Investigation on Convective Drying of Mixtures of Sewage Sludge and Sawdust in a Fixed Bed

This work is part of a project aiming to develop a renewable fuel for gasification purposes, through convective drying of sludge/wood mixtures. The first step consists of characterizing the behavior of sawdust/sludge mixtures during the application of convective drying. The influence of the mixing step (no mixing versus 30 s at 40 rpm), as well as the sawdust : sludge ratio (1:9, 2:8, 3:7, and 4:6 on a dry basis) and the effect of drying temperature (50, 80, and 110°C) were investigated. In this study, X-ray tomography, a noninvasive imaging technique, is used to assess changes in the volume, void, and exchange surface at the beginning and the end of the drying process. Results first confirm the importance of the mixing step on the drying behavior: the drying rate of the mixed sludge is lower than that of the original sludge. Nevertheless, the addition of sawdust is shown to have a positive impact on the drying process from a mass ratio of 2:8, with drying rates higher than that of the original sludge. With increasing amounts of sawdust, the initial and final bed volumes, initial and final total exchange surfaces, and initial void fraction increase linearly, but the bed volume shrinkage and final void fraction decrease linearly.     

Modeling of Convective Drying of Sawdust Using a Reaction Engineering Approach

Drying as a simultaneous heat and mass transfer process can be modeled via the reaction engineering approach (REA) where the apparent activation energy of the material is established and related to its moisture content during drying. This relationship is unique as the normalized activation energies can be collapsed into a single equation irrespective of the drying conditions and dryer types. Here, REA was applied to model the drying kinetics of sawdust using convective hot air in a laboratory setup. The normalized (relative) activation energy curve generated from one drying experiment was employed to predict the drying kinetics and temperature profiles. The REA can describe well the convective drying kinetics of sawdust, and major physics of the drying process was captured well with this technique.     

Simultaneous Heat and Mass Transfer in Shrinkable Apple Slab During Drying

The goal of the study was to determine the influence of drying shrinkage on the kinetics of convection apple slab drying. The arbitrary Lagrange-Eulerian (ALE) method was used to enter a problem with moving boundaries. It was found that drying shrinkage had a major influence on the both simulated temperature and water content in the material. The lower the moisture content in particles during drying, the more pronounced the effect of shrinkage on simulation of heat and mass transfer. It was found that application of the arbitrary Lagrange-Eulerian method for shrinkage modeling leads to a relatively simple mathematical model of the drying kinetics of shrinkable materials.     

Simultaneous Heat and Mass Transfer in Shrinkable Apple Slab During Drying

The goal of the study was to determine the influence of drying shrinkage on the kinetics of convection apple slab drying. The arbitrary Lagrange-Eulerian (ALE) method was used to enter a problem with moving boundaries. It was found that drying shrinkage had a major influence on the both simulated temperature and water content in the material. The lower the moisture content in particles during drying, the more pronounced the effect of shrinkage on simulation of heat and mass transfer. It was found that application of the arbitrary Lagrange-Eulerian method for shrinkage modeling leads to a relatively simple mathematical model of the drying kinetics of shrinkable materials.     

Dimensionless Formulation of Convective Heat Transfer in Fry‐Drying of Sewage Sludge

Fry‐drying is an alternative for heat and mass transfer intensification. The process reuses waste oil as a heating medium for drying by contact with the wet sludge. At the end of the process, a stable derived fuel is obtained, a granular solid composed of the dried indigenous sewage solid and the impregnated oil. The fry‐dried sludge is storable and transportable without any pathogen elements. Knowledge about heat and mass transfer rates during the frying process is essential in order to assess the quality of the final product such as calorific value, oil uptake, porosity changes, etc. The heat transfer properties including transfer by free convection between the solid and the frying oil are fundamental for the process design and manufacturing of the fry‐dried product. The convective heat coefficient by temperature measurement and overall energy balance calculation is determined. The heat flux is calculated from the fry‐drying kinetics including moisture loss and oil intake kinetics. Various hydrodynamic regimes for convective heat transfer during the frying process are discussed (non‐boiling, boiling, and low‐boiling regime). A dimensionless formulation for estimating the convective transfer is proposed.     

Mass Transfer Coefficient for Drying of Moist Particulate in a Bubbling Fluidized Bed

Experiments on drying of moist particles by ambient air were carried out to measure the mass transfer coefficient in a bubbling fluidized bed. Fine glass beads of mean diameter 125 μm were used as the bed material. Throughout the drying process, the dynamic material distribution was recorded by electrical capacitance tomography (ECT) and the exit air condition was recorded by a temperature/humidity probe. The ECT data were used to obtain qualitative and quantitative information on the bubble characteristics. The exit air moisture content was used to determine the water content in the bed. The measured overall mass transfer coefficient was in the range of 0.0145–0.021 m/s. A simple model based on the available correlations for bubble‐cloud and cloud‐dense interchange (two‐region model) was used to predict the overall mass transfer coefficient. Comparison between the measured and predicted mass transfer coefficient have shown reasonable agreement. The results were also used to determine the relative importance of the two transfer regions.     

Liming Pretreatment Reduces Sludge Build-Up on the Dryer Wall during Thermal Drying

In the course of sludge thermal drying, the sludge that sticks to the heated surfaces of drying equipment causes deterioration of drying efficiency and safety. The ability of alkaline pretreatment to reduce sludge build-up on dryer walls during convective drying processes was investigated. The sludge build-up was measured as the residual mass on an iron plate after parts of the sludge were scraped off the plate; the device used simulated the scraping process in drying equipment. The results showed that the sludge build-up on the plate increased at first and then decreased as the sludge water content decreased during thermal drying. The maximum amount of sludge build-up occurred when the sludge water content was about 55–60%. Liming pretreatment enhanced sludge cohesion, hydrolyzed adhesive organic substances, increased the inorganic mineral content of the sludge and, accordingly, reduced sludge build-up. When the dose of Ca(OH)₂ was 5% of dry solids (5% DS), the sludge build-up was almost negligible and the average drying rate improved by about 30%. CaO pretreatment was also very effective in preventing sludge build-up, but its effect on the sludge drying rate was not obvious at the same dosage. Compared with Ca(OH)₂ and CaO, NaOH did not reduce sludge build-up effectively or improve the sludge drying rate.     

Experimental and Numerical Investigation of the Heat and Mass Transfer for Cut Tobacco During Two-Stage Convective Drying

In this article, a two-stage convective drying strategy was presented for dehydration of flue-cured tobacco. In order to develop the multistage drying method of tobacco, two-stage drying as well as traditional single-stage drying of cut tobacco was experimentally evaluated and accurately simulated by proposed heat and mass transfer models. The experiments were performed in a dual fixed bed dryer. Different air temperature combinations of 120°C/90°C, 110°C/80°C, and 100°C/70°C were employed during two-stage drying. The drying rate and temperature variations of cut tobacco were investigated. The results showed that the average drying rates during two-stage drying were nearly 50% higher than those obtained from lower-temperature single-stage drying. On the other hand, the two-stage drying method, which used high air temperature for the early period and low temperature for the late period, could reduce the exposure of tobacco to high temperature due to the low final temperature of the dried sample. The temperature and moisture evolution of cut tobacco at different air temperature combinations were consistent with simulation results by developed heat and mass transfer models. This indicated that the models had a good prediction precision for two-stage drying of cut tobacco. The model predictions can be useful for the design of a feasible two-stage drying process for flue-cured tobacco.     

Convective Drying of Wastewater Sludge: Introduction of Shrinkage Effect in Mathematical Modeling

Drying of two kinds of wastewater sludge was studied. The first part was an experimental work done in a discontinuous cross-flow convective dryer using 1 kg of wet material extruded in 12-mm-diameter cylinders. The results show the influence of drying air temperature for both sludges. The second part consisted of developing a drying model in order to identify the internal diffusion coefficient and the convective mass transfer coefficient from the experimental data. A comparison between fitted drying curves, well represented by Newton's model, and the analytical solutions of the equation of diffusion, applied to a finite cylinder, was made. Variations in the physical parameters, such as the mass, density, and volume of the dried product, were calculated. This allowed us to confirm that shrinkage, which is an important parameter during wastewater sludge drying, must be taken into account. The results showed that both the internal diffusion coefficient and convective mass transfer coefficient were affected by the air temperature and the origin of the sludge. The values of the diffusion coefficient changed from 42.35 × 10^?9 m² · s^?1 at 160°C to 32.49 × 10^?9 m² · s^?1 at 122°C for sludge A and from 33.40 × 10^?9 m² · s^?1 at 140°C to 28.45 × 10^?9 m² · s^?1 at 120°C for sludge B. The convective mass transfer coefficient changed from 4.52 × 10^?7 m · s^?1 at 158°C to 3.33 × 10^?7 m · s^?1 at 122°C for sludge A and from 3.44 × 10^?7 m · s^?1 at 140°C to 2.84 × 10^?7 m² · s^?1 at 120°C for sludge B. The temperature dependency of the two coefficients was expressed using an Arrhenius-type equation and related parameters were deduced. Finally, the study showed that neglecting shrinkage phenomena resulted in an overestimation that can attain and exceed 30% for the two coefficients.     

Heat and Mass Transfer in Fry Drying of Wood

This article describes the coupled heat and mass (water, oil) transport phenomena in parallelepiped samples of beech (Fagus sylvatica) fried in peanut oil between 120 and 180°C. The aim was to evaluate the suitability of simultaneous fry drying and oil impregnation as an alternative wood treatment process. Water loss and oil impregnation were continuously assessed during the process. Temperature and pressure were measured at the center of the sample. The water in the peripheral layers of the wood vaporizes at atmospheric pressure. The water at the center of the wood vaporizes at overpressures of the order of 2.8 × 10⁵ Pa. High fluxes of water were recorded of about 0.006 kg/(m²s). The impregnated oil can amount to 20% of the mass of the removed water.     

Heat and Mass Transfer in Fry Drying of Wood

This article describes the coupled heat and mass (water, oil) transport phenomena in parallelepiped samples of beech (Fagus sylvatica) fried in peanut oil between 120 and 180°C. The aim was to evaluate the suitability of simultaneous fry drying and oil impregnation as an alternative wood treatment process. Water loss and oil impregnation were continuously assessed during the process. Temperature and pressure were measured at the center of the sample. The water in the peripheral layers of the wood vaporizes at atmospheric pressure. The water at the center of the wood vaporizes at overpressures of the order of 2.8 × 10⁵ Pa. High fluxes of water were recorded of about 0.006 kg/(m²s). The impregnated oil can amount to 20% of the mass of the removed water.     

Analysis of Fluidized Bed Drying Kinetics on the Basis of Interphase Mass Transfer Coefficient

A particular way to define fluidized bed drying kinetics on the basis of interphase mass transfer coefficient and the conception of general kinetic curve has been described. The presented method, which allows for minimization of laboratory tests, has been checked experimentally. The method for calculating of mass transfer interphase coefficient in the constant rate period of fluidized bed drying based on Kunii and Levenspiel bubbling bed model is shown.     

Analysis of Fluidized Bed Drying Kinetics on the Basis of Interphase Mass Transfer Coefficient

A particular way to define fluidized bed drying kinetics on the basis of interphase mass transfer coefficient and the conception of general kinetic curve has been described. The presented method, which allows for minimization of laboratory tests, has been checked experimentally. The method for calculating of mass transfer interphase coefficient in the constant rate period of fluidized bed drying based on Kunii and Levenspiel bubbling bed model is shown.     

Numerical Study on Moisture Transfer in Ultrasound-Assisted Convective Drying Process of Sludge

A coupled heat and moisture transfer model for ultrasound-assisted convective drying process of sludge was established. In this model, the permeable flow caused by acoustic pressure gradient in sludge was considered. The pore structure variety in sludge with ultrasonic irradiation was microscopically studied, and the pore size distribution of sludge was described by fractal geometry. Based on the fractal characterization, the physical properties of sludge including permeability, porosity, and tortuosity factor were determined, and the effective moisture diffusion coefficient of sludge under ultrasonic irradiation was also derived considering the effects of ultrasonic excitation energy and thermal effect on migration rate of water molecule. The effects of ultrasonic energy density and convective air temperature on convective drying process of sludge were numerically analyzed. The results showed that the ultrasonic irradiation changes the pore size distribution in sludge, the sludge flocs are dispersed, and the connectivity of pore structure is improved. Ultrasonic treatment is favorable to accelerating the moisture transport in the convective drying process of sludge, and the ultrasonic influence on moisture transport in sludge intensifies gradually with the increase of acoustic energy density from 0.2 to 0.6 W/ml. Furthermore, it can be also found that the enhancement effect of ultrasound on the average drying rate of sludge is more obvious at the connective air temperature of 65°C than that at 40°C under the uniform acoustic energy density and air velocity of 1.5 m/s.     

A Study of Coupled Heat and Mass Transfer in Composite Food Products during Convective Drying

A two-dimensional liquid diffusion model was developed to predict the variation of transient moisture content and temperature distribution within model composite food products. Rectangular-shaped potato and apple slices were used to form the model composite samples for experimental tests. To verify the predictions of the theoretical model, a series of experiments were conducted on the model composite samples using a heat pump-assisted convective dryer. Effects of using different adhesives to hold the two slices forming the composite products, flipping of the products at selected intervals of time and variation of individual slice thickness were investigated both experimentally and numerically. Predictions of the numerical model are in good agreement with the experimental results.     

Breakage and Mass Transfer Models During Drying of Rough Rice

A breakage model was investigated for thin-layer drying of rough rice. The breakage model developed can predict the percentage of head rice (E/E_o) as an exponential function of the grain moisture. Experimental data of the rice moisture content during drying were fitted with a theoretical model of the drying process to obtain the parameters. Experimental data of percentage head rice and moisture content were fitted to obtain the parameters of breakage model. Both functions were used together to obtain a drying-breakage model. This model allows us to predict the drying time required to achieve a rice moisture content desired and to estimate the head rice yield percentage for this moisture content.     

石灰调质污泥恒温干燥特性及动力学模型研究

对添加石灰的市政污泥进行恒温干燥实验,研究在不同的石灰添加量和不同的温度条件下污泥干燥特性、有效水分扩散系数和干燥活化能。结果表明:高温干燥时,石灰添加量的增加对平均干燥速率以及有效扩散系数的提高影响显著,低温干燥时影响不显著;石灰的添加可以降低干燥活化能;基于Modified Page模型建立的通用干燥模型能准确地描述石灰调质污泥的干燥特性;模型方程预测值和实验值吻合,均方根误差为0.32%。     

Modeling and Numerical Analysis of an Atypical Convective Coal Drying Process

This work presents modeling and numerical simulation of batch convective coal drying in a deep packed bed after a high-pressure steam treatment (a part of the Fleissner coal drying process). The process is atypical, because ambient air is used to dry and cool hot particles, while usually, e.g., in the deep packed bed drying of biomaterials, hot air is contacting cold particles. Product-specific data (intraparticle mass transfer, gas-solids moisture equilibrium) for coal (here lignite) are taken over from literature. Available data on coal drying in packed beds of medium height are used for model validation. Then, the model is applied to the considered industrial process. The design point of the process is critically reviewed, and alternatives are developed by systematically simulating the influence of inlet air conditions (temperature, humidity, flow-rate) and coal particle size. This type of analysis is necessary for efficiently scheduling plant dryers, since coal particle size may change, and air inlet temperature and humidity are changing with the ambient conditions.     

Convective drying behavior of sawdust-sludge mixtures in a fixed bed

This work aims at comparing the temporal evolution of 3D characteristics of the sample bed as well as the drying mechanism of sewage sludge and sawdust-sludge mixtures during the drying process. The first step are characterizing the drying behavior of sawdust-sludge mixtures during the convective drying. The influences of the mixing step (no mixing against 30 s at 40 r/min) and of the mass fractions of sawdust (10%, 20%, 30%, and 40% on a dry basis) have been investigated. X-ray tomography, a non-invasive imaging technique, was used to assess changes in the volume and total exchange surface during the drying process. Drying experiment results show that sawdust addition has a positive impact on the drying process from a mass fraction of sawdust of 20%. The X-ray tomography experiment results show that the volume and total exchange surface of the sample bed both increase with increasing amounts of sawdust during the entire drying process. Moreover, a linear decrease of both the total exchange surface and volume with the decreased normalized moisture content is observed for sludges, while a plateau is reached after a linear phase for sawdust-sludge mixtures. As expected for sludges, the drying rate decreases nearly linearly with the decreased total exchange surface during the entire drying process. However, for the sawdust-sludge mixtures, at first the drying rate decreases nearly linearly with the decreased total exchange surface, and then the total exchange surface does not change but the drying rate still decreases until it reaches zero. These promising results open the way to new management ways, especially for very pasty sludge.