Fatigue properties of friction stir welded particulate reinforced aluminium matrix composites

Few papers have discussed the friction stir welding (FSW) of particulate reinforced aluminium matrix composites and most of them focused on the set-up of the welding process parameters and their effect on microstructure, hardness and tensile behaviour. The aim of this study was to investigate the fatigue resistance of FSW joints on an as-cast particulate reinforced aluminium based composite (AA6061/22 vol.%/Al₂O_3p). The welding process was performed using different process parameters, also investigating their effect on joint microstructure. The mechanical properties of the FSW composites were compared with those of the base material and the results were correlated to the microstructural modifications induced by the FSW process on the aluminium alloy matrix and the ceramic reinforcement. FSW reduced the size of both particle reinforcement and aluminium grains, and also led to a significant increase in interparticle matrix microhardness, for all process parameters. The FSW specimens belonging to a different set of parameters, tested without any post-weld heat treatment, exhibited a very high joint efficiency (ranging from 90% to 99%) with respect to the ultimate tensile strength of the base material. The stress controlled fatigue test showed a high spread both for the base and FSW composites. Statistical analysis disclosed that all FSW specimens belonging to different process parameters showed apparently slightly worse fatigue behaviour than that of the base composite. Statistical processing applied to the different welding parameters revealed that all the welded specimens belonged to the same population. Therefore it can be concluded that the parameters used produced joints with similar microstructure and comparable fatigue behaviour. The slight difference in the fatigue behaviour of the FSW specimens whose process parameters differed form those of the unwelded composite was explained by the different microstructural homogeneity in the transition from the base to the FSW zone.     

Development of Al3Ti and Al3Zr intermetallic particulate reinforced aluminum alloy AA6061 in situ composites using friction stir processing

Aluminum rich intermetallic particles are potential reinforcements for discontinuously reinforced aluminum matrix composites (DRAMCs). The objective of the present work is to produce AA6061/Al₃Ti and AA6061/Al₃Zr composites using in situ casting technique and applying friction stir processing (FSP) to enhance the distribution and morphology of Al₃Ti and Al₃Zr particles. AA6061/Al₃Ti and AA6061/Al₃Zr DRAMCs were produced by the in situ reaction of inorganic salts K₂TiF₆ and K₂ZrF₆ with molten aluminum. The microstructure was observed using optical and scanning electron microscopy. AA6061/Al₃Ti DRAMC exhibited clusters of Al₃Ti particles while the segregation of needle shape Al₃Zr particles was observed in AA6061/Al₃Zr DRAMC. The prepared composites were subjected to FSP. Significant changes in the distribution and morphology of Al₃Ti and Al₃Zr particles were observed after FSP. The changes in microhardness and sliding wear behavior of AA6061/Al₃Ti and AA6061/Al₃Zr DRAMCs before and after FSP is detailed in this paper.     

Microstructure and mechanical properties of Cr3C2 particulate reinforced Al2O3 matrix composites

Al₂O₃ matrix with three grades of Cr₃C₂ particle size (0.5, 1.5 and 7.5 m) composites were fabricated by a hot-pressing technique. Fully dense compacts with Cr₃C₂ content up to 40 vol % can be acquired at 1400 °C under 30 MPa pressure for 1 h. The flexural strength increases from 595 to 785 Mpa for fine Cr₃C₂ particle (0.5 m) reinforced Al₂O₃ matrix composites. The fracture strength is significantly dependent on the fracture modes of matrix (intergranular or transgranular). The transgranular fracture with a compressive residual stress gives a high fracture strength of composites. At the same time, the fracture toughness increases from 5.2 MPa m^1/2 (10 vol % Cr₃C₂) to 8.0 MPa m^1/2 (30 vol % Cr₃C₂) for the coarse Cr₃C₂ particle (7.5 n) reinforced Al₂O₃ matrix composites. The toughening effects of incorporating Cr₃C₂ particles into Al₂O₃ matrix originate from crack bridging and deflection. The electrical conductivity and the possibility of electrical discharge machining of these composites were also investigated.     

A comparison between friction stir welding,linear friction welding and rotary friction welding

Three friction welding processes are compared for temperature, stresses and strains, as well as strain rates developed in the early phases of the processes, which are essential in their successful development. These are friction stir welding (FSW), linear friction welding (LFW) and rotary friction welding (RFW). Their common characteristic is the use of friction to generate adequate energy and raise temperature locally in order to create favorable conditions for welding at the interface between two parts. Although the mode of movement is different for each one of them, welds are produced through plastic deformation. The Lagrangian and coupled Eulerian-Lagrangian numerical models developed have produced results which are in qualitative agreement with experiments and have shed a light on the commonalities of these friction welding processes.     

Material flow during friction stir spot welding of dissimilar Al2024/Al materials

In the present paper, the material flow and intermixing during friction stir spot welding of dissimilar Al2024/Al materials were investigated. The dissimilar materials had quite different strength. The microstructural evolutions taking place during a series of lap and butt welds were observed. The effect of penetration depths, dwell time, rotational speed and tool geometry were systematically investigated. The material flow and formation of the intermixed region were explained by a modified model.     

Integrated modeling of friction stir welding of 6xxx series Al alloys: Process, microstructure and properties

Compared to most thermomechanical processing methods, friction stir welding (FSW) is a recent technique which has not yet reached full maturity. Nevertheless, owing to multiple intrinsic advantages, FSW has already replaced conventional welding methods in a variety of industrial applications especially for Al alloys. This provides the impetus for developing a methodology towards optimization, from process to performances, using the most advanced approach available in materials science and thermomechanics. The aim is to obtain a guidance both for process fine tuning and for alloy design. Integrated modeling constitutes a way to accelerate the insertion of the process, especially regarding difficult applications where for instance ductility, fracture toughness, fatigue and/or stress corrosion cracking are key issues. Hence, an integrated modeling framework devoted to the FSW of 6xxx series Al alloys has been established and applied to the 6005A and 6056 alloys. The suite of models involves an in-process temperature evolution model, a microstructure evolution model with an extension to heterogeneous precipitation, a microstructure based strength and strain hardening model, and a micro-mechanics based damage model. The presentation of each model is supplemented by the coverage of relevant recent literature. The “model chain” is assessed towards a wide range of experimental data. The final objective is to present routes for the optimization of the FSW process using both experiments and models. Now, this strategy goes well beyond the case of FSW, illustrating the potential of chain models to support a “material by design approach” from process to performances.     

Tool penetration during friction stir spot welding of Al and Mg alloys

The mechanism of tool penetration during friction stir spot welding of Al-alloy and Mg-alloy sheet materials is investigated and is explained as a progression of wear events, from mild wear to severe wear and then to melt wear in material beneath the base of the rotating pin. Melt wear can also occur under the rotating tool shoulder provided that sufficient penetration of the upper sheet occurs during the spot welding operation. The highest temperatures attained during FSW spot welding of Al 6111 and AZ91 base materials are close to the solidus temperatures of each base material and correspond with 0.94T_s (Al 6111) and 0.99 T_s (AZ91) where T_s is the solidus temperature of the material in degrees Kelvin.     

Immersed friction stir welding of ultrafine grained accumulative roll-bonded Al alloy

In this research, ultrafine grained strips of commercial pure strain hardenable aluminum (AA1050) were produced by accumulative roll-bonding (ARB) technique. These strips were joined by friction stir welding (FSW) in immersed (underwater) and conventional (in-air) conditions to investigate the effect of the immersion method on the microstructure and mechanical properties of the joint, aiming to reduce the deterioration of the mechanical properties of the joint. Transmission electron microscopy and X-ray diffraction analyses were used to evaluate the microstructure, showing smaller grains and subgrains in the stir zone of the immersed FSW condition with respect to the conventional FSW method. The hardness and tensile properties of the immersed friction stir welded sample and ARBed base metal show more similarity compared to the conventional friction stir welded sample. Moreover, the aforementioned method can result in the enhancement of the superplasticity tendency of the material.     

Linear friction welding of Ti6Al4V: experiments and modelling

Linear friction welding of the Ti6Al4V alloy is studied. A new definition of the energy input rate is proposed, based on an integration over time of the in-plane force and velocity; a strong correlation with the upset rate is then found. The effective friction coefficient is estimated to be 0·5±0·1 for varying frequencies and amplitudes, with only a weak dependence on the processing conditions displayed. A model is proposed that accounts for both the conditioning and equilibrium stages of the process, which is shown to be in good agreement with the experimental data. The model is used to study the mechanism by which the flash is formed. A criterion is proposed by which the rippled nature of its morphology can be predicted.     

Effect of friction stir welding on microstructure,tensile and fatigue properties of the AA7005/10 vol.%Al2O3p composite

Several studies have been recently focused on friction stir welding of aluminium alloys and some data are also reported on FSW of aluminium-based composites. The application of this solid state welding technique to particles reinforced composites seems very attractive, since it should eliminate some typical defects induced by the traditional fusion welding techniques, such as: gas occlusion, undesidered interfacial chemical reactions between the reinforcement and the molten matrix alloy, inhomogeneous reinforcement distribution after welding. The present work describes the effect of the FSW process on the microstructure and, consequently, on the tensile and low-cycle fatigue behaviour, of an aluminium matrix (AA7005) composite reinforced with 10 vol.% of Al₂O₃ particles (W7A10A). The microstructural characterization evidenced, in the FSW zone, a substantial grain refinement of the aluminium alloy matrix (due to dynamic recrystallization induced by the plastic deformation and frictional heating during welding) and a significant reduction of the particles size (due to the abrasive action of the tool). Tensile tests showed a high efficiency of the FSW joints (about 80% of the ultimate tensile strength). The low-cycle fatigue tests evidenced a fatigue life reduction for the FSW material respect to the base composite, particularly for high values of total strain range. The fracture mechanisms for the FSW specimens were those typical of metal matrix composites: interfacial decohesion, void nucleation and growth, as well as fracture of reinforcing particles, as shown by SEM analyses of the fracture surfaces.     

Microstructure and mechanical properties of dissimilar Al alloy/steel joints prepared by a flat spot friction stir welding technique

The 6061-T6 Al alloy and mild steel plate with a thickness of 1 mm were successfully welded by the flat spot friction stir welding technique, which contains two steps during the entire welding process. The rotating tools with different probe lengths of 1.0, 1.3 and 1.5 mm were used in the first step, during which a conventional spot FSW was conducted above a round dent previously made on the back plate. However, sound Al/Fe welds with similar microstructure and mechanical properties can still be obtained after the second step, during which a probe-less rotating tool was used to flatten the weld surface. The sound welds have smooth surface without keyholes and other internal welding defects. No intermetallic compound layer but some areas with amorphous atomic configuration was formed along the Al/Fe joint interface due to the lower heat input. The shear tensile failure load can reach a maximum value of 3607 N and fracture through plug mode. The probe length has little effect on the weld properties, which indicates that the tool life can be significantly extended by this new spot welding technique.     

Mechanical properties of copper to titanium joined by friction welding

This paper describes a fundamental investigation of friction welding pure copper to titanium. Friction welding was performed using a brake type friction welder. The effect of friction time and upset pressure on the mechanical and metallurgical properties were evaluated. Under constant upset pressure, the tensile strength made little difference with an increase in friction time, whereas at the constant friction time, the tensile strength increased with increasing upset pressure. Thus, the upset pressure plays a major role over the friction time and friction pressure on tensile strength. Though Cu₃Ti intermetallic compound is formed at the copper/titanium interface during welding, the tensile strength of welded joint is not affected. It may be due to the thickness of intermetallic compound layer at interface being very thin and scattered. The tensile fracture of the welded joint occurred in copper side near the interface.     

Study of friction welding characteristics of Al/SiC composite and application of grey-based TOPSIS

The present work investigates the possibility of producing friction welded joints with an advanced material like Al/SiC (aluminum–silicon carbide) composite. The study also discloses the multi response optimization in the process of continuous drive friction welding using a hybrid algorithm of grey-based TOPSIS (technique for order of performance by similarity to ideal solution). The friction welding parameters (frictional pressure, upset pressure, burn off length and rotational speed) were optimized considering the multiple performance characteristics such as proof stress, tensile strength, and microhardness. Taguchi’s L₂₇ orthogonal array was used for conducting the welding trials. The confirmation test was conducted at the optimal setting, to sort out the effectiveness of the proposed hybrid algorithm. The macro photographs of the joints and optical micrographs of the weld zone were studied. The scanning electron microscope images of the fractured surface were also examined to identify the failure mode of joints. The significant improvements in the performance characteristics prove the effectiveness of the grey-based TOPSIS method in experimental welding optimization.     

Relationship between base metal properties and friction stir welding process parameters

Friction stir welding (FSW) is a solid state welding process for joining aluminum alloys and has been employed in aerospace, rail, automotive and marine industries for joining aluminium, magnesium, zinc and copper alloys. In FSW, the base metal properties such as yield strength, ductility and hardness control the plastic flow of the material under the action of rotating non-consumable tool. The FSW process parameters such as tool rotational speed, welding speed, axial force, etc. play a major role in deciding the weld quality. In this investigation, an attempt has been made to establish relationship between the base material properties and FSW process parameters. FSW joints have been made using five different grades of aluminium alloys (AA1050, AA6061, AA2024, AA7039 and AA7075) using different combinations of process parameters. Macrostructural analysis has been done to check the weld quality (defective or defect free). Empirical relationships have been established between base metal properties and tool rotational speed and welding speed, respectively. The developed empirical relationships can be effectively used to predict the FSW process parameters to fabricate defect free welds.     

Fabrication of 5052Al/Al2O3 nanoceramic particle reinforced composite via friction stir processing route

In this research, microstructure and mechanical properties of 5052Al/Al₂O₃ surface composite fabricated by friction stir processing (FSP) and effect of different FSP pass on these properties were investigated. Two series of samples with and without powder were friction stir processed by one to four passes. Tensile test was used to evaluate mechanical properties of the composites and FSP zones. Also, microstructural observations were carried out using optical and scanning electron microscopes. Results showed that grain size of the stir zone decreased with increasing of FSP pass and the composite fabricated by four passes had submicron mean grain size. Also, increase in the FSP pass caused uniform distribution of Al₂O₃ particles in the matrix and fabrication of nano-composite after four passes with mean cluster size of 70 nm. Tensile test results indicated that tensile and yield strengths were higher and elongation was lower for composites fabricated by three and four passes in comparison to the friction stir processed materials produced without powder in the similar conditions and all FSP samples had higher elongation than base metal. In the best conditions, tensile strength and elongation of base material improved to 118% and 165% in composite fabricated by four passes respectively.     

Prediction of tensile strength of friction stir welded aluminium matrix TiCp particulate reinforced composite

The usage of particulate reinforced metal matrix composite (MMC) is steadily increasing due to its properties such as high specific strength, high specific modulus and good wear resistance. Aluminium matrix composite (AMC) plays an important role to meet the above requirements. Effective utilization of AMC is based on not only its production but also on fabrication methods. Among AMCs, those based on particulate reinforcements are particularly attractive, due to their lower production costs. Aluminium matrix titanium carbide reinforced composite (Al–TiC_p) was produced in an inert atmosphere by indigenously developed Modified Stir Casting Process with bottom pouring arrangement (3–7% TiC by weight). Friction stir welding process (FSW) is employed to make weld joints. The welding parameters such as axial force, welding speed, tool rotational speed, percentage TiC addition etc., and profile of the tool were considered for analysis. In this study, an attempt is made to predict ultimate tensile strength (UTS) of the welded joints using a mathematical model. The FSW specimens without any post-weld heat treatment belonging to a different set of parameters tested, exhibited a high joint efficiency (most of them ranging from 90% to 98%) with respect to the ultimate tensile strength of the base material AA6061. It was found from the analysis of the model that the tool pin profile and the welding speed have more significant effect on tensile strength.     

Characterization of friction stir welded boron carbide particulate reinforced AA6061 aluminum alloy stir cast composite

Development of welding procedures to join aluminum matrix composite (AMCs) holds the key to replace conventional aluminum alloys in many applications. In this research work, AA6061/B₄C AMC was produced using stir casting route with the aid of K₂TiF₆ flux. Plates of 6 mm thickness were prepared from the castings and successfully butt joined using friction stir welding (FSW). The FSW was carried out using a tool rotational speed of 1000 rpm, welding speed of 80 mm/min and axial force of 10 kN. A tool made of high carbon high chromium steel with square pin profile was used. The microstructure of the welded joint was characterized using optical and scanning electron microscopy. The welded joint showed the presence of four zones typically observed in FSW of aluminum alloys. The weld zone showed fine grains and homogeneous distribution of B₄C particles. A joint efficiency of 93.4% was realized under the experimental conditions. But, FSW reduced the ductility of the composite.