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场活化烧结技术是一种在电场、应力场和温度场作用下实现快速致密化的粉末活化烧结技术.场活化烧结的特殊致密化过程和活化机理,源自于其特有的电场、应力场以及温度场作用.本文就各种场在场活化烧结过程中的特点、作用和影响的研究进展进行介绍.对于各种场在场活化烧结中的特点、作用和影响的认识,仍存在较多问题和分歧.各场间交互作用显著.从多场耦合的角度研究场活化烧结过程,有助于更准确、全面掌握各种场的特点、作用和影响,深入揭示场活化烧结的特殊致密化过程和活化机理.通过外加磁场提高场活化烧结的均匀性,进一步赋予材料特殊性能,具有良好的研究开发前景. 相似文献
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对W-4Ni-2Co-1Fe高能球磨粉末,分别采用脉冲电流烧结 恒流电流烧结和恒流电流烧结两种工艺进行制备,研究电流烧结工艺对W-4Ni-2Co-1Fe合金性能的影响.结果表明:在脉冲电流基值、峰值、频率和占空比分别为360 A、3 000 A、50 Hz和50%,以及恒流电流为1.5 kA、总烧结时间为6 min、烧结压力为30 MPa的条件下,采用2min脉冲 4min恒流电流烧结工艺,合金的密度、硬度和抗弯强度分别达到最大值16.79g/cm3、HRA84和484 MPa;与此烧结工艺相比,采用单一的恒流电流烧结时,通过增大恒流强度可进一步提高烧结密度,但同时合金的硬度和横向断裂强度均相对降低. 相似文献
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对Cu-10Cr-0.5Al2O3(质量分数,%)混合粉末及球磨复合粉末,采用电场活化烧结技术制备高强高导电铜基块体材料,并研究脉冲峰值电流和通电烧结时间对烧结材料组织和性能的影响。结果表明,随着脉冲峰值电流增大,烧结材料的相对密度和导电率均提高,相对密度最高可达99%,硬度和抗弯强度则先上升后下降。当脉冲电流峰值为2.94 kA时,烧结材料具有较好的综合性能,相对密度、硬度、抗弯强度和电导率分别为97.5%、285HV、911MPa和50IACS%;随着通电烧结时间延长,烧结材料的密度、硬度、抗弯强度和导电率均逐渐上升,但烧结时间过长会引起硬度轻微下降;对Cu-10Cr-0.5Al2O3混合粉末进行球磨虽导致烧结材料的电导率下降,但可显著提高材料的硬度和抗弯强度。 相似文献
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以MgO为电解原料,在Na_3PO_3-MgF_2体系中采用旋转铝液阴极法制备铝镁中间合金。采用熔盐电解监控仪和Teslameter测量电解过程中的反电动势、电流强度及磁场强度等工艺参数,并利用SEM及XRD技术分析了合金产物的微观结构,探讨了旋转铝液阴极合金化过程中反电动势、电流效率及合金中镁浓度的变化规律。结果表明,旋转铝液阴极化过程可有效降低反电动势,并提高电流效率及合金中镁的质量浓度。在950℃、电流5 A、外加40 mT磁场的条件下,电解3 h可制取镁含量24.5%的铝镁合金,电流效率可达83%。所得合金样品组织致密,各元素在合金中的分布较均匀,合金物相主要为Al_(12)Mg_(17)。 相似文献
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采用传统铸造技术和半固态过流冷却技术分别制备了A390铝合金铸棒。在MVF-1A摩擦磨损试验机上研究了显微组织、外加载荷和温度对A390铝合金干滑动摩擦磨损性能的影响,对磨环材料为45#钢。采用SEM对A390铝合金磨损面形貌进行了分析。结果表明:相同载荷和温度下,经半固态处理的A390铝合金材料耐磨性能更优异。随着外加载荷的增加,A390的摩擦系数和磨损率呈现先降低和增加的趋势;载荷为80 N时,A390的摩擦系数最稳定,磨损率最小。A390的摩擦系数和磨损率对温度变化较敏感,在100℃以下,磨损率变化较小,以磨粒磨损机制为主;当温度超过100℃时,摩擦系数波动明显,磨损面塑性变形严重,此时同时发生磨粒磨损和粘着磨损。 相似文献
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采用热力学计算软件对LF2合金中的析出相进行计算,采用扫描电子显微镜、透射电子显微镜、微细相分析以及拉伸试验,对不同钛质量分数的LF2合金的微观组织和力学性能进行了研究,结果表明:LF2合金中γ′相以近球形在晶内弥散析出,尺寸约为20 nm,Laves相在晶界以纤维状和块状析出;随钛质量分数增加,γ′相数量增加,钛质量分数增加了0.92%,γ′相的质量分数是原来的1.35倍;Laves相数量增多,由纤维状变为短棒状。随钛质量分数增加,LF2强度增加,γ′相强化效果相对减弱,但γ′相仍然是最主要的强化相。 相似文献
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《钢铁研究学报(英文版)》2016,(3):276-280
The hypereutectic Fe-Cr-C hardfacing alloys with different contents of TiB2 and Nb were prepared by selfshielded flux cored arc welding.The microstructure of a series of hypereutectic Fe-Cr-C hardfacing alloys added with various TiB2 and Nb contents was investigated by using optical microscopy(OM),scanning electron microscopy(SEM)and X-ray diffraction(XRD).In addition,their Rockwell hardness,microhardness and resistance to abrasive wear were tested.The results showed that the microstructure of a series of hypereutectic Fe-Cr-C hardfacing alloys consisted mainly of martensite,austenite,primary M7C3 carbides and eutectic M7C3 carbides.With the addition of TiB2,a new hard-phase TiC was produced in the hardfacing alloys.And in the alloys added with TiB2 and Nb,a new hard composite phase TiC-NbC was formed.The microhardness of the matrix was improved by adding TiB2 and Nb,but the effect on the Rockwell hardness of Fe-Cr-C hardfacing alloys was insignificant.The addition of TiB2 and Nb can also decrease the size of the primary M7C3 carbides and make the primary M7C3 homogeneous.As a result,the reinforced matrix,the more homogeneous primary M7C3 carbides,and the new hard-phase TiC-NbC all improved the wear resistance of Fe-Cr-C hardfacing alloys. 相似文献
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XING 《中国稀土学报(英文版)》2010,28(6):927-930
Eutectic Al-12.6 wt.%Si alloys with various contents of the rare earth dement Er were prepared by the conventional casting technique.The effect of Er on the microstructure and properties of the eutectic Al-Si alloys was investigated using optical microscopy,scanning electron microscopy as well as the friction and wear tests.It was found that the addition of Er obviously improved the anti-wear properties,and reduced the friction coefficient of the alloys.The appropriate addition of Er would change the size and shape of the eutectic silicon,and thereby refine the microstructure of the Al-Si alloys.The refinement mechanism was also discussed. 相似文献
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K. A. Lindahl D. L. Olson J. U. Trefny 《Metallurgical and Materials Transactions A》1996,27(10):2958-2965
Measurements of bulk magnetic properties were investigated to evaluate whether they can be used to reveal the microstructure
and phase stability of alloys. Specifically, phase transformations in aluminum-copper alloys were followed with magnetic susceptibility
measurements. The results suggest that bulk magnetic measurements can be used to predict microstructure and, thus, properties
of alloys. The ability to characterize alloy properties and phase stability through correlation with electromagnetic measurements
may allow significant improvements in the nondestructive evaluation of advanced alloy properties and the prediction of service
life. 相似文献
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采用粉末冶金方法制备含Y2O3的稀土钼合金,利用金相显微镜、扫描电子显微镜(SEM)、X射线衍射(XRD)、能谱分析(EDS)等手段对钼合金的断裂特征和组织结构进行对比分析,研究稀土氧化物Y2O3含量对钼合金组织和性能的影响.研究表明:添加Y2O3能细化晶粒、改善钼合金的晶粒均匀性和致密度、提高钼合金的性能:拉伸强度和屈服强度随Y2O3含量的增加呈现先增高后降低的趋势,在Y2O3含量为1%时,抗拉强度达511.43MPa,屈服强度456.99MPa,分别是纯钼材料的1.31倍和1.57倍,综合力学性能最佳;在烧结坯中,Y2O3颗粒分布均匀,主要以球形和等轴状形式存在于晶界上. 相似文献
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The mechanism of formation of the fine duplex microstructure resulting from the α → γ transformation in water-quenched Ti-48Al-2Mn-2Nb
alloys was studied using transmission and analytical electron microscopy. As-cast Ti-48Al-2Mn-2Nb alloys were heat treated
in the α phase field and water quenched to room temperature. The resulting microstructure (referred to as a fine duplex microstructure)
consisted of equiaxed grains and abutting lath colonies. Both the colonies and the grains were composed of the γ phase, twinned
γ laths, and α2 laths. It was found that the transformation from α to γ in the fine duplex microstructure took place through long range diffusional
processes, and compctitive growth between the equiaxed and lath morphology occurred. Nucleation of they phase from the α matrix can occur through nucleation on stacking faults, followed by growth through the sympathetic nucleation
and growth of new γ laths on a substrate lath. The observed misorientations and the interfacial structures between the laths
were found to be consistent with such a mechanism. Compctition between such nucleation and growth mechanisms for the equiaxed
and lath morphologies of γ leads to the formation of lath colonies (of γ and α2) interspersed with equiaxed grains in these alloys.
Formerly Visiting Scientist, Metals and Ceramics Division, Oak Ridge National Laboratory
This article is based on a presentation made during TMS/ASM Materials Week in the symposium entitled “Atomistic Mechanisms
of Nucleation and Growth in Solids,” organized in honor of H.I. Aaronson’s 70th Anniversary and given October 3–5, 1994, in
Rosemont, Illinois. 相似文献
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The microstructure and strength at 1473 and 2073 K and creep properties at 2073 K were investigated in three Ir-Nb-Zr alloys
with the fcc and L12 two-phase structure. The microstructure and lattice misfit were investigated using scanning electron microscopy (SEM), transmission
electron microscopy (TEM), and X-ray diffractometry (XRD). Compression and creep tests were performed, and their deformation
structures were observed using SEM and TEM. At 1473 K, the strength of the Ir-Nb-Zr alloys was higher than that of the binary
Ir-Nb and Ir-Zr alloys, but they were almost equivalent at 2073 K. However, the ternary alloys showed great improvement on
creep at 2073 K. The time for the 2 pct creep strain of the Ir-Nb-Zr alloy was about 100 hours, while it was 1 hour for the
binary alloys. The deformation mechanisms for compressive strength and creep resistance in these Ir-Nb-Zr alloys are discussed
in terms of the deformation structure.
This article is based on a presentation made in the symposium entitled “Fundamentals of Structural Intermetallics,” presented
at the 2002 TMS Annual Meeting, February 21–27, 2002, in Seattle, Washington, under the auspices of the ASM and TMS Joint
Committee on Mechanical Behavior of Materials. 相似文献
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采用金相(OM)、透射电镜(TEM)及能谱分析(EDS)、硬度测试的方法研究了单级与双级时效热处理制度对Al-4.9Zn-1.6Mg-0.4Mn-0.1Zr-xEr合金板材硬度和显微组织的影响.结果表明,添加Er元素后合金中形成了纳米级的A13(Zr,Er)相,可以强烈地钉扎位错,细化再结晶晶粒.无论单级时效还是双级时效,Er元素的添加均可以提高合金的硬度,加快合金的时效硬化速率,使合金达到硬度峰值的时间缩短,但Er含量对提高合金硬度的影响不大.同时,晶界处出现的第二相颗粒析出带得到消除,合金中存在明显的沉淀无析出带.此外,Er元素可以促进Zn,Mg元素的固溶,而析出的A13(Zr,Er)颗粒又可以促进MgZn2相的析出. 相似文献
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采用固相烧结工艺(1 300℃保温1 h)制备低钨含量(质量分数为60%~80%)的W-Ni-Fe合金,测定合金的抗拉强度、抗压强度和伸长率,利用金相显微镜观察合金的显微组织,并通过扫描电镜(SEM)观察合金断口形貌,研究钨含量对固相烧结W-Ni-Fe合金力学性能与微观结构的影响。结果表明:随钨含量降低,合金的孔隙率和平均孔径减小,抗拉强度增大,伸长率显著提高,抗压强度变化不大。W含量为60%~80%的W-Ni-Fe合金,其孔隙率为17.8%~21.4%,抗拉强度为231~262 MPa,抗压强度2 450~2 550 MPa,伸长率为0.3%~2.3%,压拉比为9.45~11.04,都能满足易碎型穿甲弹弹芯材料的性能要求。 相似文献
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在铝合金粉末中添加质量分数为0、0.2%、0.4%及0.6%的稀土元素Y, 利用粉末冶金法制备2A12铝合金。通过金相组织观察、X射线衍射分析、扫描电子显微形貌表征、能谱分析及力学性能测试等手段, 研究了稀土元素Y对粉末冶金2A12铝合金组织和性能的影响, 总结了Y在铝合金中的分布特征。结果表明, 当稀土元素Y的质量分数为0.2%时, 2A12铝合金抗拉强度最高, 塑性最好; 添加Y可以抑制铝合金晶粒在烧结过程中的长大; 稀土元素Y主要以YAl相、Cu2Y相和YAl2相的形式分布在基体晶界处, 少量Y固溶在铝基体中。 相似文献