Freeze Drying of Saffron (Crocus sativus L.)

Saffron obtained from the dried stigmas of a flower scientifically known as Crocus sativus L. is considered to be the most precious and expensive agricultural product due to its labor-intensive harvest and post-harvest processing. The post-harvest processing such as dehydration and storage conditions determine stability, quality, and economical value of the final product. The contents of crocin (degraded carotenoids) and safranal (carotenoid oxidation products) are the key components that characterize color, taste, and aroma characteristics of saffron. In this work, the quality parameters such as crocin and safranal contents of commercial saffron that were obtained by using the freeze-drying method and natural sun drying were studied. The sarfanal contents of the samples dried in a freeze dryer were found to be five times higher than the safranal contents of the samples dried naturally under the sun, while crocin contents of the samples dried in a freeze dryer were about 40% higher than the crocin contents of the samples dried naturally under the sun. These encouraging results indicate that the freeze-drying process can be used effectively for dehydration of saffron by minimal loss of safranal and crocin contents.     

Variation in Drying Behavior and Final Moisture Content of Wood during Conventional Low Temperature Drying and Vacuum Drying of Betula pendula Timber

Conventional and vacuum drying experiments were conducted on Betula pendula timber, which was sawn from trees felled during three different seasons. The influence of the wood procurement season on drying behavior differed, on the one hand, between the drying phases above and below 30% moisture content in the conventional drying, and, on the other hand, between the conventional and vacuum drying methods. During the first steps of the conventional drying process, relative humidity in the kiln, as well as drying time and drying rate, varied according to the felling season. Variations in environmental conditions outside the kiln and the seasonal variation in the physical properties of the wood were presumed to be the reasons for differences in drying behavior. The difference in moisture content gradient, i.e., the difference in final moisture content between the inner wood and the surface layer of boards, was greater in conventionally dried timber than in vacuum-dried timber. In conventionally dried timber there was a clear seasonal variation in the gradient of final moisture content, which was greatest for winter-felled wood. The premature drying of the surface layer during the first steps of the conventional drying process of winter-felled wood was the reason for the higher gradient of moisture content. Storage of wood as logs decreased the standard deviation of the final moisture content.     

Variation in Drying Behavior and Final Moisture Content of Wood during Conventional Low Temperature Drying and Vacuum Drying of Betula pendula Timber

Conventional and vacuum drying experiments were conducted on Betula pendula timber, which was sawn from trees felled during three different seasons. The influence of the wood procurement season on drying behavior differed, on the one hand, between the drying phases above and below 30% moisture content in the conventional drying, and, on the other hand, between the conventional and vacuum drying methods. During the first steps of the conventional drying process, relative humidity in the kiln, as well as drying time and drying rate, varied according to the felling season. Variations in environmental conditions outside the kiln and the seasonal variation in the physical properties of the wood were presumed to be the reasons for differences in drying behavior. The difference in moisture content gradient, i.e., the difference in final moisture content between the inner wood and the surface layer of boards, was greater in conventionally dried timber than in vacuum-dried timber. In conventionally dried timber there was a clear seasonal variation in the gradient of final moisture content, which was greatest for winter-felled wood. The premature drying of the surface layer during the first steps of the conventional drying process of winter-felled wood was the reason for the higher gradient of moisture content. Storage of wood as logs decreased the standard deviation of the final moisture content.     

Drying Characteristics of Purslane (Portulaca oleraceae L.)

Thin layer drying rates of purslane were determined experimentally as a function of temperature with air velocity kept constant at 1.1 m/s and relative humidity below 5%. Thin layer drying data were obtained for purslane at four drying air temperatures (35, 70, 95, and 120°C). Five thin layer-drying models (Henderson and Pabis, exponential, Page, two-term exponential, and Thompson models) were fitted to the drying data. The color of purslane was determined after drying using a spectro-colorimeter (Hunter Lab) in terms of Hunter L, a, and b values. The Page model was found to be most suitable in describing the drying characteristics of purslane. New parameters developed for the model resulted in a good fit at different temperatures. Color measurement indicated that greenness decreased with an increase in drying air temperature. Typical drying times were 88.41, 138.53, 416.38, and 1371.85 min at 120, 95, 70, and 35°C, respectively.     

Drying Characteristics of Purslane (Portulaca oleraceae L.)

Abstract

Thin layer drying rates of purslane were determined experimentally as a function of temperature with air velocity kept constant at 1.1 m/s and relative humidity below 5%. Thin layer drying data were obtained for purslane at four drying air temperatures (35, 70, 95, and 120°C). Five thin layer-drying models (Henderson and Pabis, exponential, Page, two-term exponential, and Thompson models) were fitted to the drying data. The color of purslane was determined after drying using a spectro-colorimeter (Hunter Lab) in terms of Hunter L, a, and b values. The Page model was found to be most suitable in describing the drying characteristics of purslane. New parameters developed for the model resulted in a good fit at different temperatures. Color measurement indicated that greenness decreased with an increase in drying air temperature. Typical drying times were 88.41, 138.53, 416.38, and 1371.85 min at 120, 95, 70, and 35°C, respectively.     

Effect of the Treatment Temperature on the Surface Drying Set of Sugi Boxed-Heart Square Timber

High-temperature and controlled humidity treatment before drying has proven to be highly effective in preventing surface checks by forming drying sets in the surface layer of boxed-heart square timber in Japan. In this study, we examined the differences of the surface drying sets on sugi timber under different treatment temperatures. As a result, the width of a surface check after drying was much smaller at a treatment temperature of 120°C than at 80°C, and this indicates that the drying set with 120°C treatment would be larger than that with 80°C treatment. Also we observed that treatment temperature had a greater effect on the drying set as the drying advanced.     

Effect of the Treatment Temperature on the Surface Drying Set of Sugi Boxed-Heart Square Timber

High-temperature and controlled humidity treatment before drying has proven to be highly effective in preventing surface checks by forming drying sets in the surface layer of boxed-heart square timber in Japan. In this study, we examined the differences of the surface drying sets on sugi timber under different treatment temperatures. As a result, the width of a surface check after drying was much smaller at a treatment temperature of 120°C than at 80°C, and this indicates that the drying set with 120°C treatment would be larger than that with 80°C treatment. Also we observed that treatment temperature had a greater effect on the drying set as the drying advanced.     

Temperature Changes during Microwave-Vacuum Drying of Sliced Carrots

Abstract

The temperature changes during microwave-vacuum drying of sliced carrots were investigated. Sliced samples were dried to 7–10% moisture content (wet basis) at a wide range of microwave power and vacuum pressure levels. The experiments showed that for sample thickness less than 8 mm, the core temperature of the sample was the same as its surface temperature, with uniform temperature distribution within the sample. However, for sample thickness more than 8 mm, temperature gradient developed along the thickness of the sample. The experiments also showed that, with the decrease of moisture content X _w (dry basis), for samples with thickness ≤ 8 mm, the drying process of sliced carrots experienced three distinct periods: a warming-up period (X _w  = 7.68) without removal of moisture when the product temperature increased linearly with drying time until it reached the corresponding saturation temperature of water in the food at the vacuum pressure; a constant temperature period (2 ≤ X _w  < 7.68) in which most of moisture evaporated and flowed out of the sample efficiently with little resistance; and a heating-up period (X _w  < 2) in which the drying rate decreased and sample temperature increased rapidly. The mathematical models for predicting sliced sample temperature were also developed based on the energy conservation and regression of the experimental date.     

The Quantitative Effect of Drying on the Surface Color Change of Reaction Woods: Spruce Compression Wood (Picea abies L.) and Poplar Tension Wood (Populus nigra L.)

The surface color change of compression wood in spruce (Picea abies L.) and tension wood in poplar (Populus nigra L.) due to drying was investigated using CIE LAB and CIELCh colorimetry techniques. The results showed that the compression wood was lighter, yellower, less red, and more statured in color with a deeper hue after drying. Similar changes were also seen with the tension wood, except that it was less yellow and less statured in the dry condition. The color change (ΔE) of compression wood was found to be more remarkable than that of tension wood. Overall, the difference in the colorimetric parameters between the reaction woods and their corresponding normal woods was less significant after drying.     

Evaluation of the Sorption Equilibrium and Effect of Drying Temperature on the Antioxidant Capacity of the Jaboticaba (Myrciaria cauliflora)

In recent years, interest toward berries has increased (e.g., Myrciaria cauliflora or jaboticaba) because of their high phenolic content (phenolic acids, flavonoids, and anthocyanins) that has been associated with positive effects on consumer health and which play an important role in the antioxidant properties of food. This study analyzed the sorption isotherms, thermodynamic properties of sorption (isosteric heat and Gibbs free energy), and the evolution of the antioxidant capacity during the drying process. The effects of drying temperatures of 40°, 50°C, and 60°C on the antioxidant capacity and thermodynamic properties of sorption were evaluated. The gravimetric static method for sorption isotherm determination over a range of relative humidity levels from 0.10 to 0.90 was used. The sorption isotherms exhibited a Type II behavior, typical for many foods. The Guggenheim, Anderson, and Boer (GAB); Oswin; Peleg; and Lewicki models were used to fit the experimental data, and it was determined that the GAB and Peleg models were most appropriate for describing the sorption curves. The isosteric heat and Gibbs free energy were obtained from the experimental sorption equilibrium. The isosteric heat of adsorption decreased when the moisture content increased, while the Gibbs free energy increased. In addition, the phenolic content and antioxidant capacity increased while drying at 50°C and 60°C, whereas these factors decreased at 40°C. Our results provide the food industry with information concerning the best drying conditions to preserve antioxidant properties.     

Process-Based Drying Temperature and Humidity Integration Control Enhances Drying Kinetics of Apricot Halves

The effects of drying temperature (50, 60, and 70°C) and absolute humidity (65, 90, 115, 140 g/kg at the initial stage) on drying kinetics and color attributes of apricot halves under process-based drying temperature and humidity integration control (PDTHIC) were investigated. Results indicated that appropriate PDTHIC could reduce the drying time by 18.75% compared to the control group. The absolute humidity parameter should be controlled well rather than continuously dehumidify for traditional practices. The moisture effective diffusivity (D_eff) at 70°C presented drastic fluctuations with increasing absolute humidity parameters, calculated using the Weibull distribution model. The activation energy (E_a) of samples treated by continuous dehumidification and PDTHIC were 31.40 and 74.18 kJ/mol, respectively. The variation trend of color parameters was different from the conventional hot air drying probably due to the dehydration mechanism. Observation of the microstructure of the dried samples indicated that the PDTHIC process can enhance the drying rate of apricot through generating a larger pore network compared to continuous dehumidification at the same temperature. The findings of the current work clearly indicated that process-based drying temperature and humidity integration control enhances the drying kinetics of apricot halves, leading to a promising technology for energy savings.     

Comparison of Two Drying Schedules for European Hophornbeam (Ostrya carpinifolia Scop.) Lumber

Two types of conventional kiln-drying schedules (mild and harsh) based on moisture content (MC) were compared with regard to time, drying quality, and energy cost. The results were evaluated according to the classification of the European Drying Group. Proper drying periods of mild and harsh schedules were found to be 550 and 514 h, respectively. Evaluations in terms of drying quality indicated that better results were achieved with the mild schedule, especially when comparing drying defects and final MC. From an energy efficiency point of view, the harsh schedule, by saving 36 h of drying time, reduced electricity by 594 KWh and was therefore found to be $65 more profitable in this trial.     

Comparison of Two Drying Schedules for European Hophornbeam (Ostrya carpinifolia Scop.) Lumber

Two types of conventional kiln-drying schedules (mild and harsh) based on moisture content (MC) were compared with regard to time, drying quality, and energy cost. The results were evaluated according to the classification of the European Drying Group. Proper drying periods of mild and harsh schedules were found to be 550 and 514 h, respectively. Evaluations in terms of drying quality indicated that better results were achieved with the mild schedule, especially when comparing drying defects and final MC. From an energy efficiency point of view, the harsh schedule, by saving 36 h of drying time, reduced electricity by 594 KWh and was therefore found to be $65 more profitable in this trial.     

Influence of Temperature and Air Velocity on Drying Time and Quality Parameters of Pistachio (Pistacia vera L.)

Abstract

Drying is one of the important steps in pistachio processing. In this step kernel moisture content is decreased from 50 to less than 5% (d.b.) which will result in suitable condition for storage. Study of effective parameters in pistachio drying is important since these parameters influence drying time and kernel quality. In this research, a mono layer of pistachios was dried at three different temperatures (60, 75, and 90°C), and three levels of drying air velocity (1.5, 2, and 2.5 m/s). Changes of drying time, protein, fat and peroxide value were investigated for two common Iranian pistachio varieties Kalehghouchi and Fandoghi. Sensory tests were also used to check flavor of pistachios dried at the three temperature levels (60, 75, and 90°C). Statistical analysis of the data indicated that increasing the temperature to 90°C reduced drying time down by about 37% and caused a change in pistachio flavour. Taste tests indicated a consumer preference for pistachios dried at 75°C. If the air velocity is increased from 1.5 to 2.5 m/s, drying time reduces about 10 percent. Changes in temperature and air velocity have no significant effects on protein and fat content of pistachios, but if temperature reaches 90°C, peroxide value will increase to 0.55 meq/kg, which is still within the permissible limit for processed pistachios.     

Influence of Temperature and Air Velocity on Drying Time and Quality Parameters of Pistachio (Pistacia vera L.)

Drying is one of the important steps in pistachio processing. In this step kernel moisture content is decreased from 50 to less than 5% (d.b.) which will result in suitable condition for storage. Study of effective parameters in pistachio drying is important since these parameters influence drying time and kernel quality. In this research, a mono layer of pistachios was dried at three different temperatures (60, 75, and 90°C), and three levels of drying air velocity (1.5, 2, and 2.5 m/s). Changes of drying time, protein, fat and peroxide value were investigated for two common Iranian pistachio varieties Kalehghouchi and Fandoghi. Sensory tests were also used to check flavor of pistachios dried at the three temperature levels (60, 75, and 90°C). Statistical analysis of the data indicated that increasing the temperature to 90°C reduced drying time down by about 37% and caused a change in pistachio flavour. Taste tests indicated a consumer preference for pistachios dried at 75°C. If the air velocity is increased from 1.5 to 2.5 m/s, drying time reduces about 10 percent. Changes in temperature and air velocity have no significant effects on protein and fat content of pistachios, but if temperature reaches 90°C, peroxide value will increase to 0.55 meq/kg, which is still within the permissible limit for processed pistachios.     

Antioxidant activity of pea bean (Phaseolus vulgaris L.) extract

Antioxidative activity of pea bean (Phaseolus vulgaris L.) extract was evaluated by using a linoleic acid system, and the methanol extract exhibited strong antioxidative activity as measured by the thiocyanate method. The crude methanol extract was partitioned between then-butanol phase (BP) and the water phase (WP). Then, the antioxidative activity of the BP and the WP was determined by using a linoleic acid system. The WP showed strong antioxidative activity, while BP showed only weak activity as measured by the thiocyanate method. Next, the synergistic antioxidative action of WP with α-tocopherol was examined by using linoleic acid and liposome systems. The WP had a synergistic effect with α-tocopherol in both the food model and liposome systems. For purification and isolation of the antioxidative substances of the pea bean, preparative high-performance liquid chromatography was carried out with an octadecylsilyl column. Five fractions were collected, and antioxidative activity was determined in a linoleic acid system. Although fraction 1 had strong activity by the thiocyanate method, the purification of this active fraction was difficult; therefore, the partly characterized active fraction was investigated. The contents of total phenolics and sugars were 0.31±0.01 mg/g of fraction 1 and 406.1±0.1 mg/g, respectively. The ninhydrin chromogenic reaction was positive, and the ultraviolet absorption spectral λ max value in distilled water was 264.0 nm, indicating that the water-soluble antioxidative components from pea bean may be a new type of antioxidant. Isolation and identification are currently being investigated.     

Ultrasonically Enhanced Osmotic Pretreatment of Sea Cucumber Prior to Microwave Freeze Drying

A new pretreatment method involving use of ultrasound prior to microwave freeze drying of sea cucumber was examined experimentally. It was observed that ultrasound-assisted osmotic pretreatment can reduce by about 2 h the time needed for microwave freeze drying. An optimization study using response surface analysis was carried out to determine the optimal operating parameters to minimize drying time while maximizing quality.     

A Comparative Study of Four Drying Methods on Drying Time and Quality Characteristics of Stem Lettuce Slices (Lactuca sativa L.)

This article presents experimental results and analysis of four drying methods, viz. hot air drying (AD), hot air-assisted radio frequency drying (ARFD), infrared drying (IRD), and microwave-assisted hot air drying (MAD), on color, microstructure, density, rehydration capacity, and texture after rehydration of stem lettuce slices (Lactuca sativa L.). The drying time required for these drying protocols was also compared. These four drying tests were conducted at fixed air temperature (60°C) and velocity (1 m/s), as well as identical sample load (300 g), bed depth (20 mm), and the power level for ARFD, IRD, and MAD, which was fixed at 4 W/g. The results showed that the drying time required for stem lettuce slices using ARFD was the shortest (120 min), followed by MAD (140 min) and IRD (180 min); AD required the longest time (360 min). Notably, ARFD yielded uniform drying and the quality of the dried samples using ARFD was also the best among these four drying methods.     

Optimizing Drying Conditions for Vacuum-Assisted Microwave Drying of Green Peas (Pisum sativum L.)

Green peas were dried in a vacuum-assisted microwave drying system. The effects of microwave power levels (100–300 W) and system vacuum (50–400 mm Hg) on drying parameters (viz. drying efficiency and drying time) and some quality attributes (viz. linear shrinkage, apparent density, green color, rehydration, and sensory attributes) of dehydrated peas were analyzed by means of response surface methodology. A face-centered central composite design was used to develop models for the responses. Analysis of variance showed that a second-order polynomial model predicted well the experimental data. The system microwave power level strongly affected quality attributes of dehydrated peas and drying parameters. A higher vacuum during drying resulted in a better quality product. Microwave power of 237.31 W and a 360.22 mm Hg vaccum were found to be optimum drying conditions for vacuum-assisted microwave drying of green peas.     

Influence of Drying Temperature and Harvesting Season on Phenolic Content and Antioxidant and Antiproliferative Activities of Olive (Olea europaea) Leaf Extracts

Interest in plant compounds has increased, given recent evidence regarding their role in human health due to their pleiotropic effects. For example, plant bioactive compounds present in food products, including polyphenols, are associated with preventive effects in various diseases, such as cancer or inflammation. Breast and colorectal cancers are among the most commonly diagnosed cancers globally. Although appreciable advances have been made in treatments, new therapeutic approaches are still needed. Thus, in this study, up to 28 olive leaf extracts were obtained during different seasons and using different drying temperatures. The influence of these conditions on total polyphenolic content (measured using Folin–Ciocalteu assays), antioxidant activity (using Trolox Equivalent Antioxidant Capacity and Ferric Reducing Ability of Plasma assays) and antiproliferative capacity (using 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide, MTT assays) was tested in breast and colorectal cancer cells. Increased phenolic composition and antioxidant and antiproliferative capacity are noted in the extracts obtained from leaves harvested in autumn, followed by summer, spring and winter. Regarding drying conditions, although there is not a general trend, conditions using the highest temperatures lead to the optimal phenolic content and antioxidant and antiproliferative activities in most cases. These results confirm previously published studies and provide evidence in support of the influence of both harvesting and drying conditions on the biological activity of olive leaf extracts.