Extraction and preparation of bamboo fibre-reinforced composites

Natural plant fibre composites have been developed for the production of a variety of industrial products, with benefits including biodegradability and environmental protection. Bamboo fibre materials have attracted broad attention as reinforcement polymer composites due to their environmental sustainability, mechanical properties, and recyclability, and they can be compared with glass fibres. This review classifies and describes the various procedures that have been developed to extract fibres from raw bamboo culm. There are three main types of procedures: mechanical, chemical and combined mechanical and chemical extraction. Composite preparation from extracted bamboo fibres and various thermal analysis methods are also classified and analysed. Many parameters affect the mechanical properties and composite characteristics of bamboo fibres and bamboo composites, including fibre extraction methods, fibre length, fibre size, resin application, temperature, moisture content and composite preparation techniques. Mechanical extraction methods are more eco-friendly than chemical methods, and steam explosion and chemical methods significantly affect the microstructure of bamboo fibres. The development of bamboo fibre-reinforced composites and interfacial adhesion fabrication techniques must consider the type of matrix, the microstructure of bamboo and fibre extraction methods.     

Ageing effect on tensile and shrinkage behaviour of new green hybrid fibre-reinforced cementitious composites

Ageing effects on both uniaxial tensile and shrinkage behaviour of new green cementitious composites reinforced with bagasse fibre and steel fibre with ultra-high volume of fly ash are investigated in this paper. The tensile behaviour of the composites is investigated at the age of 28 days, 3 months, 6 months and 10 months after curing in weather conditions. Restrained shrinkage behaviour of the composites after curing for 3 months is tested on ring specimens. SEM tests are also conducted to study the influence of the ageing on the microstructure of the new composites. The test results show that the tensile strength of the composites at all ages increases with the decrease of the content of the fly ash and the bagasse fibre, and that the increasing application of fly ash and bagasse fibre decreases the steel ring strain and restrains the development of crack. It is also found that the tensile strength and the shrinkage of the composites such as crack width ascend greatly with time.     

Effects of fluctuation of fibre orientation on tensile properties of flax sliver-reinforced green composites

Plant-based natural fibres are often used as a reinforcing material for environmentally friendly green composites. Especially, the form of slivers of natural fibres is anticipated for increasing their stiffness and strength. However, the sliver structure has fluctuations in fibre orientation, which decreases their mechanical properties. This paper describes the effects of such fibre orientation fluctuation on tensile properties of fibre-reinforced fully green composites. The composites were reinforced with slivers of high-strength flax fibres, for which a fabrication method called ‘direct method’ was applied. To quantify the morphology of the fibre orientation, fibre orientation angles were measured on fine segments, which were divided into 1 mm × 1 mm squares on a photograph of the whole composite surface. Although it is well-known that tensile strength of unidirectional composites decreases with increasing fibre orientation angle, the tensile strength obtained here did not show any appreciable relation to the statistical properties of measured fibre orientation angles such as average and standard deviation. The concept of two-dimensional (2D) autocorrelation was used in the present study to express the degree of similarity between fibre orientation angles in two different local areas. Results show that, if high 2D autocorrelation coefficients occupy more area on a composite surface, then this composite possesses more regular fibre orientation and tends to exhibit higher tensile strength. This tendency is stronger in the composites close to on-axis alignment, whereas it became weak in the off-axis composites angled more than 15° because of shear fracture.     

Modelling tensile properties of jute fibres

Abstract

This short communication extends earlier modelling of the tensile strength and failure strain of jute technical fibres. A maximum likelihood estimate (MLE) model, a linear model and a natural logarithmic interpolation model (NLIM) are compared. The NLIM model is found to give superior predictions.     

Damage evolution in sinter-hardening powder-metallurgy steels during tensile and fatigue loading

The damage approach was used to compare the tensile and push-pull fatigue behaviour of two high-strength sinter-hardened powder metallurgy (PM) steels, with a density of 6.7 and 7.2 g/cm³. In both alloys, tensile damage was found to start when the ratio of the applied stress to UTS was greater than about 0.3. The tensile damage was due to localized yielding and, in a later stage, to the formation of several micro-cracks that joined to form more than one macrocrack. Fatigue damage was followed in the finite fatigue life regime and was found to develop through three stages. During the first one, damage increased with fatigue cycling up to the attainment of a plateau (second stage) that lasted to a fraction of about 0.9 of the fatigue life. The damage recorded during the second stage was very similar to that encountered in the tensile tests at the same stress to UTS ratio. The formation of microcracks was observed in the third stage only, when the fraction of fatigue life was greater than 0.9. During this stage damage increased very sharply and this was due to the growing and joining of the microcracks to form one long crack able to lead to final fracture.     

A comparative study of fatigue behaviour of flax/epoxy and glass/epoxy composites

Experimental investigations on flax and glass fabrics reinforced epoxy specimens, i.e. FFRE and GFRE, submitted to fatigue tests are presented in this paper. Samples having [0/90]_3S and [±45]_3S stacking sequences, with similar fibre volume fractions have been tested under tension–tension fatigue loading. The specific stress-number of cycles to failure (S–N) curves, show that for the [0/90]_3S specimens, FFRE have lower fatigue endurance than GFRE, but the [±45]_3S FFRE specimens offer better specific fatigue endurance than similar GFRE, in the studied life range (<2 × 10⁶). Overall, the three-stage stiffness degradation is observed in all cases except for [0/90]_3S FFRE specimens, which present a stiffening phenomenon of around 2–3% which could be related to the straightening of the microfibrils.     

Damage evolution and real-time non-destructive evaluation of 2D carbon-fiber/SiC-matrix composites under fatigue loading

Electrical resistance acquisition, acoustic emission (AE) monitoring and infrared thermography were employed to evaluate damage evolution of 2D carbon-fiber/SiC-matrix composite under fatigue loading. Damage evolution was discussed on the basis of the calculation results of the modulus and mechanical hysteresis variation. At lower stress levels, the majority of damage was produced in the first few cycles and then the rate of damage accumulation gradually approached a steady value as the cycles proceeded. When the applied stress exceeded the endurance fatigue limit, extensive damage took place and led to failure of the composite. Changes of composite electrical resistance, AE activity and surface temperature had fairly well agreement with the modulus and hysteresis responses. It can be concluded that it is possible to employ these real-time non-destructive evaluation methods as in-situ damage evolution indicators for this kind of composites under fatigue loading.     

Plant-based natural fibre reinforced cement composites: A review

The quest for sustainability in construction material usage has made the use of more renewable resources in the construction industry a necessity. Plant-based natural fibres are low cost renewable materials which can be found in abundant supply in many countries. This paper presents a summary of research progress on plant-based natural fibre reinforced cement-based composites. Fibre types, fibre characteristics and their effects on the properties of cement-based materials are reviewed. Factors affecting the fresh and hardened properties of cement-based composites reinforced with plant-based natural fibre are discussed. Measures to enhance the durability properties of cement-based composites containing plant-based natural fibres are appraised. Significant part of the paper is then focused on future trends such as the use of plant-based natural fibres as internal curing agents and durability enhancement materials in cement-based composites. Finally, applications and recommendations for future work are presented.     

Synergy in hybrid polymer/nanocarbon composites. A review

The aim of this review article is to report the most recent developments in the understanding of and beliefs about the properties of polymer hybrid composites that are reinforced with various combinations of nanometer-sized carbon and mineral fillers. The discussions are primarily focused on an analysis and comparison of the electrical, thermal, and mechanical properties. It is shown that the introduction of a mixed (hybrid) system of filler nanoparticles into polymer matrices enhances the macro- and microproperties of the composites as a result of the synergistic interactions between the fillers and the simultaneous creation of a unique filler network in the polymer. The synergy of various types of carbon nanofillers and combinations of nanocarbon materials with inorganic fillers manifests itself as modifications of most of the properties of hybrid polymer composites relative to the properties of a polymer system containing a single filler. The reinforcing effect is related to the structure and particle geometry of the hybrid fillers, the interactions between the fillers, the concentrations and the processing methods.The existence of synergy between different types of carbon nanofillers, as well as with mineral fillers, shows great potential and could significantly increase applications of carbon-based nanomaterials.     

A micromechanics model for the prediction of fatigue characteristics of off-axis unidirectional laminates

In this paper, the concentric cylinders model is used to predict the fatigue characteristics of off-axis unidirectional laminates. A failure criterion that uses stresses averaged along the radial distance in each constituent phase is applied to predict the S-N curves of unidirectional laminates. The predicted S-N curves compare well with the experimental data for various off-axis Glass/Epoxy laminates.     

A review of the effect of stitching on the in-plane mechanical properties of fibre-reinforced polymer composites

This paper reviews over fifty studies into the effect of through-the-thickness stitching on the in-plane mechanical properties of fibre-reinforced polymer composites. Reviewed are the in-plane tensile, compressive, flexure, interlaminar shear, creep, fracture and fatigue properties, although little work has been undertaken on the last three properties. When comparing studies it is apparent that many contradictions exist: some studies reveal that stitching does not affect or may improve slightly the in-plane properties while others find that the properties are degraded. In reviewing these studies it is demonstrated that predicting the influence of stitching on the in-plane properties is difficult because it is governed by a variety of factors, including the type of composite (eg. type of fibre, resin, lay-up configuration), the stitching conditions (eg. type of thread, stitch pattern, stitch density, stitch tension, thread diameter), and the loading condition. The implications of these findings for the use of stitching in lightweight engineering structures are discussed.     

A fatigue life prediction method for coke drum base,weld, and HAZ materials from tensile properties

The importance of material fatigue information in design has been well recognized. There are a few existing fatigue life prediction methods based on materials tensile properties. Some of these fatigue life prediction methods can be successfully applied for non-heat affected materials. However, industrial components, such as pressure vessel and pipelines are commonly constructed by welding parts together. The fatigue lives of welded section and its surrounding material could be greatly affected by the welding process. Therefore, it is beneficial to develop a fatigue life prediction model for the weld and surrounding heat affected zone (HAZ) materials based on their tensile testing data. In this paper, fatigue lives of base material and its weld and HAZ materials for constructing coke drums are studied. Mechanical properties are first obtained from the tensile tests. Then, fully-reversed strain-controlled fatigue tests were performed. It is found that the fatigue life of pure base material is roughly twice of the weld and four time of the HAZ at the same strain amplitude. Four-point correlation (FPC) method by Manson can reasonably predict the life of base material. However, it over-predicts the lives of weld and HAZ. By introducing two reduction factors R_plastic and R_elastic for the weld and HAZ material respectively into the FPC method, the over-prediction can be rectified. Therefore, the proposed modified FPC method could be applied in predicting fatigue lives of weld and HAZ materials.     

A fatigue damage model of composite materials

The mechanical properties of composite materials degrade progressively with the increasing of the number of cyclic loadings. Based on the stiffness degradation rule of composites, a phenomenological fatigue damage model is presented in this paper, which contains two material parameters. They are proportional to the fatigue life of materials and inversely proportional to the fatigue loading level. Thirteen sets of experimental data of composite stiffness degradation were employed to verify the presented model, and the statistical results showed that this model is capable of describing the damage evolution of composite materials. The characteristics of damage development and accumulation of composite materials subjected to variable loading were studied in this paper. Four sets of two-level loading experimental data were cited to verify the damage model, and the results showed that the predicted life is in good agreement with the experimental ones.     

Influence of moisture uptake on the static,cyclic and dynamic behaviour of unidirectional flax fibre-reinforced epoxy laminates

This papers aims to characterize the influence of moisture uptake on the mechanical behaviour of unidirectional flax fibre-reinforced epoxy laminates. Monotonic and cyclic tensile tests and free vibration characterization are carried out. Results show that UD flax-epoxy composites, when exposed to hygrothermal conditioning at 70 °C and 85% RH, exhibit a diffusion kinetic which follows a one dimensional Fickian behaviour. The mass uptake at equilibrium is approximately 3.3% and the diffusion coefficient 6.5 × 10⁻⁶ m² s⁻¹. Water vapour sorption is shown to induce a significant change in the shape of the tensile stress-strain curve, a decrease in the dynamic elastic modulus of about 20% and a 50% increase in the damping ratio. Contrary to all expectations, water saturation does not degrade the monotonic tensile strength of such a flax-epoxy composites and leads to an increase in the fatigue strength for a high number of cycles.     

Acoustic emission for monitoring the mechanical behaviour of natural fibre composites: A literature review

In recent years, natural fibres are increasingly used as reinforcements for the production of low-cost and lightweight polymer composites: other advantages include non-abrasive nature, high specific properties, and biodegradability. However, their limitations, including moisture absorption, poor wettability and large scattering in mechanical properties, and the not sufficient understanding of mechanisms controlling their mechanical behaviour and failure modes, still confine the use of natural fibre reinforced composites in non-structural applications. Acoustic emission (AE) proved useful for its capability of real-time monitoring over the whole material volume and high sensitivity to any process generating stress waves.This paper presents a literature review of AE applications in studies on natural fibre composites. The following fields of application are covered: (1) interface studies in single fibre composite (SFC) tests, (2) damage evolution and failure mechanisms detection and (3) crack propagation, including also current limitations of existing literature and future work.     

A smart repair system for polymer matrix composites

The widespread use of polymer composites is still caveated with concerns about the loss in structural performance that can result from impact damage. Such events give rise to delaminations which may not be easily detectable by eye. This paper describes a technique for ‘smart’ repair of delaminations in polymer composites. This involves the filling of hollow fibres with a resin, which is released into the damaged area when the fibre is fractured. A two-part epoxy resin is used as the repair medium, the two components being diluted with solvent and infiltrated into different plies of a composite based on ‘Hollex’ S2-glass fibre. Compression strength after impact tests were used as a measure of the effectiveness of the repair technique, and a potential improvement was noted after application of heat and vacuum to the damaged composite. Resin release from the fibres was noted by microscopy. A more comprehensive study is required to verify the improvement in post-impact strength, and the use of larger internal diameter fibres would enhance the amount of resin released.     

Fabrication and modelling of the macro-mechanical properties of cross-ply laminated fibre-reinforced polymer composites using artificial neural network

The mechanical behaviour of fibre-reinforced polymer composites (FRPCs) is considered very complex due to many factors such as composition, material type, manufacturing process and end user applications. This article presents the mechanical properties and artificial neural network (ANN) modelling results of cross-ply laminated FRPCs. Twenty composite samples were fabricated by varying the number of layers of carbon fibre and glass fibre as reinforcement and polyphenylene sulphide and high-density polyethylene as matrix. Mechanical properties were measured in terms of flexural modulus, hardness, impact and transverse rupture strength. Multilayer feed-forward backpropagation ANN approach was used to predict the mechanical properties by using material type, composition and number of reinforcement and matrix layers as input variables. From 20 data patterns, 16 were used for network training and remaining 4 were used to test the models. Furthermore, trend analysis was also performed to understand the influence of inputs on developed models. It is evident from the ANN prediction results that there is good correlation between predicted and actual values within acceptable mean absolute error. The outcomes of this research will help to reduce cost and time by eliminating tedious composite property measurements and to fabricate tailored composites meeting application requirements.     

Transverse cracking and delamination in cross-ply gr/ep composites under dry, saturated and immersed fatigue

Motivated by experimental observations, the finite element method is employed to model the competition between the transverse cracking and delamination modes of failure that occur in cross-ply AS4/3501-6 gr/ep coupons subjected to fatigue. The results explain the extensive delaminations and reduced crack densities that arise under immersed fatigue, as compared with fatigue in air. This revised version was published online in August 2006 with corrections to the Cover Date.     

Large dielectric constant of the chemically purified carbon nanotube/polymer composites

The chemically purified multiwalled carbon nanotube/poly(vinylidene fluoride) (MWCNT/PVDF) composites were fabricated. Raman spectroscopy and transmission electron microscopy micrographs indicated that the catalysts metal particles and amorphous carbon had been removed from the purified MWCNTs. The percolation threshold of the composites is relatively large, about 3.8 vol.%. The most important result is that the dielectric constant of the composites is enhanced remarkably, and the dielectric constant of 3600 is obtained in the composite with 8 vol.% purified MWCNT at 1 kHz. The large dielectric constant can be attributed to the preparation procedure and the interface effect between the MWCNTs and the polymer.     

Tensile,creep and fatigue behaviours of short fibre reinforced polymer composites at elevated temperatures: a literature survey

Polymer composites are suitable alternatives to metals in some applications as they are cost effective, lightweight and corrosion resistant. Short fibre reinforced polymer composites (SFRPCs) are typically subjected to complex loadings in applications, including static, cyclic, thermal and their combinations. These applications may also involve harsh environmental conditions such as elevated temperature and moisture which can dramatically affect mechanical properties. In this paper, a broad survey of the literature on mechanical behaviour of SFRPCs at elevated temperatures is presented. The mechanical behaviours included consist of tensile, creep, isothermal fatigue, thermo‐mechanical fatigue and creep–fatigue interaction. Environmental effects such as moisture and ageing at elevated temperatures are also included. The studies reviewed include experimental works, modelling works and failure mechanisms studies. A critical assessment of the information from the literature presented for each type of behaviour is also provided.