共查询到15条相似文献,搜索用时 125 毫秒
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番茄红素的提取工艺研究 总被引:2,自引:0,他引:2
鲜番茄制成糊,用Na2CO3溶液皂化,再用稀硫酸中和起泡,过滤。滤饼用乙醇处理过滤后用有机溶剂提取番茄红素。考察了皂化剂用量、皂化时间、乙醇用量、提取剂种类及其用量、料液比、浸提时间、浸提温度、pH值等因素对提取率的影响。结果显示,新鲜番茄中提取番茄红色素的最佳工艺条件为:用0.5 mol/L的Na2CO3溶液对番茄糊进行皂化,物料比为1∶2,皂化温度40℃,皂化时间30 m in;乙醇∶番茄(体积∶质量)为2∶1,处理时间10 m in;用乙酸乙酯和丙酮的混合液进行提取,乙酸乙酯∶丙酮为1∶2(体积比),物料比为1∶4,浸提温度45℃,浸提时间50 m in,pH=7。在此最佳条件下,番茄红素的相对提取率可达85.9%。 相似文献
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番茄红素提取方法的研究 总被引:35,自引:0,他引:35
研究了从番茄中提取番茄红素的方法 ,考察了提取温度、时间、料液比、浸取液等影响因素 ,确定了最佳的浸取工艺条件。使用 6# 溶剂油二级浸提番茄糊 ,在番茄糊质量与溶剂体积比为 0 33g/ml、浸提时间 2~ 3h、pH值 6、浸提温度 35℃及加入助剂条件下 ,能充分提取色素 ;若使用微波辐射法 ,在微波功率 2 0 0W、萃取时间 80s,番茄糊质量与溶剂体积比为 0 5g/ml条件下 ,能得到最好效果 相似文献
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微波法提取番茄红素的研究 总被引:2,自引:0,他引:2
研究了微波法对番茄红素提取效果的影响。确定番茄红素的最优提取条件为:微波功率420 W,处理时间为25 s,固液比为1∶2(g∶mL),提取次数为3次。 相似文献
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Cottonseed extraction with mixtures of acetone and hexane 总被引:3,自引:0,他引:3
Cottonseed flakes were extracted with mixtures of n-hexane and acetone, with the concentration of acetone varying between 10 and 75%. Adding small amounts of acetone (≤25%)
to n-hexane significantly increased the extraction of free and total gossypol from cottonseed flakes. Sensory testing detected
no difference in the odor of cottonseed meals produced either by extraction with 100% n-hexane or by extraction with a 10∶90 (vol/vol) mixture of acetone/hexane. More than 80% of the free gossypol was removed
by the 10∶90 mixture of acetone/hexane, whereas pure n-hexane extracted about 47% of the free gossypol from cottonseed flakes. A solvent mixture containing 25% acetone removed
nearly 90% of the free gossypol that was removable by extraction with pure acetone; the residual meal had only a minimal increase
in odor. In contrast, cottonseed meals produced by extraction with pure acetone had a much higher odor intensity. The composition
of the cottonseed crude oil was insignificantly affected by the acetone concentration of the extraction solvent. The results
indicate that mixtures of acetone and n-hexane can be used as extraction solvents to produce cottonseed crude oil without the concomitant development of odorous
meals. 相似文献
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The use of supercritical fluid extraction is proposed for obtaining stable extracts with high added value from natural and
economical sources. Lipid composition, namely, of FFA, TAG, and FAME, in tomato skin extracts with high lycopene content was
determined. Separation of different classes of lipids was achieved from tomato extracts using TLC followed by transesterification
and GC, and lycopene and other carotenoids were analyzed by HPLC with a photodiode array detector. In lycopene extracts obtained
using supercritical fluids, no FFA were found and polyunsatureted TAG represented only 9.2% of the total TAG content. 相似文献
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自组装了动力波实验装置,对装置的复合性能、气速与压降、驻区与气液比等关系进行测定,确定了装置正常操作的条件,气速在2 264.84 917 L/h范围内,液气比在0.015 54 917 L/h范围内,液气比在0.015 50.027 4之间,驻区稳定。以空气通过丙酮溶液模拟车间含丙酮空气,对装置的吸收效率进行测定。结果表明,以清水为吸收液时,低浓度丙酮吸收效率接近100%;以含丙酮水循环操作时,随溶液中丙酮浓度增高,吸收效率降低;吸收液中添加丙酮稳定剂时,随稳定剂浓度增加效果会下降,稳定剂浓度为处理液的1.36/10 000时,吸收率比清水提高12%,总效率可达86.2%。 相似文献