微合金化钢的动态再结晶及其显微组织的研究

应用Ｇｌｅｅｂｌｅ－１５００热模拟试验机测定了微合金化钢在不同终轧温度下的真应力－－真应变曲线，研究了终轧温度及微合金元素含量对动态再结晶的影响，研究结果表明，Ｖ，Ｎｂ可显著抑制微合金化钢轧制过程中形变奥氏体的动态再结晶，因此，在较高的终轧温度下，仍能得到细小而均匀的显微组织。     

稀土对4145H钻铤钢动态再结晶的影响

应用Geeble-1500D热模拟试验机分别对稀土含量为6×10-6和16×10-6的钻铤钢进行单道次压缩实验,测定其不同终轧温度下的真应力-真应变曲线,采用应变速率0.01 s-1,变形量60%,终轧温度为850,950,1050,1150℃,研究不同稀土含量,不同终轧温度对钻铤钢再结晶的影响。结果表明,稀土含量为16的钻铤钢能显著地抑制形变奥氏体的动态再结晶。     

82B钢线材精轧过程的再结晶行为

结合某钢厂高碳钢线材生产线轧制82B钢的工艺参数,在Gleeble1500D热模拟实验机上采用不同精轧温度制度模拟了精轧F1-F4阶段该钢的轧制变形,分析了精轧温度对精轧过程中各道次动态再结晶的影响.研究结果表明,精轧F1-F4道次变形温度的控制对82B线材的组织有重要影响,精轧温度特别是精轧出口温度过高易使F4道次轧制发生不完全动态再结晶,不利于组织控制.     

Mg-RE复合处理对SS400钢铁动态再结晶行为的影响

利用Gleeble 1500型热模拟试验机进行单道次热压缩实验,测定不同温度下的真应力真应变曲线,分析了不同Mg-RE含量对SS400钢动态再结晶行为的影响.结果表明,稀土对动态再结晶有强的固溶拖曳作用,经Mg-RE复合处理的SS400钢形变抗力大;加入Mg-RE后,SS400钢的动态再结晶开始时间增大,从而提高了再结晶温度.     

相变区等温处理对V-N钢轧后组织的影响

研究轧后等温处理工艺对微合金V—N钢γ→α相变组织的影响。对含氮量不同的两种低碳V钢进行了模拟轧制和控轧冷却，接着于650～700℃进行了等温处理，使发生γ-α相变。用光学显微镜和透射电子显微镜(TEM)观察和比较了钢中的显微组织转变特点。结果表明，随等温温度的降低及保温时间的延长，铁素体的转变量增加；增加钢中的氮含量，能明显促进轧后显微组织中铁素体的生成，有利于细化晶粒。     

Q345B微合金钢的高温变形行为

利用Gleeble-1500D热模拟试验机对V,Ti,Nb微合金化Q345B低合金高强度结构钢(HSLA)进行了高温单道次压缩实验.测量了不同变形温度和变形速率下该钢的变形行为,分析了各变形参数对该钢动态再结晶和变形抗力的影响,得出动态再结晶激活能为451.47 kJ.mol-1,并且得出峰值应力和峰值应变都与lnZ之间的关系近似于直线.     

X80管线钢热变形过程中再结晶行为及组织细化

利用Gleeble-1500D热模拟试验机研究了X80管线钢热轧过程中的再结晶行为及精轧过程中后四道次变形的再结晶特点与室温组织的关系.揭示了X80管线钢动态再结晶临界钢应变量与变形温度的关系,确定了奥氏体再结晶温度区和非再结晶温度区,所得到的技术要点对精轧过程轧制工艺制定细化奥氏体晶粒具有指导性,有助于X80管线钢获得细小均匀的室温组织.     

高速线材导卫辊轮新材料研究

研究了多元合金化材料(在低高速钢中添加V,Nb,N,Re等元素)的组织结构和性能.结果表明,由于添加元素Nb推迟α-Fe的再结晶温度,添加W,Mo,V,Nb,C,N形成复合碳、氮化物等因素,经1250℃淬火,550℃3次回火2 h,试验钢有明显的二次硬化效果,硬度HRC 64.8.550℃保温16 h后的硬度为HRC 62.6,有很好的热稳定性.耐磨性接近于普通高速钢,W,Mo含量仅为普通高速钢的50%,是一种节能型高性能耐磨材料.     

轧制工艺对微合金V-N钢显微组织和性能的影响

对0.14C-0.016V-0.014N的低碳微合金V-N钢分别进行终轧温度为950,900,850℃、形变量为30%,40%,50%的控制轧制;对轧后试样进行了拉伸试验、显微组织分析、晶粒度以及铁素体含量测定.结果表明,轧制形变量对试验钢性能和组织有明显影响.降低轧制温度及增大轧制形变量,晶粒度增大,晶粒尺寸减小,钢的强度提高.     

中间形变热处理对8090铝锂合金组织和性能的影响

研究了终轧前过时效温度和终轧温度对８０９０铝锂合金再结晶行为和力学性能的影响。结果表明：过时效温度对再结晶行为和力学性能有很大影响。终轧温度的影响与过时效温度有关。     

Modeling of microstructural evolution during dynamic recrystallization in coarse Nb microalloyed austenite

The aim of the current study was to investigate the microstructural evolution during dynamic recrystallization in coarse Nb microalloyed austenite in thin slab direct rolling （TSDR） processing. A model was developed to predict the change of the austenite grain size during the dynamic recrystallization, by using the law of mixtures. The equations initially developed for partial static recrystallization were used for partial dynamic recrystallization, by adjusting the value of the constant. The results show that the change of the austenite grain size can be reasonably described by using the equations developed according to the law of mixtures.     

Kinetics for static recrystallization after hot working of 0.38C-0.99Cr-0.16Mo steel

The restoration mechanisms for static reerystallization of work-hardened austenite were investigated by using double-pass compression tests performed on medium-carbon steel containing chromium and molybdenum. The softening fraction was defined by 2% offset method. The results show that Avrami exponent of about 0.21 is insensitive to deformation temperature, indicating that the action of steel grade should be considered. The time of 50% recrystallization (t0.5) decreases noteworthily with the increase of deformation temperature. Apparent activation energy for static recrystallization of 195 kJ/mol, which is close to that of vanadium microalloyed steel, is obtained by calculating. The increasing trend of the driving force for recrystallization is opposite to that of the deformation temperature, which is attributed to the number of operative slip system increasing as temperature increasing.     

Dynamic recrystallization behaviour of Nb-Ti microalloyed steels

The dynamic recrystallization （DRX） behavior of Nb-Ti microalloyed steels was investigated by isothermal single compression tests in the temperature range of 900-1 150 ℃ at constant strain rates of 0.1-5 s^-1. DRX was retarded effectively at low temperature due to the onset of dynamic precipitation of Nb and Ti carbonitrides, resulting in higher values of the peak strain. An expression was developed for the activation energy of deformation as a function of the contents of Nb and Ti in solution as well as other alloying elements. A new value of corrective factor was determined and applied to quantify the retardation produced by increase in the amount of Nb and Ti dissolved at the reheating temperature. The ratio of critical strain to peak strain decreases with increasing equivalent Nb content. In addition, the effects of Ti content and deformation conditions on DRX kinetics and steady state grain size were determined. Finally, the kinetics of dynamic precipitation was determined and effect of dynamic precipitation on the onset of DRX was clarified based on the comparison between precipitate pinning force and recrystallization driving force.     

合金元素Mo对冷轧双相钢组织的影响

分析Mo微合金冷轧双相钢和普通C-Mn冷轧双相钢在不同双相热处理工艺下微观结构,讨论Mo对冷轧双相钢组织变化规律的影响。实验结果表明：当两种双相钢以1700℃／s冷却时,均获得了铁素体、马氏体双相组织,马氏体均匀分布在铁素体基体上,随着加热温度的升高,普通C-Mn双相钢得到的马氏体体积分数多。当以5．4℃／s冷却时,Mo微合金双相钢得到的马氏体体积分数多;当加热到820℃保温结束后以5．4℃／s的速率冷却时,普通C-Mn钢的组织组成相为铁素体、珠光体、马氏体;Mo微合金钢的组织组成相为铁素体、贝氏体、马氏体;Mo对铁素体晶粒的细化作用不明显。     

Constitutive Modeling and Dynamic Recrystallization Mechanisms of an Ultralow-carbon Microalloyed Steel During Hot Compression Tests

The hot deformation behavior of an ultralow-carbon microalloyed steel was investigated using an MMS-200 thermal simulation test machine in a temperature range of 1 073-1 373 K and strain rate range of 0.01-10 s~(-1).The results show that the flow stress decreases with increasing deformation temperature or decreasing strain rate.The strain-compensated constitutive model based on the Arrhenius equation for this steel was established using the true stress-strain data obtained from a hot compression test.Furthermore,a new constitutive model based on the Z-parameter was proposed for this steel.The predictive ability of two constitutive models was compared with statistical measures.The results indicate the new constitutive model based on the Z-parameter can more accurately predict the flow stress of an ultralow-carbon microalloyed steel during hot deformation.The dynamic recrystallization (DRX) nucleation mechanism at different deformation temperatures was observed and analyzed by transmission electron microscopy (TEM),and strain-induced grain boundary migration was observed at 1 373 K/0.01 s~(-1).     

Plastic deformation behavior of ZK60 magnesium alloy with addition of neodymium

The hot deformation simulation of a ZK60 magnesiuln alloy at different temperatures from 373 to 673 K and different strain rates of 0.1, 0.01 and 0.002 s^-1 was studied by using the Gleebe-1500 simulator. The plastic deformation behavior was measured and the deformation activation energy was calculated. The microstructures of ZK60 magnesium alloy with an addition of neodymium during the deformation process were observed by using Polyvar-MET optical microscope and Tecnai G^2 20 TEM. The results show that the working hardening, the dynamic recovery and the dynamic recrystallization occur during the plastic deformation process at different temperatures and strain rates. The dynamic recrystallization starts when the temperature is over 473 K and the DRX grain size after hot deformation is only 5-10 μm. So the refined grains improve both the tensile strength and the elongation of alloys at room temperature. Neodymium is added into the alloy and a precipitate phase Mg12Nd that impedes the movement of dislocations is formed, which benefits to increasing mechanical properties of ZK60 magnesium alloy.     

Surface recrystallization of a single crystal nickel-base superalloy

The recrystallization behavior of a single crystal nickel-base superalloy was investigated by shot peening and subsequent annealing. Two kinds of recrystallization microstructures, which are intensively dependent on the annealing temperature, are shown in the nickel-base superalloy after shot peening and subsequent annealing. Surface recrystallized grains are obtained when the superalloy is annealed at solution treatment temperature. The nucleation of recrystallization originates from the dendritic core, wh...