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重点分析了王河煤矿高硫无烟煤的煤质特征、可选性及降灰脱硫的可行性。研究表明:简单地利用现有的物理分选方法很难将该矿区高硫无烟煤精煤硫分降到1%以下,而且精煤理论产率很低;如果将精煤硫分控制在1.2%~1.3%,并采用配煤等技术,可使精煤产率达到一个相对合理的水平;可以从高硫煤洗矸中选出硫精矿,实现资源的综合利用;也可考虑发展煤化工项目。 相似文献
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高硫煤中形态硫的热解迁移特性 总被引:1,自引:0,他引:1
对西北地区石炭纪高硫煤进行热解实验,考察了热解温度(200℃~1 000℃)和热解停留时间(20min~100min)对煤中形态硫的迁移特性的影响,并通过FTIR分析了热解过程中半焦的结构变化情况.研究表明,高硫煤中全硫随热解温度的升高先减小后增大,在600℃时达到最低;硫酸盐硫的含量较低,维持在0%~0.5%之间;硫化铁硫随着热解温度的升高逐渐减小;有机硫随热解温度的升高先减小后增大,在500℃时达到最低.无机硫脱除率高于有机硫脱除率.煤热解过程中氧和硫等杂原子官能团在半焦中不断减弱. 相似文献
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为了节约我国稀缺的炼焦煤资源和提高经济效益,从而使高硫煤作为炼焦配煤的掺合料成为可能,采用理论推理和实验对比的方法,进行了高硫煤的炼焦硫分的转化实验和不同有机硫含量配比实验。结果表明,高硫煤中富含有机硫容易出低硫焦煤,无机硫中黄铁矿在高温分解时会在煤的有机质作用下无机硫向有机硫的转化。瘦煤、焦煤、肥煤、气煤在干燥基全硫的质量分数为1.00%~2.50%时,瘦煤、焦煤、肥煤、气煤中优化的有机硫的质量分数一般小于70%、70%~90%、大于90%、大于95%。该方法是一种经济可靠,具有模拟生产效果的特点。 相似文献
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为对复杂高硫煤进行脱硫降灰研究,根据不同粒级中硫分分布差异以及硫的主要赋存形态为硫铁矿,利用摇床进行分级重选试验;将原煤分成0.5~1 mm和1~3 mm两个粒度级,分别考查了摇床冲洗水量、冲程、床面倾角等工艺参数对分选指标的影响,确定了较为合理的工艺条件;然后对两个粒级摇床粗选精煤合并进行精选,以进一步脱硫降灰;经过两段摇床重选,精煤硫分由6.77%降低到2.15%,精煤灰分由35.10%降低到12.77%。 相似文献
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兖州矿区高硫煤中的硫以无机硫为主 ,约占全硫的 62 % ,破碎后对硫铁矿硫的解离效果不好 ,适宜采用跳汰分选降硫。由于选后煤中硫分仍高于 1 % ,建议高硫煤与低硫煤配合 ,或在高硫煤中加入固硫剂 ,以满足用户对硫指标的要求。 相似文献
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为提高无烟煤分选效果,分析了糯东矿煤质特性、粒度组成和可选性,确定原煤属低中灰~中灰、中高硫~高硫、低磷、特低抗破碎强度无烟煤,煤中硫以无机硫化铁硫形式为主;煤中细粒级含量较高,需加强细粒煤分选,粗煤泥可单独分选,产品易脱水;原煤可选性为中等可选。结合原煤性质,确定糯东选煤厂产品定位为:17煤分选中、小块煤用于化工用煤,末精煤用于高炉喷吹用煤;20煤分选中、小块煤用于化工用煤,混煤用于动力用煤。通过对比分析常用选煤方法及工艺的特点,确定糯东选煤厂无烟煤分选方案为:选前+100(80)mm检查性手选、-100(80)mm混合跳汰入选、粗煤泥干扰床分选机(TBS)分选、细煤泥浮选、尾煤浓缩压滤的联合工艺流程。 相似文献
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为提高高硫煤的浮选脱硫效率,以新峪选煤厂高硫煤泥为研究对象,分析了高硫煤的粒度组成及硫形态分布,研究煤浆质量浓度、捕收剂、起泡剂和抑制剂种类及用量对高硫煤浮选脱硫效果的影响。结果表明,新峪选煤厂煤泥硫分高达3.57%,属于高硫煤,黄铁矿硫含量较高为2.18%,可通过物理分选方法脱除。当煤浆质量浓度为80 g/L,纳尔科油用量为200 g/t,仲辛醇用量为100 g/t,巯基乙酸用量为400 g/t时,高硫煤浮选效果最好,精煤硫分为2.35%,可燃体回收率为69.23%,脱硫效率最高为24.76%。 相似文献
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ONACCURACYOFANALYSISOFOFHYDROGEN1前言我公司目前应用的氢气纯度分析方法有两种,一种是爆炸反应法,另一种是焦性没食子酸吸收法。几年来,人们对两种分析方法的准确性曾有过褒贬不一的评论。这里我们也谈谈自己粗浅的观点。2爆炸法测定氢气纯度一定量的氢气样品与适量的空气之均匀混合物因反应后生成液体水而引起气体体积减少,减少的体积等于参加反应气体体积之和。其中l/3为氧气,2/3为氢气。根据氢气取样量和反应前后混气体体积之差,以及氢气在反应中的体积比例关系,可计算出样品的氢气纯度。计算公式式中:A一混… 相似文献
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P. P. Budnikoff 《Journal of the American Ceramic Society》1924,7(11):817-820
The different analytical methods proposed for the evaluation of gypsum have been subjected to an experimental test. A combination method, consisting of a fusion with KHCO3 and determination of CaO by KMnO4 titration, the SO3 by Andrews method of titration of BaCrO4 has been found to give very reliable results with the least consumption of time. 相似文献
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A model is developed for the sedimentation from a suspension of two particle species of unequal densities and of different sizes. The composition and the thickness of various layers in the sediments are predicted using graphical and analytical methods. The model predictions were in excellent agreement with experimental results, when the particle size ratio was ≥ 108. When size ratio of the particles was 2.60 and 4.31 the agreement occurred in about 50 percent of the cases. 相似文献
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A novel technique serves to monitor instantaneous rates of loss of a volatile solute from a suspended drop during drying. A highly sensitive electron capture detector is used to monitor concentrations of SF6 released into a flowing gas stream from a suspended, drying drop. Simultaneously, the appearance and morphological development of the drop are monitored with a video camera. This provides the wherewithal of relating instantaneous rates of loss of the volatile solute to particular events during the development of particle morphology.
Initial experiments have been carried out with drops of aqueous solutions of glucose, sucrose, maltodextrin and coffee extract. The results clearly display the onset of the volatiles-retentive selective diffusion phenomenon. There is also substantial loss of the volatile component later in the drying process, when the drops undergo repeated ex ansion, bursting and cratering due to the formation of internaf bubbles. These experiments appear to be the first quantitative demonstration of major losses accompanying changes in drop morphology. 相似文献
Initial experiments have been carried out with drops of aqueous solutions of glucose, sucrose, maltodextrin and coffee extract. The results clearly display the onset of the volatiles-retentive selective diffusion phenomenon. There is also substantial loss of the volatile component later in the drying process, when the drops undergo repeated ex ansion, bursting and cratering due to the formation of internaf bubbles. These experiments appear to be the first quantitative demonstration of major losses accompanying changes in drop morphology. 相似文献
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ANALYSIS OF RECENT MEASUREMENTS OF THE VISCOSITY OF GLASSES 总被引:5,自引:0,他引:5
Viscosity of Simple Soda-Silicate 500° to 1400°C Comparison of the results given by English with those of Washburn, Shelton and Libman, indicates a discrepancy in the absolute values of log10 viscosity amounting to 0.6, those of Washburn et al., being relatively too high. If correction for this is made, the isothermal curves of log10 viscosity as a function of soda content are smooth up to 50% Na2O, showing no inflection. The observations as a function of temperature T are all represented within accidental error by an equation of the type where all three constants vary regularly with the composition. Change of Viscosity of Glass (6SiO2, 2Na2O) due to Molecular Substitution of CaO, MgO and Al2O3 for Na2O The effect is clearly brought out by plotting (from the results of English) the change of log10η due to the substitution as a function of temperature. The curves each show a sharp bend at a temperature between 840° and 1050°C, which is designated the aggregation temperature Ta. If we divide these curves by the corresponding percentage substituted, we get curves for each oxide which are straight and parallel below the aggregation temperatures, the slopes (increase of change of log10η per 100°C) being −0.056 (CaO), −0.055 (MgO), −0.018 (A12O3) per per cent oxide substituted. For substitution of 1/2 molecule the slopes are −0.325 (CaO), −0.23 (MgO) and −0.18 (Al2O3) per 100°. At the aggregation temperature the change of log10η per per cent is a minimum, 0.03 to 0.06 for CaO, 0.12 for MgO, 0.07 for Al2O3. Evidence of Aggregation in Glasses, from viscosity Measurements The sharp bends in the plots of change of log10η due to substitution of an oxide for Na2O, suggest the beginning of molecular aggregation at these temperatures. These aggregation temperatures are close to the devitrification temperatures, but the effect on the viscosity curves cannot be due to actual devitrification since it does not change with time. Taking the aggregation temperatures as equal to devitrification temperatures, additional isotherms are roughly sketched into the equilibrium triangle of the system Na2O-CaO-SiO2. Change of Viscosity of Glass (4SiO2, 2Na2O) due to of Substitution of B2O3 for SiO2 The change of log10η (from the results of English) is plotted as a function of temperature, and also the change of log10η per per cent B2O3. The curves are more complex than for the substitution for Na2O. 相似文献
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面对日益激烈的市场竞争,摩托车油箱外观质量越来越成为影响销售的因素之一。文章介绍了改进工艺后的油箱涂装,该涂装体系提高了油箱外观的丰满度,降低了油箱涂装的生产成本。 相似文献