Microstructural and mechanical properties of nanometric magnesium oxide particulate-reinforced aluminum matrix composites produced by powder metallurgy method

In this research, aluminum alloy (A356.1) matrix composites reinforced with 1.5, 2.5 and 5 Vol.% nanoscale MgO particles were fabricated via powder metallurgy method. Pure atomized aluminum powder with an average particle size of 1μm and MgO particulate with an average particle size between 60 to 80 nm were used. The specimens were pressed by Cold Isostatic Press machine (CIP), and were subsequently sintered at various sintering temperatures, viz. 575, 600 and 625°C. Optimum amount of reinforcement and sintering temperature were determined by evaluating the density, microstructure and mechanical properties of composites. The composites were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD). Hardness and compression tests were carried out in order to identify mechanical properties. Reinforcing the Al matrix alloy with MgO particles improved the hardness and compressive strength of the alloy to a maximum value of 44 BHN and 288 MPa, respectively. The most improved compressive strength was obtained with the specimen including 2.5% of MgO sintered at 625°C. According to the experiments, a sintering temperature of 625°C showed better results than other temperatures. A good distribution of the dispersed MgO particulates in the matrix alloy was achieved.     

Accounting for the statistical weights of factors used when studying the liability of rolled products to brittle fracture

The interrelationships between structure, magnetic properties, and impact strength at different temperatures were studied in a 09Γ2 steel with an unchanged chemical composition after varying the heating conditions prior to rolling, as well as the final rolling temperature. These interrelations were also studied for a number of low-alloy steels of different grades (close to steel 09Γ2), which were produced in the workflow at the Nizhni Tagil Iron and Steel Works. It was shown that the coercive force and relaxation magnetization can be used to separate the effects of ferrite grain size and shape on steel properties. The constraint equations for the impact strength and magnetic properties were obtained in terms of a multiparametric model with allowance for the impact strength test temperatures. Idealized relationships between the impact strength and magnetic properties of Ст 3сп and 09Γ2 steels were obtained for the impact strength-coercive force coordinate plane with allowance for the impact strength test temperatures and statistical weight of the studied properties.     

Comparison of tribological behavior of nylon composites filled with zinc oxide particles and whiskers

Mechanical properties and tribological behavior of nylon composites filled with zinc oxides were investigated in this paper. Different effects of ZnO particles and ZnO whiskers filling on the friction and wear behavior of nylon 1010 (PA1010) composites under dry friction condition were observed. The hardness, tensile strength and scratch coefficients of two kinds of nylon composites filled with the ZnO particles and whiskers were measured. Experimental results show that ZnO particles and ZnO whiskers improve the mechanical and tribological properties of nylon composites without affecting the crystallinity of nylon matrix. Hardness, tensile strength and scratch coefficient of composites are increased by the addition of ZnO particles and ZnO whiskers. Filler shape has little effect on the friction coefficients of nylon-based composites. These composites filled with particles and whiskers have nearly the same friction coefficients which locate between 0.4 and 0.45. The wear rates of composites are strongly dependent on filler shape and filler content. Particle-filled composites exhibit the lower wear rates than whisker-filled composites when the content of filler is lower than 10 wt.%. After that, the case is reversed. Ploughing and adhesion are the main wear mechanisms of composites with the addition of both ZnO particles and ZnO whiskers.     

Study on the tribological behavior of hybrid PTFE/cotton fabric composites filled with Sb2O3 and melamine cyanurate

The tribological behavior of the hybrid PTFE/cotton fabric composites filled with microsize Sb₂O₃ and melamine cyanurate (MCA) was investigated. It was found that the wear rate of the hybrid PTFE/cotton fabric composites decreased when Sb₂O₃ was used as the filler but increased with MCA filler. It was also observed that hybrid fillers (consists of Sb₂O₃ and MCA) had a wear reduction effect on the hybrid PTFE/cotton fabric composites at lower loads but increased the wear rate at higher loads. The wear behavior of the composites was explained in terms of the topography of worn surfaces and transfer film formed on the counterpart pin.     

Solid particle erosion of unidirectional fibre reinforced thermoplastic composites

In the present study, the solid particle erosion behaviour of neat PEEK matrix and unidirectional glass fibre (GF) and carbon fibre (CF) reinforced polyetheretherketone (PEEK) and polyetherketoneketone (PEKK) composites has been studied. The erosion experiments have been carried out by using silica sand particles (200 ± 50 μm) as an erodent. Steady state erosion rates of these composites have been evaluated at different impact angles and impact velocities. The neat PEEK exhibited peak erosion rate at 30° impingement angle whereas the composites exhibited a semi-ductile behaviour with peak erosion rate at 60° impact angle. The erosion rate of the glass fibre reinforced composites was higher than that of the carbon fibre reinforced composites. The results show that the fibre orientation has a significant influence on erosion rate only at lower impact angles. The erosion rate of the composites was higher when the particles impact perpendicular to the fibre direction than parallel to the fibres. The morphology of eroded surfaces was observed under scanning electron microscope and damage mechanisms were discussed.     

Wear behaviour of Al/(Al2O3p+SiCp) hybrid composites

In this study, dry sliding metal–metal and metal–abrasive wear behaviours of the aluminium matrix hybrid composites produced by pressure infiltration technique were investigated. These composites were reinforced with 37 vol% Al₂O₃ and 25 vol% SiC particles and contained up to 8 wt% Mg in their matrixes. While matrix hardness and compression strength increased, amount of porosity and impact toughness decreased with increasing Mg content of the matrix. Metal–metal and metal–abrasive wear tests revealed that wear resistance of the composites increased with increasing Mg addition. On the other hand, abrasive resistance decreased with increasing test temperature, especially above 200 °C.     

Effect of the Graphite Content on the Tribological Behavior of Al/Gr and Al/30SiC/Gr Composites Processed by In Situ Powder Metallurgy (IPM) Method

The influence of graphite content on the dry sliding wear characteristics of Al6061/Gr composites along with Al6061/30SiC/Gr hybrid composites has been assessed using a pin-on-disc wear test. The composites with different volume fraction of graphite particles up to 13% were processed by in situ powder metallurgy (IPM) technique. The porosity and hardness of the resultant composites were also examined. It was found that an increase in the graphite content reduced the porosity, hardness, and friction coefficient of both types of composites. The hybrid composites were more porous and exhibited higher hardness and lower coefficient of friction at identical graphite contents. The increased graphite content in the range of 0–13 vol.% resulted in increased wear rate of Al/Gr composites. The Al/30SiC composite exhibited a lower wear rate as compared with the base alloy and graphite addition up to 9 vol.% improved the wear resistance of these hybrid composites. However, more graphite particles addition resulted in increased wear rate. SEM micrographs revealed that the wear mechanism was changed from mostly adhesive in the base alloy sample (Al/0Gr) to the prominently abrasive and delamination wear for Al/Gr and Al/SiC/Gr/composites.     

Effect of SiC Particle Size on Wear Properties of Al2O3·SiO2/SiC/Mg Hybrid Metal Matrix Composites

The aim of this study was to investigate the effect of SiC particle size on the wear properties of magnesium-based hybrid metal matrix composites (MMCs) reinforced with Saffil short fibers and SiC particles. Hybrid MMCs with different SiC particle sizes of 1, 7, and 20 μm, respectively, were fabricated by the squeeze infiltration process. The volume fractions of Saffil short fibers and SiC particles in the hybrid composites were 15 and 5%, respectively. Wear tests were carried out using a ball-on-disk against a steel ball under the dry sliding condition. The test results showed that the composite with large-sized SiC particles had an improved wear resistance compared with the smaller sized particles.     

Hybrid phenolic friction composites containing Kevlar® pulp Part 1. Enhancement of friction and wear performance

The friction and wear characteristics of control (without Kevlar® pulp) and hybrid (with Kevlar® pulp) phenolic composites containing milled E-glass or steel were determined at various counterface speeds and temperatures using a Chase friction tester. In general, Kevlar® pulp significantly improved the wear resistance and decreased the coefficient of friction for both types of hybrid composites. Kevlar® pulp also imparted excellent frictional stability at high speeds in steel-fiber composites and significantly reduced higher frequency ( > 5 kHz) noise at high speeds in both steel and glass-fiber composites. The stabilization of the coefficient of friction and reduction of noise was not due to the reduction of the coefficient of friction because it also occurred at constant frictional force. The addition of Kevlar® pulp to a steel-fiber-containing formulation significantly improved its overall performance.     

Effect of temperature on the charpy impact and CTOD values of type 304 stainless steel pipeline for LNG transmission

Stainless steel pipe of type 304 the with a wall thickness of 26.9 mm and the outer diameter 406.4 mm is welded by manual arc welding process. Mechanical properties and fracture toughness of type 304 stainless steel are investigated in the temperature ranging from room temperature to — 162°C. The results obtained are summarized as follows. The tensile strength noticeably increases as the temperature becomes lower while the yield strength is relatively insensitive to temperature. The Charpy impact energy and CTOD values become higher in the case that crack propagation direction is aligned to the transverse axis upon the rolling direction than longitudinal direction. The drop of fracture toughness is associated with the noticeable diminution of plastic component as temperature seduces from room temperature to — 162°C.     

Tribological Behaviour of SiC Particle Reinforced Al–Si Alloy

The purpose of this study is to explore the effect of SiC reinforcement along with immiscible element addition in spray formed Al–Si base alloy. The investigation is done for four different compositions, i.e., Al–Si base alloy, Al–Si/SiC, Al–Si–5Sn/SiC and Al–Si–10Sn/SiC composite. The dry sliding wear properties of base alloy and composites were investigated against EN 31 steel at five different normal loads (14.7, 24.5, 34.3, 44.1 and 53.9 N). The tests were carried out in dry sliding conditions with a sliding speed of 1.6 ms⁻¹ over pin-on-disc tribometer. Each composition is tested at four different temperatures 50, 75, 100 and 150 °C. To determine the wear mechanism, the worn surfaces of the samples were examined using scanning electron microscope (SEM). The composites emerge to be better wear resistant material than base alloy especially at higher loads. The optimum wear reduction was obtained in Al–Si–10Sn/SiC composite at all the different normal loads and temperatures.     

Fretting fatigue behavior of Al7075-T6 at sub-zero temperature

In some fretting fatigue applications, such as aero industry, the temperature may drop well below −50 °C Fretting fatigue behavior of aluminum alloy Al7075-T6 is investigated at temperatures of 24, 0, −25 and −50 °C in this work. The results show that (i) normal fatigue life increases considerably at sub-zero temperatures up to around 85% for low working stresses and reduces to about 40% for higher working stresses; (ii) fretting fatigue life at sub-zero temperatures rises significantly up to around 220% for low working stresses and reduces to about 50% for higher working stresses; (iii) ultimate strength of material changes from −15% to 15% under the fretting fatigue test conditions; and finally (iv) some parameters such as mechanical properties and fatigue behavior of material at low temperatures, contact load relaxation, crack closure, oxidation and some unknown sources can be thought to be responsible for fretting fatigue behavior of Al7075-T6 at sub-zero temperatures.     

填料中锌含量和焊接温度对SiC/Al复合材料接头性能的影响

通过烧结铝粉和碳化硅微粒制备SiC/Al复合材料,以组成(质量分数/％)分别为Al-20SiC、Al-20SiC-20Zn、Al-20SiC-40Zn的填料作为中间层材料,在420,520,600℃焊接温度下对复合材料进行扩散焊接,研究了填料中锌含量与焊接温度对复合材料接头性能的影响.结果表明:在420℃焊接后,接头附...     

690MPa级低合金高强钢熔敷金属冲击断裂行为研究

冲击试验是衡量金属材料韧性的最有效手段之一。对690 MPa级低合金高强钢熔敷金属进行–50℃示波冲击,分析焊接层间温度在80℃和200℃时试样的冲击性能。应用光学显微镜、扫描电子显微镜、电子背散射衍射等分析手段并采用Lepera腐蚀法,对近断口区的组织、M-A组元及夹杂物进行观察,研究冲击过程中裂纹的形核和扩展规律。结果表明:层温对熔敷金属冲击吸收功影响显著,层温80℃和200℃时,所选冲击试样裂纹形成功和扩展功分别相差6.7 J和34.0 J。进一步研究表明,两种层温下,近断口区组织主要由板条状贝氏体和粒状贝氏体组成。层温80℃时,组织主要以板条状贝氏体为主,粒状贝氏体少量分布,M-A组元以少量的颗粒状存在;层温200℃时,粒状贝氏体数量增多,M-A组元的形态以条状和块状居多,数量增加;M-A组元这种形态和数量上的变化是导致两种层温下启裂功不同的主要原因。而熔敷金属中大角度晶界数量的不同,是造成两种层温下裂纹扩展功不同的主要因素。     

On dry sliding friction and wear behavior of PPESK filled with PTFE and graphite

Novel poly(phthalazinone ether sulfone ketone) (PPESK) resins have become of great interest in applications such as bearing and slider materials. In this paper, dry sliding wear of polytetrafluoroethylene (PTFE) and graphite-filled PPESK composites against polished steel counterparts were investigated on a block-on-ring apparatus at the same sliding velocities and different loads. The results indicated that the addition of 5–25 wt% PTFE and 5–30 wt% graphite contribute to an obvious improvement of tribological performance of PPESK at room temperature. Worn surfaces were investigated using a scanning electron microscope (SEM). As a result, the friction coefficient and wear rate of the PPESK composites decreased gradually with addition of fillers. A moderately low friction coefficient and specific wear rate were reached when the filler contents were above 20 wt%. The mechanical properties of PPESK composites were also investigated. The tensile and impact strength of PPESK composites decrease slightly as the addition of fillers contents were below 15 wt%.     

Friction and Wear Behaviors of Indirect Dental Restorative Composites

Under different simulated oral environments (distilled water, artificial saliva, and a cola soft drink) and with a small-amplitude reciprocating apparatus, the friction and wear behaviors of 5 types of indirect dental restorative composites relative to uniform Si₃N₄ balls were investigated. Test parameters were: normal load with 20 N, reciprocating amplitude (1,000 μm), and frequency (0.25 Hz). Tests lasting up to 5,000 cycles were conducted. The wear damage characteristics are discussed in detail based on an analysis of friction behaviors, SEM observations, and 2- and 3-D profile microscopy. The results indicated that the hybrid resin composites with high filler weight and well filler distributions, such as Filtek P60, possess better wear resistance than nano-filled composites, such as VITA ZETA and VITA LC, with relatively low filler weight. Artificial saliva and a cola soft drink could play important roles in lowering the friction coefficient and wear loss of dental composites. The cola soft drink displayed a better lubrication effect. The degree of sensitivity to changes in lubrication conditions varies with different dental composites. Abrasive wear is the main wear mechanism for the 5 composites, but brittle cracks and delamination are more common for VITA ZETA and VITA LC.     

Tribological Behavior of Particles and Fiber-Reinforced Hybrid Nanocomposites

This article discusses the mechanical performance of alumina nanoparticles and randomly distributed short glass/carbon fiber-reinforced hybrid composites through microhardness and wear test. The open mold casting method was adapted to prepare the test coupons. The wear and friction behavior of composites sliding against hardened ground EN 32 steel in a pin-on-disc configuration is evaluated on a wear and friction tester. The microhardness properties of the neat epoxy, alumina nanoparticles, and alumina nanoparticle–embedded glass/carbon fiber–reinforced hybrid composites were determined. The morphology of the worn composites was analyzed with a scanning electron microscope. It was found that the particles as fillers contributed significantly to improve the mechanical properties and wear resistance of the polymer composites. This is because the fillers contributed to enhance the bonding strength between the fiber and the epoxy resin. Moreover, the wear and friction resistance of the glass/carbon fiber composites was increased by increasing the filler weight in the composite materials.     

Erosive Wear Mechanism of New SiC/SiC Composites by Solid Particles

A solid-particle erosive wear test by impinging silicon carbide (SiC) powders was carried out at room temperature over a range of median particle sizes of 425–600 μm, speed of 100 m/s and impact angle of 90° and assessed by wear measurements and scanning electron microscopy. Erosive wear behaviour was examined on newly fabricated nano-powder infiltration and transient eutectoid (NITE) SiC/SiC composites and two commercial composites by the chemical vapour infiltration (CVI) and NITE fabrication route. Microstructural observation was performed to examine the correlation between erosive wear behaviours and fabrication impurities. Conspicuous defects were observed in the prototype materials as the forms of porosity, fibre deformation, residual oxide, pyrolytic carbon (PyC) deformation, PyC cleavage, among others. Erosive wear behaviour was rather serious in the prototype of fabricated composites, which employ pre-SiC fibre and phenolic resin. Two dominant erosive wear mechanisms were observed: delamination of constituents, mainly caused by erosive crack propagation, and fragmentation and detachment of constituents, which usually resulted from erosive impact. A unit size of delamination was the most decisive factor affecting wear volume. The bonding strength of each constituent was mostly affected by various forms of porosities. Therefore, the fundamental cause and subsequent results must be carefully elucidated. The correlation of microstructural defect and wear behaviour was investigated with the aim of reducing dominant wear by improving fabrication conditions. The final product of the cost-effective composite had a 2.5-fold higher resistance than the commercial CVI composite. Consequently, by controlling fabrication impurities, we have been successful in developing and improving a new fabrication technique; consequently, the known defects are rarely observed in final product. A schematic wear model of erosive wear mechanisms is proposed for the newly fabricated SiC/SiC composites under particle erosion.     

Solid particle erosion behaviour of glass fibre reinforced boric acid filled epoxy resin composites

The tests which involved angular aluminium (Al₂O₃) particles with two different sizes of approximately 200 and 400 μm were conducted at the operating conditions namely different impact velocities of approximately 23, 34 and 53 m/s, two different fibre directions [0° (0/90) and 45° (45/−45)] and three different impingement angles of 30°, 60° and 90°. New composites with addition of Boric Acid filler material at 15% of resin exhibited upper wear than the neat materials without filler material. This means the filler material has decreased the erosion wear resistance. SEM views showing worn out surfaces of the test specimens were scrutinised.     

High-Temperature Friction and Wear of Ag/h-BN-Containing Ni-based Composites Against Steel

In order to attain self-lubrication in a wide range of temperatures, Ni-based powder metallurgy (P/M) composites containing different amounts (8–20 wt%) of Ag were prepared, and their friction and wear characteristics were investigated against AISI 52100 steel at temperatures of 25, 400, and 600 °C. One composite containing 12 wt% Ag and 4 wt% h-BN was also prepared and tested under the same conditions to analyze the effect of addition of h-BN on the friction and wear behaviors. The composites mainly consisted of Ni-based solid solution, free tungsten, Ag, and BN as revealed by XRD and EDS analyses. The friction coefficients and wear rates were found to decrease with increasing temperature and amount of silver. The friction coefficients shown by the composites containing relatively higher amounts of silver were in the range from 0.25 to 0.16 with temperature increasing from RT to 600 °C. The wear rates of the Ag/h-BN-containing composites were approximately an order of magnitude lower than those of the Base Alloy (having no solid lubricant) at all the temperatures. The addition of 4 wt% h-BN resulted in slightly greater friction and wear in comparison to the composites containing only silver.