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采用微波提取方法,微波功率为750W,以决明子中蒽醌的含量为考察指标,研究提取溶剂浓度、料液比、提取温度、提取时间等因素对蒽醌提取效果的影响。通过正交试验,确定微波提取决明子中蒽醌的最佳工艺条件为:乙醇浓度70%,料液比1:5,提取温度60℃,提取时间10min,在此条件下获得的总蒽醌提取率为65%。 相似文献
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采用微波蒸馏法提取孜然精油,考察微波溶剂提取和无溶剂提取孜然精油工艺中微波提取时间、微波功率、粒度和液料比等因素对孜然精油提取率的影响。同时以枯茗醛含量作为精油品质的评价指标,并通过GC对孜然精油进行分析。研究结果表明,微波溶剂提取孜然精油的最佳工艺条件为:液料比6:1、微波提取时间90min、微波功率300W,此条件下精油提取率为3.501%,精油中枯茗醛含量为19.121%。微波无溶剂提取孜然精油的最佳工艺条件为:浸泡时间30min、微波提取时间45min、微波功率200W,此条件下精油提取率为2.461%,精油中枯茗醛含量为23.910%。 相似文献
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采用单因素和正交试验设计,应用微波辅助溶剂浸提法提取转心乌洋芋皮天然红色素,对影响色素收率的微波功率、微波时间、提取料液比等主要因素进行了优化组合试验,以确定最佳提取条件。通过试验比较了色素收率结果表明:在微波功率、微波时间、提取料液比三因素中,微波功率对色素收率影响最大,其次是微波时间,提取料液比的影响较小。单因素和正交试验结果确定的最佳工艺组合为:1%HCl水溶液为提取溶剂,微波功率400W,微波时间15min,提取料液比为1:10(g/mL)。在此试验条件下,平行试验3次,转心乌洋芋皮红色素平均收率可达86.79%,与传统溶剂浸提法相比,红色素收率可提高15.85%,微波辅助溶剂浸提法能高效提取转心乌洋芋皮中天然红色素。 相似文献
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茶叶中咖啡因提取方法的比较 总被引:1,自引:0,他引:1
茶叶是人们生活中的重要饮品,我国茶叶的产销量居世界前列。如何更好地高效利用我国每年滞销的5万多吨中低档茶叶,是广大茶叶利用研究工作者和茶农们的共同心声。而茶叶中具有许多生物生理活性物质,其中咖啡因就是当中含量较高的一种。我们以绿茶为原料,通过L16(45)正交试验考察了微波辅助提取法从茶叶中提取咖啡因的影响情况,并以传统的Soxhlet提取法为对照。正交试验表明,从茶叶中提取咖啡因的最佳提取方案为:微波功率0.2kW、提取剂80%(v/v)乙醇、料液比为1:16(m/V)、浸提时间9min(间隙式提取)、温度83±5℃、连续提取3次,使用自制复合中和沉淀剂,咖啡因提取率平均达到217.5mg/10g茶样,较Soxhlet法提取6h的144.8mg/10g茶样高50.2%,最高可达221.8mg/10g茶样,比Soxhlet法的148.8mg/10g茶样高49.1%。而且微波法所得咖啡因的纯度、外观和稳定性等质量指标明显优于Soxhlet法。这为传统的茶叶提取咖啡因工艺的升级改造提供了实验依据。 相似文献
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以决明子红色素浸提率为指标,采用单因素试验法和正交试验法考察了提取剂的类型、料液比、微波功率、萃取时间、次数5个因素。对影响决明子红色素提取的工艺条件进行优化研究。试验结果表明:对微波提取决明子红色素的影响顺序依次为:提取时间〉微波功率〉提取次数〉料液比;优化工艺条件为提取时间4min,微波功率为320W,提取次数为3次,料液比为1:40,溶剂是乙酸乙酯。该条件下进行验证试验,决明子红色素浸提率可达91%。 相似文献
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Since grapevine ( Vitis spp .) rootstock material is being traded increasingly as disbudded woody material a lack of distinctive morphological features on such material necessitates an alternative and reliable means of identification. Methods described here were developed for rapid and efficient extraction of DNA from woody samples rich in phenolic compounds and polysaccharides, and for subsequent identification of varieties by RAPD PCR. Using these methods, and with the application of only one selected RAPD primer, we were able to differentiate sixteen rootstock varieties, including the seven varieties most commonly used in Germany. Problems commonly encountered with reproducibility of RAPD patterns were avoided by choosing primers with a dinucleotide sequence and a high G/C content that allowed a rather high annealing temperature of 45°C. Methods described here should also be useful for other horticultural crops, especially those with woody tissues rich in phenolic compounds and polysaccharides. 相似文献
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John Gilbert Catherine Simoneau David Cote Achim Boenke 《Food Additives & Contaminants》2000,17(10):889-893
An internet website (http://cpf.jrc.it/smt/) has been produced as a means of dissemination of methods of analysis and supporting spectroscopic information on monomers and additives used for food contact materials (principally packaging). The site which is aimed primarily at assisting food control laboratories in the European Union contains analytical information on monomers, starting substances and additives used in the manufacture of plastics materials. A searchable index is provided giving PM and CAS numbers for each of 255 substances. For each substance a data sheet gives regulatory information, chemical structures, physico-chemical information and background information on the use of the substance in particular plastics, and the food packaging applications. For monomers and starting substances (155 compounds) the infra-red and mass spectra are provided, and for additives (100 compounds); additionally proton NMR are available for about 50% of the entries. Where analytical methods have been developed for determining these substances as residual amounts in plastics or as trace amounts in food simulants these methods are also on the website. All information is provided in portable document file (PDF) format which means that high quality copies can be readily printed, using freely available Adobe Acrobat Reader software. The website will in future be maintained and up-dated by the European Commission's Joint Research Centre (JRC) as new substances are authorized for use by the European Commission (DG-ENTR formerly DGIII). Where analytical laboratories (food control or other) require reference substances these can be obtained free-ofcharge from a reference collection housed at the JRC and maintained in conjunction with this website compendium. 相似文献
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Sophie Guillot Laurence Peytavi Sylvie Bureau Renaud Boulanger Jean-Paul Lepoutre Jean Crouzet Sabine Schorr-Galindo 《Food chemistry》2006
The characterization of the aromatic profile of several apricot cultivars with molecular tracers in order to obtain objective data concerning the aromatic quality of this fruit was undertaken using headspace–solid phase microextraction (HS–SPME). Six apricot cultivars were selected according to their organoleptic characteristics: Iranien, Orangered, Goldrich, Hargrand, Rouge du Roussillon and A4025. The aromatic intensity of these varieties measured by HS–SPME–Olfactometry were defined and classified according to the presence and the intensity of grassy, fruity and apricot like notes. In the six varieties, 23 common volatile compounds were identified by HS–SPME–GC–MS. Finally, 10 compounds, ethyl acetate, hexyl acetate, limonene, β-cyclocitral, γ-decalactone, 6-methyl-5-hepten-2-one, linalool, β-ionone, menthone and (E)-hexen-2-al were recognized by HS–SPME–GC–O as responsible of the aromatic notes involved in apricot aroma and considered as molecular tracers of apricot aromatic quality which could be utilized to discriminate apricot varieties. 相似文献
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Jesus Simal-Gandara Miguel Sarria-Vidal Arjen Koorevaar Rinus Rijk 《Food Additives & Contaminants》2000,17(8):703-711
The advent of the functional barrier concept in food packaging has brought with it a requirement for fast tests of permeation through potential barrier materials. In such tests it would be convenient for both foodstuffs and materials below the functional barrier (sub-barrier materials) to be represented by standard simulants. By means of inverse gas chromatography, liquid paraffin spiked with appropriate permeants was considered as a potential simulant of sub-barrier materials based on polypropylene (PP) or similar polyolefins. Experiments were performed to characterize the kinetics of the permeation of low molecular weight model permeants (octene, toluene and isopropanol) from liquid paraffin, through a surrogate potential functional barrier (25 μm-thick oriented PP) into the food simulants olive oil and 3% (w/v) acetic acid. These permeation results were interpreted in terms of three permeation kinetic models regarding the solubility of a particular model permeant in the post-barrier medium (i.e. the food simulant). The results obtained justify the development and evaluation of liquid sub-barrier simulants that would allow flexible yet rigorous testing of new laminated multilayer packaging materials. 相似文献
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Yoko Uematsu Keiko Hirata Kumi Suzuki Kenji Iida Kazuo Saito 《Food Additives & Contaminants》2001,18(2):177-185
BADGE.2HCl and BFDGE.2HCl were determined in 28 samples of ready-to-drink canned coffee and 18 samples of canned vegetables (10 corn, 5 tomatoes and 3 others), all from the Japanese market. HPLC was used as the principal analytical method and GCMS for confirmation of relevant LC fractions. BADGE.2HCl was found to be present in one canned coffee and five samples of corn, BFDGE.2HCl in four samples of canned tomatoes and in one canned corn. No sample was found which exceeded the 1mg/kg limit of the EU for the BADGE chlorohydrins. However the highest concentration was found for the sum of BFDGE.2HCl and BFDGE.HCl.H2O at a level of 1.5mg/kg. A Beilstein test confirmed that all cans containing foods contaminated with BADGE.2HCl or BFDGE.2HCl had at lest one part coated with a PVC organosol. 相似文献
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A strong science base is required to underpin the planning and decision-making process involved in determining future European community legislation on materials and articles in contact with food. Significant progress has been made in the past 5 years in European funded work in this area, with many developments contributing to a much better understanding of the migration process, and better and simpler approaches to food control. In this paper this progress is reviewed against previously identified work-areas (identified in 1994) and conclusions are reached about future requirements for R&D to support legislation on food contact materials and articles over the next 5 or so years. 相似文献
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M. S. Garcí a-Falc n J. Simal-G ndara S. T. Carril-Gonz lez-Barros 《Food Additives & Contaminants》2000,17(12):957-964
A simple, rapid and inexpensive method has been developed for the determination of benzo[a 相似文献
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H. J. Van Den Top A. Boenke P. A. Burdaspal J. Bustos H. P. Van Egmond T. Legarda A. Mesego A. Mourino W. E. Paulsch C. Salgado 《Food Additives & Contaminants》2001,18(9):810-824
This paper describes the second part of a project undertaken to develop certified mussel reference materials for paralytic shellfish poisoning toxins. In the first part two interlaboratory studies were undertaken to investigate the performance of the analytical methodology for several PSP toxins, in particular saxitoxin and decarbamoyl-saxitoxin in lyophilized mussels, and to set criteria for the acceptance of results to be applied during the certification exercise. Fifteen laboratories participated in this certification study and were asked to measure saxitoxin and decarbamoyl-saxitoxin in rehydrated lyophilized mussel material and in a saxitoxin-enriched mussel material. The participants were allowed to use a method of their choice but with an extraction procedure to be strictly followed. The study included extra experiments to verify the detection limits for both saxitoxin and decarbamoyl-saxitoxin. Most participants (13 of 15) were able to meet all the criteria set for the certification study. Results for saxitoxin.2HCl yielded a certified mass fraction of <0.07 mg/kg in the rehydrated lyophilized mussels. Results obtained for decarbamoyl-saxitoxin.2HCl yielded a certified mass fraction of 1.59+/-0.20 mg/kg. The results for saxitoxin.2HCl in enriched blank mussel yielded a certified mass fraction of 0.48 +/- 0.06 mg/kg. These certified reference materials for paralytic shellfish poisoning toxins in lyophilized mussel material are the first available for laboratories to test their method for accuracy and performance. 相似文献
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《肉类研究》2014,(2)
<正>We are pleased to announce the launch of a new international peer-reviewed journal-Food Science and Human Wellness,ISSN 2213-4530,which is an open access journal,produced and hosted by Elsevier B.V.on behalf of Beijing Academy of Food Sciences.Food Science and Human Wellness is an international peer-reviewed English journal that provides a forum for the dissemination of the 相似文献