-0.5Zr alloys

RE-containing Mg alloys used as biodegradable medical implants exhibit good promising application due to their good mechanical properties and degradation resistance. In this work, effect of Gd on the microstructure, mechanical properties and biodegradation of as-cast Mg-2Zn-xGd-0.5Zr alloys was investigated. The results showed that there were mainly α-Mg, I-phase, W-phase and MgZn2 phase in Mg-Zn-Gd-Zr alloys. With increase of the Gd content, the strength of the alloys was enhanced due to the second phase strengthening and grain refinement. The degradation resistance of Mg-2Zn-0.5Zr alloy was increased by adding 0.5%–1% Gd due to the uniformly distributed second phases which acted as a barrier to prevent the pitting corrosion. However, increasing Gd content to 2% reduced the degradation resistance of the alloy due to the galvanic corrosion between the matrix and the second phases.The good degradation resistance and mechanical properties of as-cast Mg-2Zn-1Gd-0.5Zr alloy makes it outstanding for biomaterial application.     

The effect of 0.5 wt.% Ce additions on the electromigration of Sn9Zn BGA solder packages with Au/Ni(P)/Cu and Ag/Cu pads

It has previously been established that Sn-9Zn-0.5Ce alloy possesses mechanical properties superior to those of undoped Sn-9Zn alloy, and is free of the problem of rapid whisker growth. However, no detailed studies have been conducted on the electromigration behavior of Sn-9Zn-0.5Ce alloy. In this research, Sn-9Zn and Sn-9Zn-0.5Ce solder joints with Au/Ni(P)/Cu and Ag/Cu pads were stressed under a current density of 3.1 × 10⁴ A/cm² at room temperature for various periods of time. Due to finer grain sizes, the electromigration effects were more severe in Sn-9Zn-0.5Ce solder joints than in Sn-9Zn solder joints when joint temperature was around 80 °C. In addition, both solder joints (Sn-9Zn and Sn-9Zn-0.5Ce) with Au/Ni(P)/Cu pads possess longer current-stressing lifetimes than those with Ag/Cu pads because Ni is more resistant than Cu to migration driven by electron flow.     

热处理对粉末热挤压法制备6061铝合金强度和塑性的影响

研究了单级固溶及峰值时效处理对粉末热挤压法制备6061铝合金显微组织及室温力学性能的影响,观察了合金挤压态、固溶态及时效处理后的显微组织,并对其力学性能进行了测试.结果表明:挤压态材料的晶粒均匀细小,基体合金中存在大量的第二相颗粒,主要为Mg2Si相;热挤压后的6061铝合金经固溶时效处理(530℃×1 h水冷+170℃×6 h)后,晶粒内部析出大量的β″(Mg5Si6)相,并伴有少量棒状的β’(Mg2Si)相析出,拉伸强度和延伸率分别为311 MPa和10%,相比挤压态铝合金,其拉伸强度提高了近160%.     

两种型壳温度对DD9单晶涡轮叶片凝固组织的影响EI北大核心CSCD

为了研究1500℃和1540℃两种型壳温度对第三代单晶高温合金DD9叶片截面凝固组织的影响,采用光学显微镜、扫描电子显微镜对叶片典型截面凝固组织进行分析。结果表明:随着型壳温度的增加,DD9单晶涡轮叶片凝固组织的枝晶花样呈细小趋势,二次枝晶呈发达趋势。相同型壳温度下,叶片叶身部位的枝晶比榫头部位的枝晶更细小。随着型壳温度的增加,枝晶干和枝晶间的γ′析出相尺寸和分散度均减小,并且γ′析出相尺寸分布遵循正态分布规律。相较枝晶间区域,枝晶干区域的γ′析出相的平均尺寸减小了61%。相同型壳温度下,叶片叶身部位的γ′析出相尺寸比榫头部位的γ′析出相尺寸更细小。与截面积变小相比,提高型壳温度会使γ′析出相变小更显著。随着型壳温度的增加,γ-γ′共晶尺寸和含量减小,γ-γ′共晶组织呈葵花状和光板状两种形貌特征。     

溅射工艺参数对Ba0.5Sr0.5TiO3薄膜沉积速率和介电性能的影响

铁电/介电BST(BaxSr1-xTiO3)薄膜在微电子学、集成光学和光电子学等新技术领域有广泛的应用前景.用射频磁控溅射方法制备了厚约700 nm的Ba0.5Sr0.5TiO3薄膜,采用Al/BST/ITO结构研究了溅射功率、溅射气压、O2/(Ar O2)比和基片温度对上述BST薄膜沉积速率和介电性能的影响,并根据这些结果分析了较优的工艺条件,同时用XRD、XPS和SEM研究了薄膜的晶相、组成和显微结构.     

锰掺杂对(Na0.5Bi0.5)0.92Ba0.08TiO3压电陶瓷性能的影响

研究了 Mn掺杂对 (Na0.5Bi0.5)0.92Ba0.08TiO3系陶瓷介电、压电与铁电性能的影响. X- ray衍 射结构分析表明掺杂适量的 Mn得到单一的钙钛矿结构,无第二相出现.当添加 0.3 wt % MnCO3 时,介电常数达到 1850;矫顽场强 Ec降低至 3.54kV/mm;压电常数 d33达到 160× 10- 12 C/N.该 材料的温度稳定性也得到改善.