共查询到18条相似文献,搜索用时 140 毫秒
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本文以烘干恒重的党参粉末为原料,研究微波提取法和乙醇浸提法的提取工艺和影响因素,并将这两种优化工艺条件进行比较。这两种方法都是以乙醇作为提取溶剂,分别研究溶剂浓度、液固比、提取时间、乙醇浸提的提取温度或微波提取的微波功率对党参皂甙提取率的影响。结果表明,微波提取法中4个因素影响党参皂甙提取率的主次顺序为乙醇浓度加热时间液固比微波功率,此方法的最佳提取工艺条件为:乙醇浓度为70%,液固比为80mL.g-1,提取时间为10×20s,微波功率为320W,皂甙提取率为3.15%。乙醇浸提法中4个因素影响党参皂甙提取率的主次顺序为乙醇浓度液固比加热时间提取温度,此方法的最佳提取工艺条件优化条件为:乙醇浓度为70%,液固比80mL.g-1,加热时间为80min,提取温度70℃,提取率为2.17%。结果证明,微波提取党参皂甙具有简便快速、高效节能、重复性好的优点。 相似文献
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研究了微波辅助提取银杏叶萜类内酯的工艺.对辐射时间、微波功率、乙醇浓度和液固比进行单因素考察,根据考察结果进行正交实验设计,然后进行验证实验,并将该工艺条件与传统加热回流提取方式进行比较.结果表明,微波辅助提取银杏叶萜类内酯的较佳工艺为:辐射时间为8 min,微波功率为500 W,乙醇浓度为70%,液固比为20:1,此条件下萜类内酯提取率可达1.620 mg·g~(-1).与传统加热回流提取相比,微波辅助提取得到的萜类内酯提取率高出31%,溶剂用量减少33%,提取时间大大缩短.该方法是一种较为理想的银杏叶萜类内酯提取方法. 相似文献
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以槐花米为原料,芦丁产率为评价指标,进行微波辐射下提取芦丁的工艺研究,考察了微波功率、提取温度、时间和固液比等对芦丁产率的影响。结果表明,优化工艺条件为:槐花米2 g,澄清石灰水50 mL,温度120℃,功率500 W,提取时间为20 min。优化工艺条件下,粗产品的产率为3.5%,纯度为83.6%。微波法提取芦丁具有提取率高、提取时间短、产品纯度高等优点,为综合开发该资源提供了有益的参考。 相似文献
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This study was aimed at evaluating the physicochemical properties and oxidation stability of castor oil using microwave-assisted solvent extraction (MAE). MAE was performed using 5% ethanol in hexane as solvent at different extraction times, power intensities and solvent-to-feed (S/F, ml of solvent to gram of feed) ratios. The process parameters were optimized by statistical approach using historical data design of response surface method (RSM). The oils were characterized for yield, physicochemical properties, dielectric properties and oxidation stability, and comparison was also made with oil extracted using Soxhlet method. Results show that the maximum oil yield of 37% was obtained at 20 min with microwave power intensity of 330 W and S/F ratio of 20. The main fatty acid composition of castor oil is ricinoleic acid. The density, refractive index, dielectric properties and oxidation stability of oils are not affected by the extraction methods and extraction parameters of MAE. However, the MAE-extracted oil is more viscous compared to that by Soxhlet method. With extra caution on oil oxidation, MAE could be a promising solvent extraction method with an 86% less in processing time and a higher yield. 相似文献
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《分离科学与技术》2012,47(2):289-299
ABSTRACTPhenolic compounds were extracted from pistachio hull using microwave-assisted solvent extraction (MASE). The effects of four parameters, microwave power, extraction time, solvent to sample ratio, and ethanol concentration were evaluated. The extraction conditions were optimized by response surface methodology to enhance the total phenolic content (TPC). Optimal conditions were found as 140 W microwave power, 4.5 min extraction time, 19:1 (v/w) solvent to sample ratio, and 56% ethanol concentration to get maximum TPC (62.24 mg GAE/g dry hull). Also, MASE was compared with conventional solvent extraction (CSE) and MASE gave higher TPC, yield, and antioxidant activity. 相似文献
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考察了表面活性剂协同微波提取金莲花黄酮的工艺,筛选出了具有明显增效作用的表面活性剂十二烷基硫酸钠(SDS),最后通过正交实验优化了提取工艺.结果表明,最佳工艺条件为:以质量浓度0.75 g/L的表面活性剂SDS水溶液为提取剂,提取溶剂用量为40 mL/g金莲花,微波功率600 W,温度70℃,提取时间5 min.在该工艺条件下,金莲花黄酮的提取率为5.35%.与溶剂浸提法相比,提取时间显著缩短,金莲花黄酮的提取率提高约30%. 相似文献
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通过微波辅助混合溶剂提取技术结合响应面法优化原花青素提取条件,以期建立更高产率的提取方法。在单因素设计基础之上,选取液料比、微波功率、萃取时间、萃取温度4个主要因素对原花青素提取率的影响,建立多元回归拟合分析,得出原花青素提取最佳工艺条件为:液料比1:10,萃取温度61℃,微波功率625 W,萃取时间39 min,此条件下原花青素提取率1.78%,为预测值的89.45%。 相似文献
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微波-表面活性剂协同提取山竹外衣色素 总被引:2,自引:2,他引:2
研究了微波-表面活性剂协同提取法(MAME)提取山竹外衣色素的工艺条件与过程。考察了提取剂中表面活性剂类型和含量、提取液pH、微波提取功率、时间、浸泡固液质量比和时间对色素提取率的影响,实验结果表明:pH=1时,以w(聚氧乙烯十二酸失水山梨醇单酯)=0.08%的乙醇溶液〔φ(CH3CH2OH)=70%〕为提取剂,山竹外衣按m(山竹外衣)∶m(提取剂)=1∶263浸泡于提取剂中5 m in、微波功率800 W下提取25 s,色素提取率为96.26%。该法一次提取率是传统溶剂法的1.78倍,提取时间是溶剂法的1/240,聚氧乙烯十二酸失水山梨醇单酯对色素提取有增溶作用。 相似文献
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《分离科学与技术》2012,47(1):243-262
Abstract Microwave-assisted extraction (MAE) was applied for the extraction of astaxanthin from Haematococcus pluvialis and response surface methodology (RSM) was used to optimize extraction parameters to the content of astaxanthin. Four independent variables such as microwave power (W), extraction time (sec), solvent volume (mL), and the number of extraction were optimized in this paper. The optimal conditions were determined and tri-dimensional response surfaces were plotted from the mathematical models. The F-test and p-value indicated that microwave power, extraction time, the number of extraction, and their quadratic had a highly significant effect on the response value (p <0.01), then the solvent volume and the interaction effects of microwave power and the number of extraction also displayed significant effect (p <0.05). Considering the extraction efficiency, the optimized conditions of MAE were as follows: microwave power was 141 W, extraction time 83 sec, solvent volume 9.8 mL, the number of extraction four times. About 594 ± 3.02 µg astaxanthin was extracted from Haematococcus pluvialis the dried powders (100 mg) under the optimal conditions, and it close to the predicted contents (592 µg). The antioxidant activities of the extracts obtained under optimal conditions were analyzed, and the results showed that the extracts presented strong ability of inhibiting the peroxidantion of linoleic acid, exhibited strong radical-scavenging properties against the DPPH, as well as strong reducing power. 相似文献