张力异步轧制对高压电解电容器阳极铝箔织构的影响

研究了张力异步轧制参数以及再结晶退火对高压电解电容器用高纯铝箔织构的影响．结果表明：张力异步轧制条件下,快、慢辊各织构的含量随速比的变化不明显,立方织构含量不高,而S织构和C织构的含量增加．再结晶退火后,张力异步轧制铝箔的快、慢辊侧立方织构、旋转立方织构以及有利织构之和较无张力条件均有所增加．     

5052铝合金轧制织构演变的定量分析

采用X射线衍射仪研究了5052铝合金在冷轧过程中织构的演变规律,建立了织构体积分数与轧制真应变的数学关系式。结果表明,在冷轧过程中初始的cube织构逐渐转化为纤维轧制织构,随冷轧压下量的增加,cube、r-cube、remainder和r-Goss组分的体积分数减少,而纤维组分的体积分数增加;织构体积分数与轧制真应变的数学关系式能很好地模拟铝合金轧制过程中织构的演变;分析了轧制过程中不同织构组分的演变速率,发现随轧制真应变的增加,纤维组分的形成速率先增加而后降低。     

线材冷轧织构演变的定量研究

为了探讨圆柱型线材压扁过程中晶粒取向的变化规律,借助于XRD织构衍射仪与三维取向分布函数(ODF)分析,研究了异步轧制的ECAP一道次处理后的实验样品的织构随着冷轧压下量的演变规律.实验结果表明:从快辊侧分析,织构取向密度沿着冷轧实验试样的厚度从表层到中心层随着形变量的增加,冷轧纯铁试样中主要织构组分逐渐形成了<110>//RD(轧向)的α-纤维织构和<111>//ND(轧面法向)的γ-纤维织构,且织构组分的取向密度级别逐渐增加.另外,通过反极图分析与定量计算可以知道:不同压下量下, <110>织构组分体积分数由表及里呈现增长趋势.<100>织构组分体积分数在压下量为0%,40%时由表及里先上升后下降.当压下量为80%时则出现相反变化趋势.当压下量为0%时,<111>织构组分体积分数先下降后升高.而压下量为40%,80%时<111>织构组分体积分数呈现上升趋势,沿着试样厚度存在一定差别.     

蚀坑法研究冷轧及退火工艺对无取向硅钢织构演变的影响

以太原钢铁公司经酸洗后的热轧低硅板卷为实验材料,采用蚀坑法研究了一定退火工艺及不同冷轧工艺对无取向硅钢织构的影响,结果表明,总变形量及退火工艺是影响织构形成的重要因素,采用可逆轧制方法(冷轧总变形量控制在70%左右,分8道次完成,并且平均分配各道次压下率)和890 ℃加热,保温4 min,然后水冷,可以获得较高的{100}面系织构组分占有率的无取向硅钢.     

稀土电解电容器铝箔制备过程中的织构演变规律

采用蚀坑法、EBSD微取向分析和X射线法等手段,对稀土电解电容器用铝箔制备过程中的织构演变规律进行了研究.结果表明,冷轧态织构主要要类型是立方织构({001}《100》)、黄铜织构({011}《211》)、高斯织构({011}《100》)、S织构({123}《634》)和铜型织构({112}《111》).铝箔的再结晶织构主要类型是立方织构({001}《100》)、高斯织构({011}《100》)、R织构({124}《211》).随着Ce含量的增加,稀土铝箔的再结晶织构中立方织构增加,但并不是越多越好.在稀土的质量分数为0.007 4%时立方织构含量最多.同时R织构随Ce含量的增加先减少,后略有增加.随着再结晶退火温度的增加立方织构的含量增加,R织构含量减少,在530 ℃退火时立方织构含量最多.     

冷轧及退火对310S奥氏体不锈钢的微观结构和组织的影响：基于X射线和电子背散射衍射分析（英文）

本文研究了热处理对310S奥氏体不锈钢的微观结构和组织的影响。对样品材料进行冷轧,使其厚度分别减少20%、50%和90%,然后在1023、1223和1323 K下退火5、15和30 min。在厚度减少20%后,奥氏体内产生孪晶,且可观察到形变诱发的α’马氏体,孪晶的体积分数大于α’马氏体。当厚度变化由50%增加到90%,α’马氏体的体积分数由11%增加到69%,孪晶被α’马氏体取代。发生形变后奥氏体相主要为Brass、Goss和S织构,α’马氏体的主要纹理为R-Cu、R-cube、F和E组份。随着形变量增大,Brass织构增加,Goss织构减少。退火过程中,马氏体向奥氏体转变,并发生了再结晶,使Goss和Brass再结晶织构的体积分数增加。材料退火后的结构与冷轧后的大致相同。1223 K下退火5 min的马氏体转变速度明显高于1023 K下的。在1023 K下退火5 min,由于马氏体不完全转变和初级再结晶,未能检测到等轴组织。获得超细晶粒组织的最佳退火温度为1023 K,退火时间为15 min。在1173 K和1273 K时出现快速再结晶和晶粒生长。     

面心立方金属冷拔织构的计算机模拟

为了预测面心立方金属线材在冷拔过程中形变织构的演变规律,采用Taylor模型对面心立方金属冷拔织构进行模拟.采用线性规划求解剪切速率,通过计算每五个滑移系组合对应的晶粒转动的平均值作为最终的晶粒转动来解决滑移系选择模糊性问题.模拟结果表明,面心立方金属线材在拉拔过程中产生〈111〉和〈001〉纤维织构组分,〈111〉为稳定的织构组分.在变形量较小的情况下,〈001〉、〈111〉纤维织构组分比较漫散.随着变形量的增加,〈001〉、〈111〉纤维织构组分的漫散程度变小.模拟与拉拔铜线材形变织构实测结果的对比表明,采用Taylor模型能够很好模拟冷拔面心立方金属材料形变织构的演变规律.     

IF钢生产过程中的织构演变

对IF钢生产过程中热轧、冷轧及退火试样的织构演变进行研究。分别借助EBSD和XRD测定和计算了热轧、退火及冷轧试样的取向分布函数及相关织构组分的体积分数。结果发现,热轧板在变形过程中发生了动态再结晶,晶粒为细小的等轴晶,为后续组织发展提供了基础;热轧后试样中的织构很弱,不会影响冷轧织构组分及含量。冷轧过程是织构形成的主要过程,试样中含有4种主要的织构组分：{001}〈110〉、{111}〈110〉、{111}〈112〉和{112}〈110〉。退火过程中发生再结晶,4种冷轧织构组分在退火过程中均分别转变为{111}面织构。     

汽车车身用Al-Mg-Si合金薄板织构及r值的研究

采用织构测定分析、TEM观察和拉伸实验研究了退火态、固溶态及T4态汽车车身用Al-0.9Mg-1.0Si-0.7Cu-0.6Mn合金薄板的再结晶晶粒取向、拉伸变形时的晶粒转动规律及其对板材塑性应变比r值的影响.结果表明：具有copper和brass取向的冷轧铝板经410℃×1 h退火或540℃×0.5 h固溶处理后,其再结晶主织构均为绕板法线方向旋转20°的立方取向,即Cube＋ND20,自然时效对再结晶织构无明显影响;单向拉伸过程中主织构Cube＋ND20取向晶粒绕板法线ND向〈100〉方向旋转5°左右,成为Cube＋ND15取向,同时取向密度降低;不同热处理状态铝板在拉伸变形任意应变量时的r值均大致相同.     

不同Mg/Si比对含Zn的Al-Mg-Si合金再结晶组织及性能的影响

为改善Al-Mg-Si系合金汽车板综合性能,通过浇铸法制备出3组合金成分铸锭,并经过均匀化、热轧、中间退火、冷轧,获得1 mm厚的合金板材.合金板材经560℃固溶30 min后,立即在100℃条件下预时效8 h,室温停放14天,模拟铝板转运存储过程,并拉伸变形2%,再在185℃下进行20 min烘烤处理,实现烘烤硬化.采用金相显微镜、装备电子背散射衍射的扫描电镜对合金进行显微组织观察及织构分析,通过万能电子试验机进行力学性能测定,研究不同Mg/Si比和高Zn元素对合金再结晶组织及织构、烘烤硬化性以及腐蚀敏感性的影响.结果表明,Mg/Si比相等合金再结晶组织更加均匀细小,平均晶粒尺寸190μm,存在相对较少的Cube织构{001}100和较多的P型织构{011}122;高Mg合金、高Si合金局部晶粒粗大,Cube织构{001}100较多,P型织构{011}122较少;预时效后,Mg/Si比相等合金强度较高,且烘烤硬化性优异,烤漆硬化增量达到107 MPa;烤漆后,更多的Zn原子扩散到晶界上,强化晶界微电流反应,欠时效态Mg/Si比相等合金较高Mg合金、高Si合金抗腐蚀敏感性降低,被腐蚀深度为121μm.     

Texture of deformed Cu-Cr-Zr alloys

The influences of plastic deformation, aging treatment, and alloying elements on the texture of Cu-Cr-Zr alloys were explored. The texture component and intensity of Cu-Cr-Zr alloys under various working conditions after aging treatment were characterized using the orientation distributing function (ODF). The influence of Zr content on the texture of Cu-Cr-Zr alloys was also analyzed. The reduction pass and deformation level were primary factors influencing the texture. Rolling texture appeared in a rolled plate and the fibrous textures of {111} and {001} were detected after 80% deformation. Fibrous texture with a main constituent of {111} improved the tensile strength of the alloy wire. The texture contents of {110}<331> and {110}<112> were predominated, whereas, those of {113}<332> and {112}<111> were in the minority in the Cu-Cr-Zr alloy with a higher Zr content (>0.5wt%). However, in the samples with a lower Zr content (<0.1wt%), the texture contents of {113}<332>, {112}<111>, and {111}<110> were in the majority.     

基于元胞自动机方法的CSP流程冷轧低碳钢再结晶过程的模拟研究

采用元胞自动机方法对CSP流程冷轧低碳钢再结晶过程进行模拟研究。结果表明,冷轧变形量为71.4%的CSP流程冷轧低碳钢的再结晶开始温度为540℃左右,再结晶结束温度为600-620℃;计算机模拟得到再结晶完成温度为604℃,再结晶完成时间为96 min;再结晶完成时,其晶粒平均直径为7.0μm,而晶粒尺寸分布主要集中在2-14μm,此类尺寸晶粒约占晶粒总数的90%,且具备了Weibull分布函数的特征。同时冷轧低碳钢再结晶完成时,{111}〈110〉和{111}〈112〉织构组分的含量最高,总计为63.12%,{110}〈110〉和{112}〈110〉织构组分的含量则分别为9.67%和7.6%,而{001}〈110〉织构组分的含量最低。     

Mechanical performance and texture characteristic of an IF steel containing Nb and Ti by double cold rolling

Single cold rolling and double cold rolling were applied to hot rolled strips with different reduction ratios. The evolutions of {100},{111} and Goss face texture during double rolling were investigated by comparing the orientation distribution function(ODF) of the double rolled sample with that of the single rolled one. The double cold rolling texture is characterized by a higher γ-texture and a lower α-texture,and the {111}<112> component is improved remarkably. Based on the TEM observation and mechanical...     

Texture evolution of 440 MPa grade Nb-bearing high strength IF steel during rolling and annealing process

The texture evolution from rolling process to annealing process of 440 MPa grade Nb-bearing high strength IF steel (IF-HSS) was studied. Moreover, the texture of different section in thickness direction of steel sheet after annealing was investigated. Macro-texture measurements using XRD shows that hot rolling texture in Nb-bearing IF-HSS includes a weak γ-fiber and α-fiber, of which main texture components are {001}<110>,{111}<110> and {111}<112>. It is worthy of note that the γ-fiber skeleton line formed after hot rolling. During cold rolling, the absolute maximum shifts to {111}<112> along the γ-fiber and the maximum along the α-fiber shifts to {112} <110>. During recrystallization annealing process, the weaker α-fiber and stronger γ-fiber cold rolling texture transformed to a very strong γ-fiber annealing texture. After annealing the main components from surface to mid-section along thickness display the same character for both α-fiber and γ-fiber, while textures intensity at 1/4 section is higher than that of surface and mid-section.     

退火温度对Ti-IF钢性能及织构的影响

对冷轧压下率为80%、厚1 mm的Ti-IF钢经不同温度退火处理后进行拉伸试验,测量其塑性应变比r值。观察退火试样的显微组织,并利用电子背散射衍射技术（EBSD）对其性能和再结晶织构进行分析。结果表明,冷轧试验钢分别在780、810、840℃退火3 min后,均发生了再结晶;随着退火温度的升高,大多数晶粒尺寸由5-6μm增大到9-10μm;试验钢的r值随退火温度升高而增大;退火钢再结晶织构表现为强烈的{111}织构,主要由{111}〈110〉和{111}〈112〉两类取向晶粒组成。     

Cold Rolling Texture in Ordered CuZn Alloy

The texture of 80% cold rolling CuZn ordered alloy was investigated. The development of rolling texturein 50%Cu-50%Zn(at.) alloy has been characterized by a inhomogenous {111} fiber texture with strong {111} <112>component, which is significantly different from the conventional Cu-Zn alloys. The main characters of cold rollingtextures in ordered CuZn alloy are obviously similar to that in IF steel with bcc structure or ordered Fe3A1-basedalloys with imperfect B2 structure. From the rolling texture obtained by experiments and simulations,it can be estimated that main deformation mechanism are characterized by the activation of slip systems with <111> Burgersvector in CuZn ordered alloy.     

Influence of texture pretreatment on cold rolling texture of ELC-BH sheet

In order to further investigate how cold rolling texture is produced in an extra low-carbon and high strengthbake-hardening sheet steel (for short, hereafter, coiled ELC-BH sheet) with r value as high as 2.67, texture change intexture pretreatment and its effects on the cold rolling texture are researched by means of Orientation Distribution Funchon (ODf) method. Experimental results show that the cold rolling texture which Produces very strong {111 } annealing texture actually is caused by texture change in the texture pretreatment, and the strong {111 } texture obtainedrough this texture pretreatment is an essential condition of engendering the cold rolling texture, while the stability of{111 } texture components in cold rolling is a sufficient condition of emerging thes one.     

FCC金属的织构对力学性能的影响

为了研究FCC金属的织构对材料力学性能的影响,利用织构分析结果和Schmid定律,提出了FCC金属材料轧制时等效滑移系数和Schmid因子的计算方法.利用该方法分别计算了立方织构、黄铜织构和铜织构材料轧制时在法向、轧向和横向的等效滑移系数和Schmid因子的理论值.结果表明,立方织构材料轧制时在法向、轧向和横向的等效滑移系数和Schmid因子都相同,分别是8和0.41;黄铜织构材料轧制时在法向、轧向和横向的等效滑移系数和Schmid因子分别是4和0.41、2和0.27、2和0.82;铜织构材料轧制时在法向、轧向和横向的等效滑移系数和Schmid因子分别是2和0.27、2和0.82、4和0.41.并对FCC金属的变形机理与力学性能的各向异性进行了深入的讨论.