共查询到20条相似文献,搜索用时 15 毫秒
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Samaneh Shapouri Seyed Mohammad Elahi Laya Dejam Zohreh Bagheri Atefeh Ghaderi Shahram Solaymani 《SILICON》2018,10(5):1911-1919
Due to the industrial applications of nasno materials, the growth of Copper oxide (CuO) nanowires (NWs) at the same and opposite directions of the electric and gravitational fields was investigated to study the effects of fields on the NWs properties. The experiments were designed to grow NWs using thermal oxidation method at 450 °C for 50 h. NWs growth was evaluated to study two distinct cases; first, substrates exposed to the gravitational field and second those treated with electric field (EF) in-lined with gravitation field (GF). It was observed that the electric field developed a diameter homogeneity while compressing the NWs and decreasing the diameters. Furthermore, the GF influenced only the length of the NWs, while the EF had an impact on both length and diameter of the NWs. The direction of fields played an important role in NWs morphology and intensity of XRD pattern and optical properties. It was also observed that field direction greatly influenced the NWs length and diameter. 相似文献
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以KMnO4和乙醇经氧化还原反应所得γ-MnOOH为前驱物,在10 mol/L KOH溶液中于140℃水热条件下反应72 h,制得了比表面积为53 m2/g的带状Birnessite型层状氧化锰.应用XRD、SEM和氮气吸脱附等技术对制备产物进行了结构和形貌表征.同时,在1.0 mol/L Na2SO4水溶液中研究了带状氧化锰的电容性质.结果显示,当扫描速度为5 mV/s时,其比电容为180F/g.循环测试2000圈后,比电容保持率为72%. 相似文献
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以三水硝酸铜为反应物,氨水为络合剂,氢氧化钠为沉淀剂,乙醇水混合溶液为反应溶剂,聚乙二醇为分散剂,采用络合沉淀法,成功制备出平均粒径约20nm的氧化铜单晶纳米粉体。通过单因素实验和正交实验考察了硝酸铜溶液初始浓度、反应温度及氢氧化钠与硝酸铜物质的量比等因素对产物粒径大小的影响,利用x射线衍射(XRD)、透射电镜(TEM)和红外光谱仪(FT-IR)等对产物进行表征分析。研究结果表明,影响其粒径大小主要因素的主次顺序依次是:反应温度,硝酸铜溶液初始浓度及氢氧化钠与硝酸铜的物质的量比;优化制备工艺条件为:反应温度70℃,硝酸铜溶液初始浓度0.3mol/L,氢氧化钠与硝酸铜的物质的量比3:1,氨与硝酸铜的物质的量比5:1;氧化铜纳米粉体的红外吸收峰出现了红移和蓝移同时并存的反常现象。 相似文献
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采用硅溶胶-凝胶法改性乙二胺氯化铜络合物,制备了一种具有温敏连续多变色性能的改性乙二胺/氯化铜复合材料。探讨了溶胶组分中正硅酸四乙酯用量对复合材料的稳定性以及引发剂盐酸对其温敏变色性能的影响,考察了改性乙二胺/氯化铜复合材料的温敏变色机理。结果表明,在120℃复合材料水配体被取代,发生从无色到黄色的颜色变化,在160℃时水分子重新与中心铜离子配位,同时氮配体发生质子转移,复合材料颜色由黄色变为蓝色。正硅酸四乙酯改性后复合材料有较好的稳定性,随着盐酸浓度增加,氯离子配位几率增大,改性乙二胺/氯化铜复合材料的颜色变得更深。 相似文献
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Polycrystalline Al2 O3 fabricated into plates or shapes by hot-working techniques exhibits high in-line transmittance from 0.4 to 5.5 μm. Examination of the product by an inverse pole figure technique demonstrated a strong {0001} texture normal to the pressing direction for both equiaxed and textured microstructures. The crystallographic texture was attributed to the dominance of basal slip in deformation. A comparison of transmissivity in the 2 principal directions of a forged plate strongly suggested that a reduction of birefringence resulting from the crystallographic texture was partially responsible for the high transmissivity. The absorption coefficient at 4.5 μm was 0.15 mm-1 , ∼ that for sintered Al2 O3 and 5 times that for sapphire 相似文献
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《国际聚合物材料杂志》2012,61(1-2):233-242
Abstract Progress in structure and properties of polymeric supramolecular assembly in Japan is reviewed. 相似文献
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Electrical and Optical Properties of Tin Oxide Films 总被引:1,自引:0,他引:1
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Saira Jabeen Bakhtiar Muhammad Sagheer Gul Muhammad Farooq 《Polymer-Plastics Technology and Engineering》2015,54(13):1379-1409
In this review, an overview of various types of nanofillers is presented with special emphasis on structure, synthesis and properties of carbon nanotube, nanodiamond, and nanobifiller of carbon nanotube/nanodiamond, carbon nanotube/graphene oxide and carbon nanotube/graphene. In addition, polymer/carbon nanotube, polymer/nanodiamond, and polymer/nanobifiller composites have been discussed. The efficacy of different fabrication techniques for nanocomposites (solution casting, in-situ, and melt blending method) and their properties were also discussed in detail. Finally, we have summarized the challenges and future prospects of polymer nanocomposites reinforced with carbon nanofillers hoping to facilitate progress in the emerging area of nanobifiller technology. 相似文献
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Six preparation methods for polymeric organic-inorganic nanocomposites and their respective mechanisms and features are reviewed. The extraordinary properties of polymeric organic-inorganic nanocomposites are discussed,and their potential applications are evaluated. 相似文献
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以蚕丝蛋白为模板,在相对温和的条件下通过生物矿化的手段形成具有特殊形貌的α-GaOOH颗粒,并通过在不同温度下煅烧α-GaOOH得到α-Ga2O3和β-Ga2O3.采用扫描电镜(SEM)、透射电镜(TEM)、X射线衍射仪(XRD)和荧光分光光度计(PL)等手段研究了丝素蛋白多肽和矿化时间对颗粒的影响,对其生物矿化机理进行了初步探讨.结果表明,所制备的β-Ga2O3具有优良的发光特性,丝素蛋白多肽模板以无定形的结构与产物结合在一起,并且经过高温烧结后仍以碳膜的形式包覆在材料的表面.这种碳膜结构对于提高材料的生物学性能起着重要的作用. 相似文献
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Six preparation methods for polymeric organic-inorganic nanocomposites and their respective mechanisms and features are reviewed. The extraordinary properties of polymeric organic-inorganic nanocomposites are discussed,and their potential applications are evaluated. 相似文献
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