几种生物陶瓷材料的裂纹扩展特性

采用破坏力学中的双扭矩实验法，研究了玻璃陶瓷、云母陶瓷、氧化铝陶瓷、氧化锆陶瓷材料分别在大气、水环境中的静负荷和循环负荷下的裂纹扩展特征，阐明了水环境和循环负荷对材料裂纹扩展特性（KI－V特征）的影响。所研究的材料在水环境下的裂纹扩展速度均加快，但玻璃陶瓷和氧化锆陶瓷材料更为明显。在静负荷下这几种材料的裂纹扩展阻力由小到大的次序为：玻璃陶瓷（N－0），玻璃陶瓷（N－11），云母陶瓷，氧化锆陶瓷和氧化铝陶瓷，对于氧化铝和氧化锆陶瓷材料在循环负荷下的裂纹扩展速度均明显加快。     

Cyclic fatigue of ceramics

The fatigue behaviour of alumina, zirconia-toughened alumina (ZTA) and tetragonal zirconia (TZP) have been investigated using three different techniques. Direct push-pull testing has been used to generate both static and cyclic fatigue data. The results clearly show that all the materials studied are susceptible to both static and cyclic fatigue, and that the times to failure under cyclic loading are considerably shorter than under static loads. The fatigue failure origins have been identified and the influence of surface condition on fatigue life has been assessed. The slow propagation of cracks subject to cyclic tensile and compressive loads has been studied using compact tension specimens and tapered double cantilever beam specimens. These investigations have confirmed the existence of cyclic fatigue effects in coarse-grained alumina and have shown the crack increment per cycle (da/dN) to have a power-law dependence on the peak stress intensity factor. A technique, based on repeated indentation, has been used to investigate the propagation of sub-surface cracks subjected to cyclic loading in both fine-grained alumina and ZTA. The results of the investigation suggest that compressive or closure loads on the crack faces are factors which affect the cyclic fatigue crack growth in ceramics. Based on those observations, an explanation is proposed for the mechanical cyclic fatigue effects in the ceramics investigated.     

ENVIRONMENTAL EFFECTS ON CRACK PROPAGATION IN ALUMINIUM ALLOYS

Abstract Crack propagation rates have been measured in two aluminium alloys under cyclic and static loading, in air, and in salt solution. On the basis of these results, a model is proposed, whereby corrosion fatigue crack propagation may be interpreted in terms of fatigue and static stress corrosion characteristics. Two interacting processes are operative; one is "stress assisted dissolution", which tends to inhibit mechanical failure by crack blunting and microbranching. The other is "environment assisted fracture" which occurs too rapidly for dissolution to occur. One or other of these processes is always observed to be dominant. This proposal is discussed in relation to other recent models for corrosion fatigue cracking. The effects of frequency, waveform and mean stress variations are also considered.     

Crack growth in ferroelectric ceramics under electric loading

Summary A crack with growth in ferroelectric ceramics under purely electric loading is analyzed. The crack tip stress intensity factor for the growing crack under small scale conditions is evaluated by employing the model of nonlinear domain switching. The electrical fracture toughness is obtained from the result of the stress intensity factor. It is shown that the ferroelectric material can be either toughened or weakened as the crack grows. Fatigue crack growth in a ferroelectric material under cyclic electric loading is also examined. The incremental fatigue crack growth under cyclic electric loading is obtained numerically. The fatigue crack growth rate is affected strongly by the electrical nonlinear behavior. It is found that the curve of fatigue crack growth rate versus electric field intensity factor is linear on the log-log plot at intermediate values of the electric field intensity factor.     

显微结构对Sialon陶瓷室温疲劳短裂纹扩展行为的影响

本文采用不同相组成和不同显微结构的。α-β-Sialon复相陶瓷作为对比试样,以压痕裂纹模拟陶瓷材料本身固有的微小裂纹,通过四点弯曲试样,在相同力学参数条件下,结合扫描电子显微镜对疲劳断口的观察,研究了α-β-Sialon复相陶瓷的室温疲劳短裂纹扩展现象和微观机理．研究发现,长柱状β-Sialon晶粒含量多、长径比大的材料具有较高抵抗疲劳失效的能力·此外,疲劳断口表明,α-β-Sialon复相陶瓷疲劳短裂纹扩展的机制主要有：应力腐蚀、摩擦造成的晶粒桥接弱化和接触损伤．     

Numerical investigation of fatigue characteristics of concrete pavement

In concrete pavements, fatigue is one of the major causes of distress. Repeated loads result in the formation of cracks. The propagation of these cracks cause internal progressive damage within the structure, which ultimately leads to failure of the pavement due to fatigue. This paper presents a theoretical investigation of crack propagation within concrete pavement and its fatigue characteristics under cyclic loading. A numerical fatigue performance model has been developed for this purpose. The model is based on fictitious crack approach for the propagation of cracks and stress degradation approach for estimating the bridging stress under cyclic loading. Using the numerical model, a parametric study has been performed for a typical concrete pavement to evaluate its fatigue characteristics for different foundation strengths. The method can be used for prediction of crack propagation in concrete pavement under cyclic loading and gives an estimate of the incremental damage or the entire crack history of the pavement.     

Static mode fatigue crack propagation and generalized stress intensity correlation for fatigue–brittle polymers

Stable fatigue crack propagation is predominantly described by the Paris power law correlation of the crack growth rate with the amplitude cyclic stress intensity. The Paris relationship works well for most ductile materials but does not capture the response for fatigue–brittle materials lacking a cyclic damage mechanism, including ceramics and many polymers. Instead, crack growth rate of fatigue–brittle materials correlates to the peak cyclic stress intensity factor, \(\hbox {K}_{\mathrm{max}}\). This work shows that \(\hbox {K}_{\mathrm{max}}\) correlation of fatigue crack growth is derived directly from static mode crack tip behavior with constant correlation coefficients, and that \(\Delta \hbox {K}\) correlations are not generally applicable for static mode crack propagation in fatigue–brittle polymers. This derivation predicts load ratio, frequency, and waveform effects, which are included in a general static mode fatigue crack propagation law. Fatigue crack propagation data of a known fatigue–brittle polymer are presented to demonstrate static mode crack propagation behavior correlation with \(\hbox {K}_{\mathrm{max}}\) with constant parameters.     

FATIGUE CRACK GROWTH LAWS FOR BRITTLE AND DUCTILE MATERIALS INCLUDING THE EFFECTS OF STATIC MODES AND ELASTIC-PLASTIC DEFORMATION

A fatigue crack growth damage accumulation model is used to derive laws for the fatigue crack growth rates of brittle and ductile materials. The damage accumulated during cyclic loading is assumed to be proportional to the cyclic change in the plastic displacement in the crack tip yielded zone. The static mode contribution to the fatigue damage is assumed to be proportional to some power of the crack tip displacement. The laws are applicable in either the small or large scale yielding regimes provided that the stress ratio remains positive. Static modes are assumed to be controlled by the fracture toughness value in brittle materials, and by the gradient of the crack growth resistance curve in ductile materials. In the analysis of ductile materials it is assumed that the crack growth resistance of the material is not significantly altered by fatigue crack growth.
The growth rate equations are expressed in terms of the near field value of the J -integral, i.e. the value which would be calculated from assuming the material deformed in a non-linear elastic manner during the increasing load part of the fatigue cycle. Examples are given of the predictions of the growth law for ductile materials. It is predicted that after the initiation of stable tearing the crack growth rate, when expressed in terms of the cyclic change in the stress intensity factor, depends on both the structural geometry and the degree of crack tip plastic deformation. In both brittle and ductile materials the fatigue crack growth rate is predicted to accelerate as the failure criteria relevant to static crack instability are approached.     

Influence of Inhibitor Concentration on Corrosion Fatigue Crack Initiation and Propagation

The paper reports the effect of0.01,0.1 and 1%NaNO2, a passive inhibitor, on corrosion fatigue (CF) crack initiation and propagation for a low strength structural steel A537 in 3.5%NaCl aqueous solution. The experimental results show that inhibitor increases the required cycles of CF crack initiation effectively, and this effect increases with increasing inhibitor concentration.However, there is nearly no effect of NaNO2 on CF crack propagation. The same CF crack propagation rate was found in all kinds of solutions. The results also indicate that the passive time in 1%NaNO2 solution during plastic deformation is much longer than cyclic time. NaNO2 passivates the specimen sudece and repairs passive film damaged by cyclic loading during the crack initiation. while the passsive film is not formed fully due to continuous plastic deformation at the crack tip during the CF crack propagation, which is much different from that in the stress corrosion cracking and general corrosion     

CRACK FACE INTERACTIONS AND NEAR-THRESHOLD FATIGUE CRACK GROWTH

Rough fracture surfaces usually influence substantially the fatigue growth properties of materials in the regime of low growth rates. Friction, abrasion, interlocking of fracture surface asperites and fretting debris reduce the applied load amplitude to a smaller effective value at the crack tip (“sliding crack closure”, or “crack surface interaction” or “crack surface interference”). The influence of these phenomena on the fatigue crack growth properties of structural steel is discussed and compared for the two kinds of mixed mode loading employed in this work. Mixed mode loading was performed by (A): cyclic mode III + superimposed static mode I and (B): cyclic mode I + superimposed static mode III loading. Such loading cases frequently occur in rotating load-transmission devices. Several differences are typical for these two mixed-mode loading cases. A superimposed static mode I load increases the crack propagation rate under cyclic mode III loading whereas cyclic mode I fatigue crack propagation is retarded when a static mode III load is superimposed. Increase of the R -ratio (of the cyclic mode III load) leads to an insignificant increase of fracture surface interaction and subsequently to a small decrease of the crack growth rate for cyclic mode III loading, whereas higher R -values during cyclic mode I+ superimposed static mode III loading lead to a significant reduction of the crack growth rates.     

Nanoscopic fatigue and stress corrosion crack growth behaviour in a high-strength stainless steel visualized in situ by atomic force microscopy

In situ atomic force microscope (AFM) imaging of the fatigue and stress corrosion (SC) crack in a high‐strength stainless steel was performed, under both static and dynamic loading. The AFM systems used were (1) a newly developed AFM‐based system for analysing the nanoscopic topographies of environmentally induced damage under dynamic loads in a controlled environment and (2) an AFM system having a large sample stage together with a static in‐plane loading device. By using these systems, in situ serial clear AFM images of an environmentally induced crack under loading could be obtained in a controlled environment, such as in dry air for the fatigue and in an aqueous solution for the stress corrosion cracking (SCC). The intergranular static SC crack at the free corrosion had a sharp crack tip when it grew straight along a grain boundary. The in situ AFM observations showed that the fatigue crack grew in a steady manner on the order of sub‐micrometre. The same result was obtained for the static SC crack under the free corrosion, growing straight along a grain boundary. In these cases, the crack tip opening displacement (CTOD) remained constant. However, as the static SC crack was approaching a triple grain junction, the growth rate became smaller, the CTOD value increased and the hollow ahead of the crack tip became larger. After the crack passed through the triple grain junction, it grew faster with a lower CTOD value; the changes in the CTOD value agreed with those of the crack growth rate. At the cathodic potential, the static SC crack grew in a zigzag path and in an unsteady manner, showing crack growth acceleration and retardation. This unsteady crack growth was considered to be due to the changes in the local hydrogen content near the crack tip. The changes in the CTOD value also agreed with those of the crack growth rate. The CTOD value in the corrosive environment was influenced by the microstructure of the material and the local hydrogen content, showing a larger scatter band, whereas the CTOD value of the fatigue crack in dry air was determined by the applied stress intensity factor, with a smaller scatter band. In addition, the CTOD value in the corrosive environment under both static and dynamic loading was smaller than that of the fatigue crack; the environmentally induced crack had a sharper crack tip than the fatigue crack in dry air.     

A probabilistic static fatigue model for transverse cracking in CFRP cross-ply laminates

This paper presents a delayed-fracture model for transverse cracking in CFRP cross-ply laminates under static fatigue loading. First, a delayed-fracture model for a crack in a brittle material was established on the basis of the slow crack growth (SCG) concept in conjunction with a probabilistic fracture model using the three-parameter Weibull distribution. Second, the above probabilistic SCG model was applied to transverse cracking in cross-ply laminates under static fatigue loading. The stress and the length of the unit element in the transverse layers were calculated with the aid of a shear-lag analysis, taking the residual stress into account. The transverse crack density was expressed as a function of applied stress and time with the parameters in the Paris law and the Weibull distribution function specified, in addition to the mechanical and geometrical properties. Unknown parameters were determined from experiment data gathered in static tensile and static fatigue tests. The reproduced transverse crack density at various applied loads agreed well with the experiment results.     

Fatigue behavior of surface cracked filament wound pipes with high tangential strength in corrosive environment

The aim of this study is to examine the corrosion fatigue behavior of filament wound composite pipes with a surface crack under alternating internal pressure. The filament wound pipes are composed of multi-layered E-glass/epoxy composites with a [±75°]₃ lay-up. The surface notches were formed on the outer surface of the pipe along the pipe axis. Dilute (0.6 M) HCl acid was applied to the surface crack region by a corrosion cell mounted on the outer surface of the pipe. The results of an experimental investigation into the corrosion fatigue tests are conducted to observe the oil leakage failure and the crack propagation of the composite pipe subjected internal pressure loading with an open ended condition in which the pipe can be deformed freely in the axial direction. The internal pressure was generated by conventional hydraulic oil for fatigue loading. The fatigue tests are performed at 0.42 Hz frequency and a stress ratio of R = 0.05 in accordance with ASTM D-2992 standard. The oil leakage from the crack tip was observed after the crack propagation reached to the critical stress intensity level. The fatigue crack propagation behavior with the environment exposure was strongly dependent on the crack parameters such as crack-depth ratio and crack-aspect ratio. The micro structure of the fracture surface with the effect of environment and the fatigue loading were also observed.     

Fatigue fracture toughness of metals

The paper considers the peculiarities of fatigue crack propagation and final fracture of metals under cyclic loading. It is shown that the value of the fatigue fracture toughness of steels in an embrittled state is appreciably lower than that of the fracture toughness under static loading. A model of the transition from stable to unstable fatigue crack propagation is justified.     

Analysis of temperature distribution near the crack tip under constant amplitude loading

An analytical/numerical method has been developed to find the temperature rise near the crack tip under fatigue loading. The cyclic plastic zone ahead of the crack tip is assumed to be the shape of the source of heat generation and some fraction of plastic work done in cyclic plastic zone as heat generation. Plastic work during fatigue load was found by obtaining stress and strain distribution within the plastic zone by Hutchinson, Rice and Rosengren (HRR) crack tip singularity fields applied to small scale yielding on the cyclic stress strain curve. A two‐dimensional conduction heat transfer equation, in moving co‐ordinates, was used to obtain temperature distribution around the crack tip. Temperature rise was found to be a function of frequency of loading, applied stress intensity factor and thermal properties of the material. A power–law relation was found between the rise in temperature at a fixed point near the crack tip and range of stress intensity factor.     

SHEAR FATIGUE CRACK GROWTH: A LITERATURE SURVEY

A fatigue crack is often initiated by a localized cyclic plastic deformation in a crystal where the active slip plane coincides with the plane of maximum shear stress. Once a crack is initiated, the crack will propagate on the maximum shear plane for a while and, in the majority of the cases, will eventually change to the plane of the applied tensile stress. The “shear” and “tensile” modes of fatigue crack propagation are termed stage I and stage II fatigue crack growth. They are also known as mode II and mode I fatigue crack growth. However, the mechanism of the tensile mode fatigue crack propagation is shear in nature. Considerable progress has been made recently in the understanding of mode II fatigue crack growth. This paper reviews the various test methods and related data analyses. The combined mode I and mode II elastic crack tip stress field is reviewed. The development and the design of the compact shear specimen are described and the results of fatigue crack growth tests using the compact shear specimens are reviewed. The fatigue crack growth tests and the results of inclined cracks in tensile panels, center cracks in plates under biaxial loading, cracked beam specimens with combined bending and shear loading, center cracked panels and the double edge cracked plates under cyclic shear loading are reviewed and analyzed in detail.     

Monitoring of corrosion‐fatigue degradation of grade R4 steel using an electrochemical‐mechanical combined approach

The study deals with degradation and failure of mooring chains by the combined effect of corrosion and mechanical cyclic stresses on steel. Monitoring of the corrosion‐fatigue damage was carried out using electrochemical assessment during the application of the cyclic mechanical loading on grade R4 martensitic steel specimens, immersed in artificial seawater. The spontaneous potential of the steel specimens and Electrochemical Impedance Spectroscopy measurements were performed to assess the corrosion degradation. Tests conducted under fully reversed stress‐controlled loading have shown earlier failure caused by the corrosive environment when compared with the tests performed in ambient air. The corrosion potential response was used to identify the crack initiation and propagation stages.     

Cyclic loadings and crystallization of natural rubber: An explanation of fatigue crack propagation reinforcement under a positive loading ratio

Natural rubber is known to have excellent fatigue properties. Fatigue crack propagation studies show that, under uniaxial tension loading, fatigue crack growth resistance increases with the loading ratio, even if the peak stress increases. Studies dealing with crack initiation confirm this trend. If strain induced crystallization is believed to play a major role in this reinforcement process, it is not clear yet by which mechanism this reinforcement takes place. Using SEM investigation, it is shown here that the reinforcement process is associated with strong crack branching in the crack tip region. From experimental results it is shown that under particular reinforcing loading condition a cyclic strain hardening process can be observed on the natural rubber which is able to overcome classically observed softening effects. A cumulative strain induced crystallization process is proposed to explain the stress ratio effect on fatigue crack initiation and propagation properties of natural rubber.     

High temperature fatigue of discontinuously-reinforced metal–matrix composites

This paper reviews the current knowledge on the fatigue behavior of discontinuously-reinforced metal–matrix composites at high temperature. The effect of cyclic loading at high temperature on the micromechanims of deformation, crack nucleation, and crack propagation are dealt with. The overall performance of these composites under isothermal and thermo-mechanical fatigue loading have been examined. A brief account of the current industrial applications of discontinuously-reinforced metal–matrix composites in components subjected to fatigue at high temperature is provided     

High-strength biofunctional zirconia: mechanical properties and static fatigue behaviour of zirconia-apatite composites

Zirconia and zirconia-apative (hydroxyl- and fluor-) composites were sintered at 1225°C by glass-encapsulated hot isostatic pressing. In addition to the general assessment of the mechanical properties of the materials, the static fatigue behaviour of the zirconia-hydroxylapatite composite was evaluated by measuring the slow crack propagation at different loads in a circulating 0.9% NaCl solution at 37°C. The mean fracture strengths of the materials in three-point bending mode were 770, 860 and 910 MPa for zirconia-fluorapatite, zirconia-hydroxylapatite and zirconia, respectively. The high value of the slow crack growth stress exponent, calculated from the average strength at the different loading rates, indicates that the zirconia-hydroxylapatite has excellent fatigue resistance in addition to high strength. The even distribution of the apative phases as islets in the zirconia matrix may contribute to mineralization and direct bone apposition to this type of ceramic composites. The machinability of zirconia materials is discussed.