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1.
Subcritical crack growth and rapid fracture of the mechanically alloyed aluminum alloy IN-9052* reinforced with SiC particles have been investigated. Fatigue crack growth rates for the composite exceed those of the unreinforced alloy, except that the threshold stress intensity for growth is higher for the composite. Fracture toughness of the composite is about 9 MPa√m compared to a (reported) value of 29 MPa√m for the unreinforced alloy. The contributions to fracture toughness from work done within the plastic zone and in formation of the void sheet have been computed using analytical models. Fracture toughness is shown to result almost entirely from work done within the plastic zone of the growing crack. The matrix microstructure and the particulate characteristics are found to account for the elastic and fracture properties of this composite.  相似文献   

2.
The effects of alkali-metal impurity (AMI) content, temperature, and crack-mouth-opening displacement (CMOD) rate on the fracture toughness of 2090-T8 Al-Li-Cu alloy extrusions were studied, particularly for short-transverse (S-L) orientations. Decreasing AMI content resulted in increasing room-temperature fracture toughness, especially for underaged S-L and T-L specimens. Unlike most Al-Li based alloys, material with very low (<2 wt. ppm) AMIs produced by vacuum refining had a high S-L fracture toughness (up to 38 MPa√m for proof strengths ∼440 MPa) as well as high toughness in other orientations. The increase in room-temperature fracture toughness with decreasing AMI content was associated with a decrease in the proportion of brittle intergranular and cleavagelike islands, and a corresponding increase in the proportion of high energy dimpled fracture modes, on fracture surfaces. Both the present and previous studies indicate that the brittle islands result from liquid-metal embrittlement due to the presence of discrete sodium-potassium rich liquid phases. For medium to high AMI contents (5 to 37 wt ppm), S-L fracture toughness increased with decreasing temperature due to solidification of these phases and a consequent decrease in the mobility of embrittling atoms. The ability of embrittling atoms to keep up with crack tips also depended on crack velocity so that CMOD rate influenced fracture toughness. The grain structure (degree of recrystallization) appeared to be another important parameter affecting fracture toughness.  相似文献   

3.
The high-temperature strength and creep resistance of low carbon arc cast (LCAC) unalloyed molybdenum, oxide dispersion strengthened (ODS) molybdenum, and molybdenum-0.5 pct titanium-0.1 pct zirconium (TZM) molybdenum have attracted interest in these alloys for various high-temperature structural applications. Fracture toughness testing of wrought plate stock over a temperature range of −150 °C to 1000 °C using bend, flexure, and compact tension (CT) specimens has shown that consistent fracture toughness results and transition temperatures are obtained using subsized 0.5T bend and 0.18T disc-CT specimens. Although the fracture toughness values are not strictly valid in accordance with all ASTM requirements, these values are considered to be a reasonable measure of fracture toughness. Ductile-to-brittle transition temperature (DBTT) values were determined in the transverse and longitudinal orientations for LCAC (200 °C and 150 °C, respectively), ODS (<room temperature and −150 °C), and TZM (150 °C and 100 °C). At test temperatures > DBTT, the fracture toughness values for LCAC ranged from 45 to 175 MPa√m, TZM ranged from 74 to 215 MPa√m, and the values for ODS ranged from 56 to 149 MPa√m. No temperature dependence was resolved within the data scatter for fracture toughness values between the DBTT and 1000 °C. Thin sheet toughening is shown to be the dominant toughening mechanism, where crack initiation/propagation along grain boundaries leaves ligaments of sheetlike grains that are pulled to failure by plastic necking. Specimen-to-specimen variation in the fraction of the microstructure that splits into thin sheets is proposed to be responsible for the large scatter in toughness values at test temperatures > DBTT. A finer grain size is shown to result in a higher fraction of thin sheet ligament features at the fracture surface. As a result finer grain size materials such as ODS molybdenum have a lower DBTT.  相似文献   

4.
The fatigue and fracture resistance of a commercially made, single-phase Nb-base alloy with 35 at. pct Ti, 5 at. pct Cr, 6 at. pct Al, and several elements to increase solid solution strengthening have been investigated. The threshold for fatigue crack growth was determined to be ≈7 MPa√m and fracture toughness ≈35 MPa√m. Crack growth was intermittent and sporadic; the fracture path was tortuous, crystallographic, and appeared to favor the {100} and {112} planes. Fatigue crack closure was measured directly at the crack tip. The fatigue and fracture properties of the commercial alloy are compared against those of Nb-Cr-Ti and Nb-Cr-Ti-Al alloys. The comparison indicated that Ti addition is beneficial for, but Al addition is detrimental to, both fracture toughness and fatigue crack resistance.  相似文献   

5.
The results of a recent study of the effects of ternary alloying with Ti on the fatigue and fracture behavior of a new class of forged damage-tolerant niobium aluminide (Nb3Al-xTi) intermetallics are presented in this article. The alloys studied have the following nominal compositions: Nb-15Al-10Ti (10Ti alloy), Nb-15Al-25Ti (25Ti alloy), and Nb-15Al-40Ti (40Ti alloy). All compositions are quoted in atomic percentages unless stated otherwise. The 10Ti and 25Ti alloys exhibit fracture toughness levels between 10 and 20 MPa√m at room temperature. Fracture in these alloys occurs by brittle cleavage fracture modes. In contrast, a ductile dimpled fracture mode is observed at room-temperature for the alloy containing 40 at. pct Ti. The 40Ti alloy also exhibits exceptional combinations of room-temperature strength (695 to 904 MPa), ductility (4 to 30 pct), fracture toughness (40 to 100 MPa√m), and fatigue crack growth resistance (comparable to Ti-6Al-4V, monolithic Nb, and inconnel 718). The implications of the results are discussed for potential structural applications of the 40Ti alloy in the intermediate-temperature (∼700 °C to 750 °C) regime.  相似文献   

6.
The effect of hydrogen on the fracture toughness behavior of a nickel-base superalloy, Alloy X-750, in the solutionized and aged condition was investigated. Notched bend specimens were tested to determine if the fracture process was stress or strain controlled. The fracture was observed to initiate at a distance between the location of maximum stress and maximum strain, suggesting that fracture required both a critical stress and strain. The effect of hydrogen was further investigated and modeled using fracture toughness testing and fractographic examination. The fracture toughness of the non-charged specimen was 147 MPa√m. Charging with hydrogen decreased the fracture toughness, K Ic , to 52 MPa√m at a rapid loading rate and further decreased the toughness to 42 MPa√m for a slow loading rate. This is consistent with the rate-limiting step for the embrittlement process being hydrogen diffusion. The fracture morphology for the hydrogen-charged specimens was intergranular ductile dimple, while the fracture morphology of noncharged specimens was a mixture of large transgranular dimples and fine intergranular dimples. The intergranular failure mechanism in Alloy X-750 was a microvoid initiation process at grain boundary carbides followed by void growth and coalescence. One role of hydrogen was to reduce the void initiation strain for the fine intergranular carbides. Hydrogen may have also increased the rate of void growth. The conditions ahead of a crack satisfy the critical stress criterion at a much lower applied stress intensity factor than for the critical fracture strain criterion. A model based on a critical fracture strain criterion is shown to predict the fracture behavior.  相似文献   

7.
The temperature dependence of fatigue crack propagation is considered in an Fe-1 pct Cr-0.5 pct Mo alloy steel. This material was tested at temperatures between 425 and 550 °C, a frequency of 1 Hz, and anR-ratio of 0.1. It is shown that the effect of temperature can be explained in terms of a thermal activation energy for fatigue. The magnitude of this activation energy is a function of ΔK and varies from more than 150 kJ/mole at 15 MPa√m to 30 kJ/mole above 30 MPa√m. The magnitude of these activation energies supports the idea that oxidation, and not creep, is the rate-controlling time-dependent process for the test conditions studied.  相似文献   

8.
Microstructural effects on fracture toughness in AA7010 plate   总被引:5,自引:0,他引:5  
The influence of recrystallization and quench rate after solution treatment on the fracture toughness of 7010 aluminum plate has been studied in longitudinal-transverse (L-T) and short-longitudinal (S-L) orientations for T76-type heat treatments. Extensive fractographic analysis was carried out to identify the failure mechanisms, including simultaneous scanning electron microscope (SEM) observation of fracture surfaces and underlying microstructures. A slow quench rate was strongly detrimental because it modified the dominant failure mode from a relatively high energy primary void growth mechanism to lower energy transgranular shear and grain boundary ductile failure in the L-T and S-L orientations, respectively. Low energy failure was associated with coarse ν precipitation during the quench in both L-T and S-L orientation tests, with intragranular and intersubgranular particles contributing to L-T quench sensitivity, and intergranular particles contributing to S-L sensitivity. Partial recrystallization was generally detrimental, with recrystallized grains being shown to be a preferential crack path. The commonly supposed susceptibility of recrystallized grains to intergranular failure did not explain this behavior, particularly in fast quench materials, as recrystallized grains primarily failed by transgranular void growth from the large intermetallics with which they were intrinsically associated. Exceptional S-L orientation quench sensitivity was observed in unrecrystallized material and attributed to a synergistic interaction between heterogeneous boundary precipitation and the specific location of coarse intermetallics along grain boundaries in the unrecrystallized condition. Quantitative assessment of individual contributions to overall fracture resistance is discussed for cases where multiple failure mechanisms occur, highlighting the importance of interacting and noninteracting mechanisms.  相似文献   

9.
Oxide dispersion-strengthened (ODS) and molybdenum-0.5 pct titanium-0.1 pct zirconium (TZM) molybdenum have excellent creep resistance and strength at high temperatures in inert atmospheres. Fracture toughness and tensile testing was performed at temperatures between − 150 °C and 450 °C to characterize 6.35-mm-thick plate material of ODS and TZM molybdenum. A transition from low fracture-toughness values (5.8 to 29.6 MPa√m) to values >30 MPa√m is observed for TZM molybdenum in the longitudinal orientation at 100 °C and in the transverse orientation at 150 °C. These results are consistent with data reported in literature for molybdenum. A transition to low fracture-toughness values (<30 MPa√m) was not observed for longitudinal ODS molybdenum at temperatures >−150 °C, while a transition to low fracture-toughness values (12.6 to 25.4 MPa√m) was observed for the transverse orientation at room temperature. The fine spacing of La-oxide precipitates which are present in ODS molybdenum results in a transition temperature that is significantly lower than any molybdenum alloy reported to date, with upper-bound fracture-toughness values that bound the literature data. A comparison of fracture-toughness values obtained using 1T, 0.5T, and 0.25T three-point bend specimens shows that a 0.5T bend specimen could be used as a subsized geometry.  相似文献   

10.
Niobium-chromium alloys, both single and two phase, were alloyed with titanium in order to enhance fracture toughness and fatigue crack growth resistance. The selection of titanium as an alloying element and the relationship of electronic bonding to toughness are examined. The results indicated that toughness increased with a decreasing number of D +s electrons. Titanium was found to increase the toughness of solid-solution Nb-Cr alloys from ≈8 to 87 MPa√m, while for the twophase “insitu composites,” toughness was increased from ≈5 to 20 MPa√m, although this is less than expected. Fracture toughness of the composites correlated nonlinearly with the volume fraction of the phases. The evidence suggests that the toughness of the composites is decreased due to fracture of the intermetallic particles and constraint on matrix deformation imposed by the intermetallic. Fracture characteristics of the Nb-Cr-Ti materials are compared to those of Nb-Cr and Nb-Si materials.  相似文献   

11.
A study has been made of the mechanics and mechanisms of fatigue crack propagation in a commercial plate of aluminum-lithium alloy 2090-T8E41. In Part I, the crack growth and crack shielding behavior of long (≳5 mm) through-thickness cracks is examined as a function of plate orientation and load ratio, and results compared to traditional high strength aluminum alloys. It is shown that rates of fatigue crack extension in 2090 are, in general, significantly slower (at a given stress intensity range) than in traditional alloys, although behavior is strongly anisotropic. Differences in growth rates of up to 4 orders of magnitude are observed between the L-T, T-L, and T-S orientations, which show the best crack growth resistance, and the S-L, S-T, and L + 45, which show the worst. Such behavior is attributed to the development of significant crack tip shielding (i.e., a reduction in local crack driving force), primarily resulting from the role of the crack path morphology in inducing crack deflection and crack closure from the consequent asperity wedging. Whereas crack advance perpendicular to the rolling plane (e.g., L-T,etc.) involves marked crack path deflection and branching, thereby promoting very high levels of shielding to cause the slowest growth rates, fatigue fractures parallel to the rolling plane (e.g., S-L,etc.) occur by an intergranular, delamination-type separation, with much lower shielding levels to give the fastest growth rates. The implications of such “extrinsic toughening” effects on the fracture and fatigue properties of aluminum-lithium alloys are discussed in detail. R. O. RITCHIE, Professor and Director, Center for Advanced Materials, Lawrence Berkeley Laboratory  相似文献   

12.
The plane-strain initiation fracture toughness (K JICi ) and plane-stress crack growth resistance of two Al-Cu-Mg-Ag alloy sheets are characterized as a function of temperature by a J-integral method. For AA2519 +Mg+Ag, K JICi decreases from 32.5 MPa√m at 25 °C to 28.5 MPa√m at 175 °C, while K JICi for a lower Cu variant increases from 34.2 MPa√m at 25 °C to 36.0 MPa√m at 150 °C. Crack-tip damage in AA2519+Mg+Ag evolves by nucleation and growth of voids from large undissolved Al2Cu particles, but fracture resistance is controlled by void sheeting coalescence associated with dispersoids. Quantitative fractography, three-dimensional (3-D) reconstruction of fracture surfaces, and metallographic crack profiles indicate that void sheeting is retarded as temperature increases from 25 °C to 150°C, consistent with a rising fracture resistance. Primary microvoids nucleate from smaller constituent particles in the low Cu alloy, and fracture strain increases. A strain-controlled micromechanical model accurately predicts K JICi as a function of temperature, but includes a critical distance parameter (l*) that is not definable a priori. Nearly constant initiation toughness for AA2519+Mg+Ag is due to rising fracture strain with temperature, which balances the effects of decreasing flow strength, work hardening, and elastic modulus on the crack-tip strain distribution. Ambient temperature toughnesses of the low Cu variant are comparable to those of AA2519+Mg+Ag, despite increased fracture strain, because of reduced constituent spacing and l*.  相似文献   

13.
Mechanisms influencing the plane-strain fracture toughness behavior of commercial aluminum-lithium alloys at cryogenic temperatures are investigated as a function of microstructure and plate orientation. It is confirmed that certain alloys show a markedincrease in tensile ductility and toughness withdecrease in temperature, although such behavior is not found in the short-transverse orientations, or for all alloys and aging conditions. Specifically at lower temperatures, the majority of Al-Li alloys, namely 2090-T8E41, 8091-T8X, 8090-T8X, and 2091-T351, show a significantincrease in fracture toughness in the in-plane orientations (L-T, T-L), without any apparent change in fracture mode. Such behavior is attributed primarily to loss of through-thickness constraint resulting from enhanced short-transverse delamination (termed crack-divider delamination toughening), consistent with observed reductions in plane-strain ductility and short-transverse (S-L, S-T) toughness. Conversely, in underaged microstructures of 8091, 8090, and peak-aged 2091, a decrease in toughness with decreasing temperature is found for both L-T and S-L orientations, behavior, which is associated conversely with a fracture-mode change from ductile void coalescence to brittle transgranular shear and integranular delamination at lower temperatures. W{upeikang} Y{upu}, formerly with the Department of Materials Science and Mineral Engineering, University of California, Berkeley  相似文献   

14.
This article presents the results of a study of the fatigue and fracture behavior of a damage-tolerant Nb-12Al-44Ti-1.5Mo alloy. This partially ordered B2 + orthorhombic intermetallic alloy is shown to have attractive combinations of room-temperature ductility (11 to 14 pct), fracture toughness (60 to 92 MPa√m), and comparable fatigue crack growth resistance to IN718, Ti-6Al-4V, and pure Nb at room temperature. The studies show that tensile deformation in the Nb-12Al-44Ti-1.5Mo alloy involves localized plastic deformation (microplasticity via slip-band formation) which initiates at stress levels that are significantly below the uniaxial yield stress (∼9.6 pct of the 0.2 pct offset yield strength (YS)). The onset of bulk yielding is shown to correspond to the spread of microplasticity completely across the gage sections of the tensile specimen. Fatigue crack initiation is also postulated to occur by the accumulation of microplasticity (coarsening of slip bands). Subsequent fatigue crack growth then occurs by the “unzipping” of cracks along slip bands that form ahead of the dominant crack tip. The proposed mechanism of fatigue crack growth is analogous to the unzipping crack growth mechanism that was suggested originally by Neumann for crack growth in single-crystal copper. Slower near-threshold fatigue crack growth rates at 750 °C are attributed to the shielding effects of oxide-induced crack closure. The fatigue and fracture behavior are also compared to those of pure Nb and emerging high-temperature niobium-based intermetallics.  相似文献   

15.
Ambient- to elevated-temperature fracture and fatigue-crack growth results are presented for five Mo-Mo3Si-Mo5SiB2-containing α-Mo matrix (17 to 49 vol pct) alloys, which are compared to results for intermetallic-matrix alloys with similar compositions. By increasing the α-Mo volume fraction, ductility, or microstructural coarseness, or by using a continuous α-Mo matrix, it was found that improved fracture and fatigue properties are achieved by promoting the active toughening mechanisms, specifically crack trapping and crack bridging by the α-Mo phase. Crack-initiation fracture toughness values increased from 5 to 12 MPa√m with increasing α-Mo content from 17 to 49 vol pct, and fracture toughness values rose with crack extension, ranging from 8.5 to 21 MPa√m at ambient temperatures. Fatigue thresholds benefited similarly from more α-Mo phase, and the fracture and fatigue resistance was improved for all alloys tested at 1300 °C, the latter effects being attributed to improved ductility of the α-Mo phase at elevated temperatures.  相似文献   

16.
Micromechanisms influencing crack propagation in a unidirectional SiC-fiber (SCS-8) continuously reinforced Al-Mg-Si 6061 alloy metal-matrix composite (SiCf/Al-6061) during monotonie and cyclic loading are examined at room temperature, both for the longitudinal (0 deg or L-T) and transverse (90 deg or T-L) orientations. It is found that the composite is insensitive to the presence of notches in the L-T orientation under pure tension loading due to the weak fiber/matrix interface; notched failure strengths are ∼1500 MPa compared to 124 MPa for unreinforced 6061. However, behavior is strongly dependent on loading configuration, specimen geometry, and orientation. Specifically, properties in SiCf/Al in the T-L orientation are inferior to unreinforced 6061, although the composite does exhibit increasing crack-growth resistance with crack extension (resistance-curve behavior) under monotonie loading; peak toughnesses of ∼16 MPa√m are achieved due to crack bridging by the continuous metal phase between fibers and residual plastic deformation in the crack wake. In contrast, such bridging is minimal under cyclic loading, as the ductile phase fails subcritically by fatigue such that the transverse fatigue crack-growth resistance is superior in the unreinforced alloy, particularly at high stress-intensity levels. Conversely, fatigue cracks are bridged by unbroken SiC fibers in the L-T orientation and exhibit marked crack deflection and branching; the fatigue crack-growth resistance in this orientation is clearly superior in the composite.  相似文献   

17.
Fracture toughness of the lean duplex stainless steel LDX 2101   总被引:1,自引:0,他引:1  
Fracture toughness testing was performed on the recently developed lean duplex stainless steel LDX 2101 (EN 1.4162, UNS S32101). The results were evaluated by master curve analysis, including deriving a reference temperature. The master curve approach, originally developed for ferritic steels, has been used successfully. The reference temperature corresponds to a fracture toughness of 100 MPa√m, which characterizes the onset of cleavage cracking at elastic or elastic-plastic instabilities. The reference temperature, T 0, was −112 °C and −92 °C for the base and weld materials, respectively. In addition, the fracture toughness is compared with impact toughness results. Complementary crack tip opening displacements (CTODs) have also been calculated. The toughness properties found in traditional duplex stainless steels (DSS) are generally good. The current study verifies a high fracture toughness for both base and weld materials and for the low alloyed grade LDX 2101. Even though the fracture toughness was somewhat lower than for duplex stainless steel 2205, it is still sufficiently high for most low-temperature applications.  相似文献   

18.
Fatigue crack growth rate behavior in CORONA 5, an alloy developed for applications requiring high fracture toughness, has been examined for eight material conditions. These conditions were designed to give differences in microstructure, strength level (825 to 1100 MPa [120 to 160 ksi]), and oxygen content (0.100 to 0.174 wt pct), in such a manner that the separate effects of these variables could be defined. For all eight conditions, fatigue crack growth rates (da/dN) are virtually indistinguishable over the full spectrum of stress-intensity range (ΔK) examined,viz., 8 to 40 MPa√m (7 to 36 ksi√in). Concomitantly, it is noted that over the sizable solution annealing range studied (830° to 915 °C [1525° to 1675 °F]), the primary α-phase morphology was substantially invariant. Eachda/dN curve exhibits a bilinear form with a transition point (ΔKT) between 16 and 19 MPa√m (15 and 17 ksi√in). A change in microfractographic appearance occurs at ΔKT, as extensive secondary cracking along α/β interfaces is observed at all hypertransitional levels ofAK, but not for AK < ΔKT. For each material condition, the mean length of primary α platelets is approximately the same as the cyclic plastic zone size at ΔKT. Accordingly, locations ofAKT (and their similarity for the different material conditions) are rationalized in conformance with a cyclic plastic zone model of fatigue crack growth. Finally, the difference in behavior of CORONA 5, as compared to conventional α/β alloys such as Ti-6A1-4V, is rationalized in terms of crack path behavior.  相似文献   

19.
The fracture resistance of a binary TiAl alloy   总被引:6,自引:0,他引:6  
The fracture resistance of a binary Ti-47Al (in at. pct) alloy has been investigated. The binary alloy was cast, forged, and heat treated to a fully lamellar microstructure with a colony size of either 640 or 1425 μm. Fracture toughness tests were performed in a scanning electron microscope (SEM) equipped with a loading stage. Direct observations of the fracture process indicated that crack extension commenced at a stress intensity level of 1.2 to 4 MPa√m. The crack path was primarily interlamellar and crack extension across an individual colony or across similarly oriented colonies was relatively easy. In contrast, crack arrest was prevalent when the crack encountered the boundaries of unfavorably oriented colonies. To extend into an unfavorably oriented neighboring colony, the K level of the approaching crack had to be increased significantly to renucleate a microcrack at a location away from the crack tip, resulting in the formation of an interconnecting ligament that must be fractured to further crack growth. This interaction between the crack and the microstructure led to a large variation in the slope of the K R curves. Comparison of the K R curves for the binary Ti-47Al alloy against published data for quinary Ti-47Al-xNb-yCr-zV alloys indicates that the initiation toughness of the quinary alloys is higher by a factor of 5 to 10, implying the existence of a significant beneficial effect of alloying additions on the initiation toughness.  相似文献   

20.
The deformation and fracture behavior of 8090 Al-Li alloy at low temperature has been studied by the in situ SEM observation of L-T and S-T oriented specimens. It shows that the overall deformation mode of both L-T and S-L oriented specimens changes from the planar slip to the homogeneous deformation with decreasing temperature. Such change in the deformation mode with the test temperature results in the increase in elongation of L-T oriented specimen with decreasing temperature, but not that of S-L oriented specimen. It has been suggested that the different mechanism is operating in controlling the low temperature mechanical behavior of Al-Li alloys depending on the specimen orientation. It shows that the overall deformation mode, e.g., homogeneous deformation vs. planar slip, is critical when the fracture occurs mostly transgranularly such as in L-T orientation. On the other hand, when the fracture occurs intergranularly such as in S-L orientation, other factors such as grain boundary strength play a more critical role than the overall deformation mode.  相似文献   

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