共查询到20条相似文献,搜索用时 187 毫秒
1.
介质(Ag/AgI)镀层空芯玻璃光纤是一种较好的传输红外激光的柔性光纤材料.采用液相化学沉积法成功地制备了内径分别为1.0、0.53、0.32mm,长度为1.5m的介质(Ag/AgI)镀层玻璃空芯光纤.利用傅里叶红外光谱仪和 LJL-35A CO2激光器分别测试了介质(Ag/AgI)镀层玻璃空芯光纤的传输损耗,测试结果表明:介质(Ag/AgI)镀层空芯玻璃光纤在2.5~20μm波长范围内有较低的损耗值;随着光纤内径(α)的增大,空芯光纤的传输损耗(α)降低,这与Migagi理论(α ∝1/α3)相符合.另外,由于光纤的注入端头发热致使介质(Ag/AgI)镀层空芯玻璃光纤的传输损耗随注入功率的增加而增大. 相似文献
2.
利用分步法高温固相反应合成Cd_3Al_2Ge_3O_(12)基质和Cd_3Al_2Ge_3O_(12):Mn石榴石荧光粉,给出立方晶格常数,研究材料的阴极射线发光性质。Cd_3Al_2Ge_3O_(12):Mn石榴石具有较长的黄色余辉特性,是一种抗闪烁材料。微量过渡金属杂质对锗酸盐石榴石发光产生严重猝灭作用。 相似文献
3.
本文采用空气氛化Fe(CO_3)_x(OH)_(2(1-x))悬浮液体系,控制体系的pH和掺入适量的钇元素,合成出纳米级铁黄γ-FeOOH微晶。由DTA-TG和XRD分析得出,由γ-FeOOH直接脱水得到的γ-Fe_2O_3样品,具有很好的热稳定性,其γ-α相变温度可达725℃,且粒径为纳米级,并具有很好的气敏灵敏度和选择性。600℃烧结的气敏元件,对液化石油气(LPG)的灵敏度S大于70;而在700℃下烧结的元件,对C_2H_2灵敏度S大于40;它们均对选定测试的气体CO、H_2、汽油(Petrol)。C_2H_2和LPG有很好的选择性。 相似文献
4.
5.
6.
用电弧等离子体法制各纳米α-Fe_2O_3并研究其气敏特性,结果表明,在没有掺杂的情况下,纳米α-Fe_2O_3就具有较好的气敏特性。其原因是纳米粒子具有较大的比表面积和较高的晶界比例,从而导致对气体的吸附能力和扩散能力增强。本文用原位XRD方法研究了纳米α-Fe_2O_3的气敏机理,结果表明,在还原性气氛和加热条件下,α-Fe_2O_3并没有被还原成Fe_3O_4,其气敏机理主要是表面效应控制型。 相似文献
7.
8.
9.
10.
11.
Abhishek K. Kothari Erkan Konca Brian W. Sheldon Kengqing Jian Hao Li Zhenhai Xia Wangyang Ni Robert Hurt 《Journal of Materials Science》2009,44(22):6020-6027
Anodic alumina was reinforced with three types of carbon nanofibers differing in the orientation of their graphene structure—perpendicular
to the fiber axis, and parallel to the fiber axis both with dense core and hollow core (i.e., nanotubes). This study was designed
to identify potential toughening and damage tolerant mechanisms in these nanoscale fiber-reinforced composite coatings. The
dense carbon fibers improved contact damage resistance and reduced frictional resistance in sliding contacts. The hollow core
reinforcements were much more promising for improving the fracture toughness of the composite coatings. 相似文献
12.
Pyramidal lattice sandwich structures with hollow composite trusses were fabricated using a thermal expansion molding approach. Composite lattice structures with three relative densities were fabricated with two fiber architectures and the out-of-plane compression properties were measured and compared. Lattice cores with a fraction of carbon fibers circumferentially wound around the hollow trusses (Variant 2) exhibited superior mechanical properties compared with similar structures comprised of unidirectional fibers (Variant 1). The out-of-plane compressive properties of composite pyramidal lattice structures in Variant 2 were well-matched by analytical predictions. Unusual strain hardening behavior was observed in the plateau region for Variant 2, and the energy absorption capabilities were measured and compared with the similarly constructed silicone rubber–core truss pyramidal lattice structures (Variant 3). The energy absorption per unit mass of selected hollow truss composite lattice structures reported here surpassed that of both hybrid truss counterparts (Variant 3) and hollow truss metallic lattice structures. 相似文献
13.
几种中空纤维膜对氧气,环氧丙烷透过性的比较 总被引:1,自引:0,他引:1
为选定适合气-固-液三相生物反应过程膜反应器中的膜材料,采用氧电极测试了几各收集到的聚砜、聚丙烯及聚氟乙烯中空纤维膜对氧气的通透性,其中的聚丙烯中空纤维适于做膜生物反应器中的透气膜,同时还测定了聚砚、聚偏氟乙和聚丙烯腈地水溶液中环氧丙烷的通透性,在实验条件下它们之间的差异不大。 相似文献
14.
A new type of lightweight sandwich panels consisting of vertically aligned hollow Al–Si alloy tubes as core construction and carbon fiber composite face sheets was designed. The hollow Al–Si alloy tubes were fabricated using precision casting and were bonded to the face sheets using an epoxy adhesive. The out-of-plane compression (i.e. core crushing), in-plane compression, and three-point bending response of the panels were tested until failure. The hollow Ai–Si alloy tubes core configuration show superior specific strength under crushing compared to common metallic and stochastic foam cores. Under in-plane compression and three-point bending, the buckling of face sheets and debonding of hollow cores from the face sheets were observed. Simple analytical relationships based on the concepts of mechanics of materials were provided for the compression tests, which estimate the sandwich panels’ strength with high fidelity. For three-point bending, detailed finite element analysis was used to model the response and initial failure of the sandwich panels. 相似文献
15.
采用相转化/烧结技术制备了致密的Bi1.5Y0.3Sm0.2O3-La0.8Sr0.2MnO3–d双相复合陶瓷中空纤维膜. 所得的中空纤维膜具有非对称结构, 靠近膜管内表面部分是指状孔结构, 而靠近膜管外表面则是非常致密的结构. 中空纤维膜的内部尾端的氧气含量与膜管内外的氧分压、纤维膜的长度等有很大的关系. 由于随着氧气的渗透, 膜管内的氧分压沿轴向是增大的, 可以将膜管均分为n段, 采用活塞式流动模型结合Wagner氧渗透理论对双相复合中空纤维膜的氧渗透过程进行了模拟, 模拟结果和实测的相符合, 对于估算膜组件的氧气生产能力具有很好的指导意义. 相似文献
16.
A zirconia hollow fiber membrane in the macrorange was for the first time successfully synthesized via a template method coupled with a sol-gel process. A polypropylene hollow fiber was employed as the template. The preparation procedure includes repeated impregnation of the template in the proper zirconia sol precursor, and calcination to burn off the template, producing the zirconia hollow fiber. The resulting hollow fiber membrane is almost identical to its template in terms of morphology, exhibiting a hollow core structure. In addition to that, it has a bimodal porous substructure that is different from its template, narrowly distributed nanoskeleton pores, and uniform textural pores or throughpores. The wall thickness and substructures can be conveniently controlled by the synthetic conditions and postheat treatment. Moreover, the thus-prepared zirconia hollow fiber was applied for the microextraction and concentration of a nerve agent degradation product followed by liquid chromatography-mass spectrometric analysis. Since the zirconia fiber exists as an individual device and is directly usable for extracting, handling is more convenient than, for example, an adsorbent in powder form that needs to be coated on a rod for the extraction process. In addition, it is easily prepared and is superior to the monolithic material in this sense. Pinacolyl methylphosphonic acid, one degradation product of organophosphorus nerve agent (soman), was used as the model analyte. Zirconia hollow fiber was demonstrated to be a highly selective adsorbent for the phosphonic acid-containing compounds with high sensitivity. Limit of detection was as low as 0.07 ng/mL (0.39 nM). 相似文献
17.
Zhang S Liu T Chen L Ren M Zhang B Wang Z Wang Y 《Journal of materials science. Materials in medicine》2012,23(8):2001-2011
A bioartificial liver bioreactor requires a bifunctional hollow fiber that is hemocompatible on one side and cytocompatible on the other side. In this study, we developed a single-layer skin polyethersulfone (PES) hollow fiber with smooth inner surface and rough/porous outer surface for an artificial liver bioreactor. The hemocompatibility of the inner surface was evaluated by hemolysis, complement activation and clotting time. The cytocompatibility of the outer surface with HepG2 cells was examined by morphology, proliferation and liver-specific functions. The inner surface of the PES hollow fiber exhibited lower hemolysis and complement activation than cellulose acetate (CA) hollow fiber and a prolonged blood coagulation time. HepG2 cells readily adhered to the outer surfaces of the PES hollow fibers, and proliferated to form multicellular aggregates with time. Furthermore, HepG2 cells cultured on the outer surface of the PES hollow fiber exhibited higher proliferation ability and liver-specific functions than those grown on the CA hollow fiber. These results suggest that the single-layer skin PES hollow fiber is a bifunctional hollow fiber with good hemocompatibility on the inner side and cytocompatibility on the outer side. Thus, porous and single-layer skin PES hollow fibers may have potential as materials for an artificial liver bioreactor. 相似文献
18.
The fiber-optic delivery of sparks in gases is challenging as the output beam must be refocused to high intensity (approximately 200 GW/cm(2) for nanosecond pulses). Analysis suggests the use of coated hollow core fibers, fiber lasers, and photonic crystal fibers (PCFs). We study the effects of launch conditions and bending for 2 m long coated hollow fibers and find an optimum launch f# of approximately 55 allowing spark formation with approximately 98% reliability for bends up to a radius of curvature of 1.5 m in atmospheric pressure air. Spark formation using the output of a pulsed fiber laser is described, and delivery of 0.55 mJ pulses through PCFs is shown. 相似文献
19.
海藻酸钙水凝胶空心纤维在药物传递、组织工程等领域具有潜在的应用价值。但传统的纤维制备方法,如静电纺丝或模具法等,很难或无法制备海藻酸钙空心纤维。本研究首先采用自制的两相微流控装置,连续制备出形貌均一稳定的海藻酸钙空心纤维,并通过显微镜和扫描电子显微镜(SEM)对其空心结构进行了表征。然后考察了装置中内相毛细管尖端管径、内外相流体流速比以及氯化钙浓度对空心纤维内外径尺寸和厚度的影响,结果表明,空心纤维的尺寸在一定范围内可以进行调控。最后将这种空心纤维应用于封装和培养L929成纤维细胞,结果表明,成纤维细胞存活率较高,并且有沿着空心纤维内壁成直线生长的趋势。这种方法为纤维状细胞的培养提供了一种思路。 相似文献
20.
膜蒸馏海水淡化用疏水性钇稳定氧化锆中空纤维膜的制备与表征 总被引:1,自引:0,他引:1
采用相转化/高温烧结技术方法制备了多孔钇稳定氧化锆(YSZ)中空纤维膜, 中空纤维膜的外径1.92 mm, 壁厚为0.21 mm。SEM分析表明: 纤维膜为典型的三明治结构, 靠近膜内外表面为指状孔, 中间区域为海绵状层。采用阿基米德法测得其孔隙率为54%。用泡点法测得其平均孔径为0.56 μm。通过表面接枝氟硅烷将其亲水性的表面改变为疏水性。真空式膜蒸馏实验表明YSZ中空纤维膜具有优异的盐水淡化性能。当膜的外侧与温度为80℃、浓度为4wt%的循环盐水接触, 膜的内侧用真空泵抽至4×103 Pa时, 膜的水渗透通量高达48.3 L/(m2•h), 脱盐率大于99.7%。 相似文献