CONTROLLING HIGHTEMPERATURE DEFORMATION BY VARYING MICROSTRUCTURE IN A Ti47Al2Cr2Nb ALLOY

１　ＩＮＴＲＯＤＵＣＴＩＯＮγＴｉＡｌａｌｌｏｙｓａｒｅａｔｔｒａｃｔｉｖｅｓｔｒｕｃｔｕｒａｌｍａｔｅｒｉａｌｓｂｅｃａｕｓｅｏｆｔｈｅｉｒｐｏｔｅｎｔｉａｌａｐｐｌｉｃａｔｉｏｎｓｉｎａｅｒｏｓｐａｃｅａｎｄａｕｔｏｍｏｂｉｌｅｉｎｄｕｓｔｒｉｅｓ［１］．ＣｕｒｒｅｎｔｒｅｓｅａｒｃｈｏｎγＴｉＡｌｉｓｐｒｉｍａｒｉｌｙｆｏｃｕｓｅｄｏｎｉｍｐｒｏｖｉｎｇｉｔｓｒｏｏｍｔｅｍｐｅｒａｔｕｒｅｄｕｃｔｉｌｉｔｙ,ｔｏｕｇｈｎｅｓｓａｎｄｈｉｇｈｔｅｍｐｅｒａｔｕｒｅｃｒｅｅｐｒｅ…     

DEFORMATION STRUCTURES IN A Ti45Al 10Nb ALLOY AT ROOM TEMPERATURE

１　ＩＮＴＲＯＤＵＣＴＩＯＮＩｎｒｅｃｅｎｔｙｅａｒｓ，ａｎｕｍｂｅｒｏｆｐａｐｅｒｓｈａｖｅｓｔｕｄｉｅｄｔｈｅｄｅｆｏｒｍａｔｉｏｎｓｔｒｕｃｔｕｒｅｏｆＴｉＡｌｂａｓｅａｌｌｏｙｓｉｎａｎａｔｔｅｍｐｔｔｏｉｍｐｒｏｖｅｉｔｓｄｕｃｔｉｌｉｔｙ［１－６］．ＩｔｈａｓｂｅｅｎｃｌａｉｍｅｄｔｈａｔｔｈｅｈｉｇｈＣＲＳＳｆｏｒ〈１１０］ｏｒｄｉｎａｒｙｓｌｉｐｉｎＡｌｒｉｃｈｓｉｎｇｌｅｐｈａｓｅＴｉＡｌａｌｌｏｙｓｉｓｒｅｓｐｏｎｓｉｂｌｅｆｏｒｔｈｅｉｒｌａｃｋｏｆｄｕｃｔｉｌｉｔ…     

THERMAL ACTIVATION ANALYSIS ON TENSILE DEFORMATION IN Ti47Al2Mn2Nb ALLOY

１　ＩＮＴＲＯＤＵＣＴＩＯＮγＴｉＡｌ／α２Ｔｉ３ＡｌｔｗｏｐｈａｓｅｉｎｔｅｒｍｅｔａｌｌｉｃｓｏｒＴｉＡｌａｌｌｏｙｈａｓｒｅｃｅｎｔｌｙｒｅｃｅｉｖｅｄｉｎｃｒｅａｓｉｎｇａｔｔｅｎｔｉｏｎｂｅｃａｕｓｅｏｆｉｔｓｐｏｔｅｎｔｉａｌａｓａｓｔｒｕｃｔｕｒａｌｍａｔｅｒｉａｌｆｏｒｈｉｇｈｔｅｍｐｅｒａｔｕｒｅａｐｐｌｉｃａｔｉｏｎｓ,ｗｈｉｃｈａｒｉｓｅｓｆｒｏｍｉｔｓｅｌｅｖａｔｅｄｈｉｇｈｔｅｍｐｅｒａｔｕｒｅｓｔｒｅｎｇｔｈ,ｌｏｗｄｅｎｓｉｔｙａｎｄｇｏｏｄｏｘｉｄａｔｉｏ…     

β Phase decomposition in Ti–5Al–5Mo–5V–3Cr

The decomposition of the β phase during rapid cooling of the near β titanium alloy Ti–5Al–5Mo–5V–3Cr has been studied using in situ X-ray synchrotron diffraction combined with ex situ conventional laboratory X-ray diffraction and transmission electron microscopy (TEM). Evidence is found supporting the suggestion by De Fontaine et al. (Acta Mater. 1971;19) that embryonic ω structures form by the correlation of linear (1 1 1)β defects at high temperatures. Further cooling causes increased correlation of these defects and the formation of athermal ω structures within the β matrix at temperatures ～500 °C. Post-quench aging at 570 °C resulted in the nucleation of α laths after ～90 s at temperature, with the laths all initially belonging to a single variant type. Aging for 30 min produced an even distribution of α precipitates with a lath morphology ～1.5 μm × 0.2 μm in size composed of both the expected Burgers variants. Mechanical property data suggests that the ω structures alone have no real effect; however, hardness increases were observed as the α phase developed. The utilization of thermal regimes similar to those presented in this paper could offer a method to engineer the α phase in near β titanium alloys and hence control mechanical properties.     

Ti5Mo5V2Cr3Al合金中绝热剪切带的微观结构演化

利用分离式Hopkinson压杆,对Ti5Mo5V2Cr3Al(TB10)合金帽形试样进行强迫剪切试验,通过光学显微镜和透射电镜技术观测其绝热剪切带(ASB)内的微观结构。结果表明,ASB的过渡区由具有高位错密度的沿着剪切方向的宽度为20～50nm的拉长组织构成;剪切带中心由大量低位错密度(相对ASB的过渡区)的直径为50～100nm的晶粒组成,具有典型的再结晶组织特征。在绝热剪切变形过程中ASB内的平均绝热温升约为784℃。ASB内发生了动态再结晶,晶粒尺寸为50～100nm。     

0Cr12Mn5Ni4Mo3Al钢小型高压容器的焊接工艺

介绍了某型号小型高压容器的结构特点和技术要求;分析半奥氏体沉淀硬化不锈钢0Cr12Mn5Ni4Mo3Al的焊接性和气瓶的焊接技术难点;制订了焊接工艺方案;详细说明了高压容器试制时的焊接过程和控制焊缝缺陷及焊接变形的方法与措施.探伤与液压试验和爆破试验的结果表明:首批试制的高压容器的焊接质量符合设计要求,工艺方案完全适合于小型、薄壁、偏心、细直径高压容器的焊接加工.现已进行了多个批次的生产,焊接质量稳定,并且满足设计要求.     

DEFORMATION-INDUCED α2→γ TRANSFORMATION IN A HOT DEFORMED Ti-45A1-10Nb ALLOY

1.IntroductionTwo-phase(a2 7)TiAl-basedall0ysarecurrentlyunderextensiveinvestigationbe-causetheirmechanicalpr0pertiesaresuperi0rtoeitherthesinglephasecr20rtheryall0ysl1].Themicrostructureofthetwo-phasealloyswasf0undtohaveastronginfluence0ntheme-chanicalpr0pertiesI2].Themainmicrostructuralcharacteristics0ftheall0yswithlamellarstructurewhichconsistsofalternatinglayers0f0rdered7anda2lamellaewiththecri-entationrelati0nship{lll}./(OOO1)..3<11O>./<1120>.,)havebeenstudiedindetailbymanyinvestigat0r…     

0Cr12Mn5Ni4Mo3Al不锈钢自锁螺母的开裂原因

某0Cr12Mn5Ni4Mo3Al不锈钢自锁螺母在服役过程中出现开裂。对开裂螺母进行了宏观和微观断口形貌观察、表面能谱分析、显微组织及力学性能分析与测试等。结果表明：该螺母开裂原因为应力腐蚀开裂(SCC)。裂纹起源于法兰面与螺母体交接处,螺母体与法兰面呈直角此处易积液,螺母表面处理方式为钝化和涂MoS₂,其耐蚀能较差。在腐蚀性潮湿大气环境中,干湿交替作用下螺母产生局部腐蚀点,在腐蚀点处萌生裂纹,裂纹在螺母圆周切向拉应力作用下扩展直至螺母开裂。     

时效处理温度对0Cr12Mn5Ni4Mo3Al钢力学性能的影响

对0Cr12Mn5Ni4Mo3Al钢进行固溶热处理,选定430 ℃、480 ℃、520 ℃、560 ℃、590 ℃共5个温度进行时效处理试验,探讨了时效处理温度对0Cr12Mn5Ni4Mo3Al钢的硬度和拉伸性能的影响规律,确定了制备某设备上的高压无扩口导管钢材的最佳固溶处理温度范围为1 000～1 050 ℃,最佳时效温度范围为480～520 ℃.     

Ti3Al─Nb合金不同组织状态下拉伸断裂行为显微分析

用透射电镜及备有拉伸装置的Ｓ５７０扫描电镜，研究了Ｔｉ３ＡｌＮｂ（Ｔｉ２４Ａｌ１４Ｎｂ３Ｖ０．５Ｍｏ）（摩尔百分数）合金在不同热处理制度下的组织形貌以及试样的拉伸断裂过程。结果表明：合金在α２＋β两相区固溶１ｈ水冷处理，组织由α２相、Ｂ２相和ｏ相组成。初生α２相体积分数不同，合金试样拉伸断裂机制不同，初生α２相体积分数低时，变形主要在Ｂ２相，裂纹主要在Ｂ２相内形核，随着Ｂ２相的减少，合金塑性提高。初生α２相体积分数高时，变形主要在α２相，裂纹主要萌生于α２相内，随着Ｂ２相的增多，合金塑性提高。细小的随机分布的针状α２相对合金拉伸断裂行为有良好作用。随固溶温度升高，α２相中位错密度逐渐减少，Ｂ２相中位错密度逐渐增多     

A MICROSTRUCTURAL ANALYSIS OF 7050 Al ALLOY

The microstructure of 7050 AI alloy in T74 condition has been studied by means of transmis-sion electron microscopy and dynamical diffraction simulation.It was found that the alloystudied contains mainly AI3Zr superlattice phase,η′-phase and Al_7Cu_2Fe constituent phase.The η′-phase has an orthorombic crystal structure with a=0.492 nm,b=0.852 nm andc=0.701 nm.The orientation relationship between the η′-phase and matrix was determinedas(101)_m∥(010)_(η′)[111]_m∥[001]_(η′)     

AN IN-SITU STUDY ON DISLOCATION BEHAVIOR OF CRACK-TIP IN Ti_3Al-Nb ALLOY

ＡＮＩＮＳＩＴＵＳＴＵＤＹＯＮＤＩＳＬＯＣＡＴＩＯＮＢＥＨＡＶＩＯＲＯＦＣＲＡＣＫＴＩＰＩＮＴｉ３ＡｌＮｂＡＬＬＯＹ①ＷｕＹｉｎｇ，ＺｈｅｎＬｉａｎｇ，ＹａｎｇＤｅｚｈｕａｎｇＳｃｈｏｏｌｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎｄＥｎｇｉｎｅｒ...     

Al—Ti—B晶粒细化合金中的有效形核相

研究了ＡｌＴｉＢ晶粒细化合金中各化合物相ＴｉＡｌ３、ＴｉＢ２和ＡｌＢ２对铝晶粒的细化作用。结果表明，ＴｉＡｌ３相是有效形核相，ＴｉＢ２和ＡｌＢ２相不能单独作为形核相，Ｂ对ＡｌＴｉＢ的细化作用有显著影响，但Ｂ及硼化物不能单独影响细化过程，而是富集在ＴｉＡｌ３相中对细化过程产生重要影响。     

TENSILE DEFORMATION AND FRACTURE BEHAVIOR OF Ti_3Al-Nb ALLOY AT HIGH TEMPERATURE

ＴＥＮＳＩＬＥＤＥＦＯＲＭＡＴＩＯＮＡＮＤＦＲＡＣＴＵＲＥＢＥＨＡＶＩＯＲＯＦＴｉ３ＡｌＮｂＡＬＬＯＹＡＴＨＩＧＨＴＥＭＰＥＲＡＴＵＲＥ①ＷｕＹｉｎｇ，ＺｈｅｎＬｉａｎｇ，ＹａｎｇＤｅｚｈｕａｎｇＳｃｈｏｏｌｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａｎ...     

EFFECT OF TEST TEMPERATURE ON DEFORMATION MECHANISM OF Ti_3Al-Nb ALLOY

ＥＦＦＥＣＴＯＦＴＥＳＴＴＥＭＰＥＲＡＴＵＲＥＯＮＤＥＦＯＲＭＡＴＩＯＮＭＥＣＨＡＮＩＳＭＯＦＴｉ３ＡｌＮｂＡＬＬＯＹ①ＷｕＹｉｎｇ，ＬｉａｎｇＷｅｉ，ＣｕｉＹｕｅｘｉａｎ，ＬｉＤａｏｍｉｎｇ，ＹａｎｇＤｅｚｈｕａｎｇＳｃｈｏｏｌｏｆＭａｔｅｒｉａ...     

IN-SITU OBSER VATION OF SINGLE-POINT WEAR OF PM Al-Ti ALLOY

ＩＮＳＩＴＵＯＢＳＥＲＶＡＴＩＯＮＯＦＳＩＮＧＬＥ－ＰＯＩＮＴＷＥＡＲＯＦＰＭＡｌＴｉＡＬＬＯＹ①ＷｕＪｉｎｍｉｎｇ，ＷｕＮｉａｎｑｉａｎｇ，ＷａｎｇＧｕａｎｇｘｉｎ，ＬｉＺｈｉｚｈａｎｇＤｅｐａｒｔｍｅｎｔｏｆＭａｔｅｒｉａｌｓＳｃｉｅｎｃｅａ...     

Ti3Al5Mo5V合金在热压缩变形状态下的组织和应力分析

采用Gleeble-1500热模拟机对Ti3Al5Mo5V合金进行热压缩变形，对α β相、β相钛合金变形后的显微组织进行了分析，比较了合金在不同变形条件下所产生的应力变化趋势和影响因素。结果表明，在Ti3Al5Mo5V合金热变形中，α β相无论在高应变速率还是在低应变速率下，都发生了再结晶，且随温度升高所产生的应力急剧下降，流变软化明显，应力对温度变化敏感。β相在高应变速率下产生动态回复，低应变速率下只发生晶界滑移，应力对温度变化不敏感。     

Ti－24Al－14Nb－3V－0．5Mo合金的超塑性

研究了温度及应变速率对Ｔｉ－２４Ａｌ－１４Ｎｂ－３Ｖ－０．５Ｍｏ（ａｔ．－％）合金超塑性能的影响．试验结果表明，在９８０℃，３．５×１０~（－４）ｓ~（－１）的最佳超塑变形条件下，合金显示出较高的超塑性；应变速率敏感性指数ｍ为０．６９，拉伸延伸率Ｅｌ．为８１８％．根据其细小的α_２＋β_０两相组织和等温拉伸的试验方法，确定合金的超塑性属于细晶组织超塑性．在超塑变形过程中，合金无空洞产生，显微组织发生动态粗化．